US3634093A
Expired / Lapsed
US
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Detoxication of tung meal
Assignee: University of Mississippi
•
Filing: 1969-10-14
•
Granted: 1972-01-11
•
Expires: 1989-10-14
Abstract
Abstract Commercial tung meal may be detoxicated to prepare an animal feed or fertilizer rich in protein and carbohydrate by macerating the meal in water followed by the extraction of toxic substances therefrom with an alcohol.
Inventors
- 👤 Chian L Huang
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-09 04:59
CPC Classifications
A; A23; A23L; A23L5/00; A23L5/20; A23L5/23; Y; Y10; Y10S; Y10S426/00; Y10S426/807
Claims Analysis
Total Claims: 24
Claim 1
Independent Claim
29 words
in process step (c) the dewatered swollen tung meal is treated with about three times its weight of alcohol at a temperature of 60* C. for about 1 hour.
Claim 2
Dependent Claim
23 words
The process of claim 1 wherein step (a) is conducted in conditions substantially resistant to fermentation and continued for at least 1 hour.
Claim 3
Dependent Claim
44 words
in process step (c) the dewatered swollen tung meal is treated with from about one to about 10 times its weight of a lower alcohol at a temperature of about 0* C. to about 100* C. for a period of at least one-half hour.
Claim 4
Dependent Claim
34 words
in process step (b) the sifted tung meal is soaked in water at a temperature of about 0* C. to 100* C. for a period of from about 1 to about 96 hours; and
Claim 5
Dependent Claim
31 words
in process step (b) the sifted tung meal is soaked in three times its weight of water at a temperature of about 80* C. for about 12 hours while being agitated;
Claim 6
Dependent Claim
57 words
in process step (d) the toxic matter is extracted by contact with about three times its weight of an alcohol selected from a group consisting of methanol, ethanol, propanol, butanol, and pentanol at a temperature of about 60* C. for about an hour while being agitated, and wherein the tung meal is dried following process step (e).
Claim 7
Dependent Claim
43 words
in process step (d) the water-soaked swollen dewatered tung meal is treated with about one to 10 times its weight of the alcohol at a temperature of about 0* C. to about 100* C. for a period of about 1/2 to 24 hours.
Claim 8
Dependent Claim
25 words
The process of claim 1 wherein the organic solvent is selected from the group consisting of saturated alcohols containing from one to nine carbon atoms.
Claim 9
Dependent Claim
21 words
The process of claim 3 wherein step (a) is conducted in a substantially acid condition to provide substantial resistance to fermentation.
Claim 10
Dependent Claim
11 words
The process of claim 1 wherein the organic solvent is ethanol.
Claim 11
Dependent Claim
17 words
The process of claim 1 wherein the acid condition is a pH value of 1 to 3.
Claim 12
Dependent Claim
6 words
The process of claim 1 wherein:
Claim 13
Dependent Claim
6 words
The process of claim 1 wherein:
Claim 14
Dependent Claim
28 words
The process of claim 8 wherein step (c) is repeated from one to 19 times and the alcoholic solution of toxic matter is removed between treatments with alcohol.
Claim 15
Dependent Claim
10 words
The process of claim 9 wherein the alcohol is ethanol.
Claim 16
Dependent Claim
14 words
The process of claim 10 wherein the step (c) is repeated three additional times.
Claim 17
Dependent Claim
105 words
A sequential process for preparing a foodstuff from tung meal containing particulate tung hull, which comprises: a. removing a portion of the hull mAterial from the tung meal; b. soaking the tung meal in from about one to about 10 times its weight of water at a pH from about 0.1 to 7.0, to macerate, and swell the meal and to dissolve water-soluble toxic matter; c. separating the water and dissolved toxic matter from the swollen tung meal; d. extracting toxic matter from the dewatered swollen tung meal with a lower aliphatic alcohol; and e. separating the alcohol and toxic matter from the tung meal.
Claim 18
Dependent Claim
17 words
The process of claim 12 wherein the sequence (d) through (e) is repeated two to 20 times.
Claim 19
Dependent Claim
14 words
The process of claim 12 wherein the tung meal is dried after step (e).
Claim 20
Dependent Claim
6 words
The process of claim 12 wherein:
Claim 21
Dependent Claim
6 words
The process of claim 15 wherein:
Claim 22
Dependent Claim
10 words
The process of claim 16 wherein the alcohol is ethanol.
Claim 23
Dependent Claim
24 words
The process of claim 16 wherein the sequence of process steps (d) thru (e) is repeated three additional times prior to the drying step.
Claim 24
Dependent Claim
10 words
The process of claim 18 wherein the alcohol is ethanol.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1975-01-10 | 1975-07-12 | 1976-01-11 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1979-01-10 | 1979-07-12 | 1980-01-11 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1983-01-10 | 1983-07-12 | 1984-01-11 | $7700.00 | Window Closed / Lapsed |