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US3848469A Expired / Lapsed US ⏱️ 0.0 years remaining

Sample introduction system for gas chromatograph

Assignee: Individual
•
Filing: 1973-04-04
•
Granted: 1974-11-19
•
Expires: 1993-04-04
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Abstract

Abstract A system for the introduction of a liquid, a vaporous or a gaseous sample into gas chromatographs comprises a sampler unit and a sample inlet unit. The two units intercommunicate by means of passages provided with sealing bushings in which a metering element moves which is formed as a bent tube with rods. The metering element is filled with a sample at the instant the ports of the tube communicate with the chambers of the sampler unit, and the sample introduction process is effected at the instant the ports of the tube communicate with the chambers of the sample inlet unit. The sample is forced out of the metering element due to the pressure differential between the sample receiving chamber and the over-pressure chamber.

Inventors

  • 👤 L Chizhov

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-27 13:24
CPC Classifications
G; G01; G01N; G01N30/00; G01N30/02; G01N30/04; G01N30/24; G01N30/16

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 275 words
A sample introduction system for gas chromatographs, comprising: a sampler unit having a flow-type filling chamber hermetically sealed from the atmosphere and an exhaust chamber; two connecting passageways communicating said filling chamber with said sample; a passageway connecting said exhaust chamber, for venting to the atmosphere; a sample inlet unit having a sample receiving chamber sealed froM the atmosphere and communicating with a source of carrier gas and a chromatographic column, an overpressure chamber communicating with said carrier gas source and vented to the atmosphere; means for providing a pressure differential between said sample receiving chamber and said overpressure chamber; passages provided with sealing bushings, between said filling chamber and said sample receiving chamber and between said exhaust chamber and said overpressure chamber; a metering element formed as a bent tube with parallel ends pointing in the same direction; exit ports formed in said tube ends; rods connected with said ends of said tube beyond said exit ports, said tube and rods being slidably mounted in said sealing bushings and being capable of reciprocating between two fixed positions so that in one said fixed position of said tube with rods and said exit ports of said tube communicate with the said chambers of said sampler unit, with said chambers of said sample inlet unit being sealed from said chambers of said sampler unit by the outer surfaces of said rods, whereas in the other fixed position said exit ports of said tube communicate with said chambers of said sample inlet unit, with said chambers of said sample inlet unit being sealed from said chambers of said sampler unit by the outer surface of said tube.
Claim 2
Dependent Claim 275 words
A sample introduction system for gas chromatographs, comprising: a sampler unit having a flow-type filling chamber hermetically sealed from the atmosphere and an exhaust chamber; two connecting passageways communicating said filling chamber with said sample; a passageway connecting said exhaust chamber, for venting to the atmosphere; a sample inlet unit having a sample receiving chamber sealed froM the atmosphere and communicating with a source of carrier gas and a chromatographic column, an overpressure chamber communicating with said carrier gas source and vented to the atmosphere; means for providing a pressure differential between said sample receiving chamber and said overpressure chamber; passages provided with sealing bushings, between said filling chamber and said sample receiving chamber and between said exhaust chamber and said overpressure chamber; a metering element formed as a bent tube with parallel ends pointing in the same direction; exit ports formed in said tube ends; rods connected with said ends of said tube beyond said exit ports, said tube and rods being slidably mounted in said sealing bushings and being capable of reciprocating between two fixed positions so that in one said fixed position of said tube with rods and said exit ports of said tube communicate with the said chambers of said sampler unit, with said chambers of said sample inlet unit being sealed from said chambers of said sampler unit by the outer surfaces of said rods, whereas in the other fixed position said exit ports of said tube communicate with said chambers of said sample inlet unit, with said chambers of said sample inlet unit being sealed from said chambers of said sampler unit by the outer surface of said tube.
Claim 3
Dependent Claim 69 words
A sample introduction system as claimed in claim 1, wherein said rods are solid and connected to the end surfaces of said tube in tight relation thereto, the outer diameter of said tube being equal to the diameter of said rods, and said exit ports of the tube are formed in the lateral surface thereof at the point of connection of said rods with the ends of said tube.
Claim 4
Dependent Claim 26 words
A sample introduction system as claimed in claim 1, wherein said sealing bushings are elastically urged in the direction of the motion of said metering element.
Claim 5
Dependent Claim 59 words
A sample introduction system as claimed in claim 1, incorporating a check valve provided at the gas carrier entrance passage in said sample receiving chamber, the check valve being formed as a passage, whereinto said rod of said metering element enters at the instant of sample introduction, the diameter of said passage being equal to that of said rod.

References Cited (Backward Citations)

US2991647A Cited
GB954067A Cited
US3401565A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1977-11-18 1978-05-20 1978-11-19 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1981-11-18 1982-05-20 1982-11-19 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1985-11-18 1986-05-20 1986-11-19 $7700.00 Window Closed / Lapsed

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