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US3865554A Expired / Lapsed US ⏱️ 0.0 years remaining

Pressure-and temperature-controlled apparatus for large-scale production of crystals by the czochralski technique

Assignee: Arthur D Little Inc
•
Filing: 1971-09-23
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Granted: 1975-02-11
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Expires: 1991-09-23
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Abstract

Abstract Furnace assembly providing a working volume the pressure in which may range from 10 5 torr to 135 atmospheres. Controlled temperatures up to 3,000*C are attainable. A crystal-pulling rod and a crucible-supporting rod extend into the furnace. The crystal-pulling rod is rotated and driven translationally through an extended excursion in a slow crystal-pulling mode and relatively fast positioning mode; while the crucible support rod is rotated and driven translationally through a relatively short excursion in a crucible positioning mode. The main furnace housing is lifted up and swung away to permit ready access to the crucible holding zone for interchange of rf coils and crucible holders as well as for easy safe removal of large crystals suspended from the pulling rod. Means are provided continuously to indicate the precise position of the crystal-pulling rod, to monitor the operation within the furnace by TV, and to control the operations within the furnace from a remote location.

Inventors

  • 👤 Joseph F Wenckus
  • 👤 Roger A Castonguay
  • 👤 Bernard C Hanfly
  • 👤 Francis J Mallahan

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-05 13:12
CPC Classifications
C; C30; C30B; C30B15/00; C30B15/30; Y; Y10; Y10T; Y10T117/00; Y10T117/10; Y10T117/1004; Y10T117/1008; Y10T117/1024; Y10T117/1032; Y10T117/1072

