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US3645127A Expired / Lapsed US ⏱️ 0.0 years remaining

Remote leak detection

Assignee: VEECO INSTRUMENTS ACQUISITION CORP
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Filing: 1970-01-12
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Granted: 1972-02-29
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Expires: 1990-01-12
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Abstract

Abstract In a method and apparatus for remote detection of leaks in vessels wherein the vessel to be tested is pressurized with a tracer gas and a hand probe connected via a flexible conduit to a mass spectrometer apparatus is used to selectively sample the atmosphere near the surface of the vessel, a continuous flow of a condensable carrier gas of a different molecular weight than the tracer gas is injected into the vacuum system near the probe tracer inlet to increase capillary conductance and thereby cut down on response time as well as to sweep the line clean of residual tracer gas molecules and thereby prevent background indications. The carrier gas is condensed at a cold trap in the conduit upstream of the analytical portion of the mass spectrometer apparatus and thereby pumped out of the system.

Inventors

  • 👤 Guy E Mongodin
  • 👤 Leon Malmed

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-26 00:57
CPC Classifications
G; G01; G01M; G01M3/00; G01M3/02; G01M3/04; G01M3/20; G01M3/202

Claims Analysis

Total Claims: 10
Claim 1
Independent Claim 330 words
Improved apparatus for detecting and locating leaks in vessels which have been pressurized with tracer gas of a selected molecular weight, said apparatus being characterized by short response times and the absence of background indications, comprising a. mass spectrometer means for quantitatively detecting and indicating the presence therein of molecules of said tracer gas, said mass spectrometer means having vacuum means For drawing selected atmospheric samples through said mass spectrometer means and for maintaining a suitable vacuum environment therein; b. flexible vacuum conduit means operatively connected to said mass spectrometer means for conducting said selected atmospheric samples thereto; c. a source of a continuous viscous flow of a carrier medium for increasing the capillary conductance of said vacuum conduit and preventing tracer gas hang-up therein, said supply source including flexible carrier conduit means; d. sniffer probe means operatively coupled to said flexible vacuum conduit means and said flexible carrier conduit means for probing the outer surface of the vessel under leak test, said sniffer means comprising sample inlet means for selectively sampling the atmosphere at the outer surface of said vessel for the presence of tracer gas molecules, and carrier inlet means in communication with said flexible carrier conduit means, said sniffer means further comprising a series of passageways leading from said carrier inlet means to said sample inlet means and then to said flexible vacuum conduit means for injecting a carrier medium stream into said vacuum system at a point in proximity to said sample inlet means so that any tracer gas molecules entering with said atmospheric samples will immediately be caught up by said carrier stream and conducted through said vacuum conduit to said spectrometer apparatus in a viscous flow; and e. carrier trap means associated with said mass spectrometer means on the upstream side thereof for removing said carrier medium from said vacuum system upstream of the analytical portion of said mass spectrometer means so that said carrier medium has no effect on the operating environment thereof.
Claim 2
Dependent Claim 330 words
Improved apparatus for detecting and locating leaks in vessels which have been pressurized with tracer gas of a selected molecular weight, said apparatus being characterized by short response times and the absence of background indications, comprising a. mass spectrometer means for quantitatively detecting and indicating the presence therein of molecules of said tracer gas, said mass spectrometer means having vacuum means For drawing selected atmospheric samples through said mass spectrometer means and for maintaining a suitable vacuum environment therein; b. flexible vacuum conduit means operatively connected to said mass spectrometer means for conducting said selected atmospheric samples thereto; c. a source of a continuous viscous flow of a carrier medium for increasing the capillary conductance of said vacuum conduit and preventing tracer gas hang-up therein, said supply source including flexible carrier conduit means; d. sniffer probe means operatively coupled to said flexible vacuum conduit means and said flexible carrier conduit means for probing the outer surface of the vessel under leak test, said sniffer means comprising sample inlet means for selectively sampling the atmosphere at the outer surface of said vessel for the presence of tracer gas molecules, and carrier inlet means in communication with said flexible carrier conduit means, said sniffer means further comprising a series of passageways leading from said carrier inlet means to said sample inlet means and then to said flexible vacuum conduit means for injecting a carrier medium stream into said vacuum system at a point in proximity to said sample inlet means so that any tracer gas molecules entering with said atmospheric samples will immediately be caught up by said carrier stream and conducted through said vacuum conduit to said spectrometer apparatus in a viscous flow; and e. carrier trap means associated with said mass spectrometer means on the upstream side thereof for removing said carrier medium from said vacuum system upstream of the analytical portion of said mass spectrometer means so that said carrier medium has no effect on the operating environment thereof.
Claim 3
Dependent Claim 28 words
Apparatus as defined in claim 1 wherein said carrier medium is a condensable gas and said carrier trap means comprises a cold trap for condensing said carrier gas.
Claim 4
Dependent Claim 20 words
Apparatus as defined in claim 2 wherein said carrier gas is of a different molecular weight than said tracer gas.
Claim 5
Dependent Claim 13 words
Apparatus as defined in claim 2 wherein said carrier gas is carbon dioxide.
Claim 6
Dependent Claim 18 words
Apparatus as defined in claim 2 wherein said carrier source is at a pressure no less than atmospheric.
Claim 7
Dependent Claim 64 words
Apparatus as defined in claim 2 further comprising first pressure gauge means for determining and indicating the fluid pressure in said system on the upstream side of said cold trap and second pressure gauge means for determining and indicating the fluid pressure in said system on the immediate downstream side of said cold trap upstream of the analytical portion of said mass spectrometer apparatus.
Claim 8
Dependent Claim 56 words
Apparatus as defined in claim 1 further comprising sample inlet adjustment means for controlling said sample inlet means to regulate the sensitivity of said apparatus, and carrier inlet adjustment means for controlling said carrier inlet means to regulate the flow pressure of said carrier medium and thereby the capillary conductance of said flexible vacuum conduit means.
Claim 9
Dependent Claim 142 words
In a leak detection method which includes pressurizing the vessel under leak test with a tracer gas of a selected molecular weight and employs mass spectrometer apparatus having a vacuum source connected via flexible tubulation to a hand probe for quantitatively analyzing samples of the atmosphere at the outside of the vessel wall for tracer gas molecules, an improvement for shortening response times and eliminating tracer gas hang-up in said tubulation which comprises increasing the capillary conductance of said interconnecting tubulation and simultaneously continuously purging said tubulation of tracer gas molecules by injecting into said vacuum system at a point in proximity to the sample inlet thereof a continuous viscous flow of a condensable carrier gas and thereafter condensing said carrier gas out of said system downstream of said interconnecting tubulation and upstream of the analytical portion of said mass spectrometer apparatus.
Claim 10
Dependent Claim 142 words
In a leak detection method which includes pressurizing the vessel under leak test with a tracer gas of a selected molecular weight and employs mass spectrometer apparatus having a vacuum source connected via flexible tubulation to a hand probe for quantitatively analyzing samples of the atmosphere at the outside of the vessel wall for tracer gas molecules, an improvement for shortening response times and eliminating tracer gas hang-up in said tubulation which comprises increasing the capillary conductance of said interconnecting tubulation and simultaneously continuously purging said tubulation of tracer gas molecules by injecting into said vacuum system at a point in proximity to the sample inlet thereof a continuous viscous flow of a condensable carrier gas and thereafter condensing said carrier gas out of said system downstream of said interconnecting tubulation and upstream of the analytical portion of said mass spectrometer apparatus.

References Cited (Backward Citations)

US2706398A Cited
US2996661A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1975-02-28 1975-08-30 1976-02-29 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1979-02-28 1979-08-30 1980-02-29 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1983-02-28 1983-08-30 1984-02-29 $7700.00 Window Closed / Lapsed

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