Claims Analysis

Total Claims: 13
Claim 1
Independent Claim 245 words
A PRESSURE- AND TEMPERATURE-CONTROLLED APPARATUS ADAPTED FOR GROWING CRYSTALS BY THE CZOCHRALSKI TECHNIQUE, COMPRISING IN COMBINATION A. PRESSURE-TIGHT FURNACE MEANS PROVIDING AN ENCLOSURE DIFINING THEREIN A WORKING VOLUME THE ATMOSPHERE OF WHICH MAY BE VARIED WITH RESPECT TO TEMPERATURE AND TO PRESSURE FROM A VACUUM TO AT LEAST 100 ATMOSPHERES, SAID FURNACE MEANS BEING FORMED OF A MAIN CYLINDRICAL FURNACE HOUSING OF ESSENTIALLY CONSTANT DIAMETER THROUGHOUT HAVING A TOP SECTION AND BOTTOM FLANGE MEANS AND A FURNACE BASE MEMBER HAVING THE SAME INSIDE DIAMETER AS SAID MAIN FURNACE HOUSING AND BEING SEALABLE WITH SAID MAIN FURMACE HOUSING THROUGH MATING FLANGE MEANS TO LIMIT SAID ATMOSPHERE ESSENTIALLY TO SAID VOLUME; B. FURNACE SEALING MEANS ENGAGEABLE WITH SAID MATING FLANGE MEANS AND COMPRISING TWO SEMICIRCULAR, INTERNALLY GROOVED MEMBERS AND BOLT MEANS ADAPTED TO LOCK SAID GROOVED MEMBERS IN ENGAGED POSITION AROUND SAID MATING FLANGE MEANS; C. CRYSTAL-PULLING ROD MEANS EXTENDING FROM EXTERNAL OF SAID MAIN FURNACE HOUSING INTO SAID VOLUME AND MOVABLE THEREIN IN BOTH ROTATIONAL AND TRANSLATIONAL MODES D. CRYSTAL-PULLING ROD BEARING AND SEALING ASSEMBLY MEANS LOCATED IN SAID TOP SECTION OF SAID MAIN FURNACE HOUSING AND PROVIDING THE SOLE SEALING MEANS BETWEEN SAID CRYSTAL-PULLING ROD MEANS AND SAID PRESSURE-TIGHT FURNACE MEANS; E. ROTATIONAL AND TRANSLATION CRYSTAL-PULLING ROD DRIVING MEANS LOCATED EXTERNAL OF SAID PRESSURE-TIGHT FURNACE MEANS AND RIGIDLY MOUNTED ON SAID MAIN FURNACE HOUSING, SAID TRANSLATIONAL DRIVING MEANS INCLUDING MEANS TO SELECTIVELY DRIVE SAID RODS IN A SLOW CRYSTAL-GROWING MODE OR IN A RIPID-POSITIONING MODE;
Claim 2
Dependent Claim 245 words
A PRESSURE- AND TEMPERATURE-CONTROLLED APPARATUS ADAPTED FOR GROWING CRYSTALS BY THE CZOCHRALSKI TECHNIQUE, COMPRISING IN COMBINATION A. PRESSURE-TIGHT FURNACE MEANS PROVIDING AN ENCLOSURE DIFINING THEREIN A WORKING VOLUME THE ATMOSPHERE OF WHICH MAY BE VARIED WITH RESPECT TO TEMPERATURE AND TO PRESSURE FROM A VACUUM TO AT LEAST 100 ATMOSPHERES, SAID FURNACE MEANS BEING FORMED OF A MAIN CYLINDRICAL FURNACE HOUSING OF ESSENTIALLY CONSTANT DIAMETER THROUGHOUT HAVING A TOP SECTION AND BOTTOM FLANGE MEANS AND A FURNACE BASE MEMBER HAVING THE SAME INSIDE DIAMETER AS SAID MAIN FURNACE HOUSING AND BEING SEALABLE WITH SAID MAIN FURMACE HOUSING THROUGH MATING FLANGE MEANS TO LIMIT SAID ATMOSPHERE ESSENTIALLY TO SAID VOLUME; B. FURNACE SEALING MEANS ENGAGEABLE WITH SAID MATING FLANGE MEANS AND COMPRISING TWO SEMICIRCULAR, INTERNALLY GROOVED MEMBERS AND BOLT MEANS ADAPTED TO LOCK SAID GROOVED MEMBERS IN ENGAGED POSITION AROUND SAID MATING FLANGE MEANS; C. CRYSTAL-PULLING ROD MEANS EXTENDING FROM EXTERNAL OF SAID MAIN FURNACE HOUSING INTO SAID VOLUME AND MOVABLE THEREIN IN BOTH ROTATIONAL AND TRANSLATIONAL MODES D. CRYSTAL-PULLING ROD BEARING AND SEALING ASSEMBLY MEANS LOCATED IN SAID TOP SECTION OF SAID MAIN FURNACE HOUSING AND PROVIDING THE SOLE SEALING MEANS BETWEEN SAID CRYSTAL-PULLING ROD MEANS AND SAID PRESSURE-TIGHT FURNACE MEANS; E. ROTATIONAL AND TRANSLATION CRYSTAL-PULLING ROD DRIVING MEANS LOCATED EXTERNAL OF SAID PRESSURE-TIGHT FURNACE MEANS AND RIGIDLY MOUNTED ON SAID MAIN FURNACE HOUSING, SAID TRANSLATIONAL DRIVING MEANS INCLUDING MEANS TO SELECTIVELY DRIVE SAID RODS IN A SLOW CRYSTAL-GROWING MODE OR IN A RIPID-POSITIONING MODE;
Claim 3
Dependent Claim 26 words
An apparatus according to claim 1 wherein said pressure-tight furnace means includes external cooling means in the form of coils adapted to circulate a fluid coolant.
Claim 4
Dependent Claim 23 words
An apparatus according to claim 1 wherein said pressure-tight furnace means has associated therewith a self-resetting pressure-relief valve and a solenoid-actuated relief valve.
Claim 5
Dependent Claim 25 words
An apparatus according to claim 1 wherein said pressure-tight furnace means includes audible pressure warning means associated with and actuated by said furnace sealing means.
Claim 6
Dependent Claim 22 words
An apparatus according to claim 1 wherein said crystal-pulling rod means incorporates fluid channels therein adapted to circulate a fluid coolant therethrough.
Claim 7
Dependent Claim 24 words
An apparatus according to claim 1 wherein said crucible-support rod means provides a passage for thermocouple lead wires extending into said crucible holding means.
Claim 8
Dependent Claim 42 words
An apparatus according to claim 1 wherein said main furnace housing support and lifting means comprises a hydraulically operated lifting shaft attached to said main furnace housing and means to prevent the rotation of said shaft until it reaches said predetermined height.
Claim 9
Dependent Claim 65 words
An apparatus according to claim 1 wherein said crucible holding means comprises a crucible holder terminating at its lower end in a neck member adapted for attachment through a collar member to said crucible-support rod, and outer shielding means surrounding said crucible holder, said crucible holder and said outer shielding means being readily interchangeable, thereby providing means to hold crucibles of varying sizes and configurations.
Claim 10
Dependent Claim 19 words
An apparatus according to claim 1 wherein said heating means comprise rf coil means surrounding said crucible holding means.
Claim 11
Dependent Claim 19 words
An apparatus according to claim 1 wherein said heating means comprise resistance heater means surrounding said crucible holding means.
Claim 12
Dependent Claim 36 words
An apparatus according to claim 10 wherein said resistance heater means comprises a graphite resistance heater, a copper pad, means to circulate a liquid coolant in said copper pad, and means to support said heater means.
Claim 13
Dependent Claim 39 words
An apparatus according to claim 1 wherein said heating means has leads terminating in connecting means engageable with connecting means positioned within said furnace base member, whereby said heating means may be readily interchanged to accommodate different sized crucibles.

References Cited (Backward Citations)

US3002320A Cited
US3372003A Cited
US3353914A Cited
US3337303A Cited
US3493770A Cited
US3501406A Cited
US3552931A Cited
US3650701A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-02-10 1978-08-12 1979-02-11 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-02-10 1982-08-12 1983-02-11 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-02-10 1986-08-12 1987-02-11 $7700.00 Window Closed / Lapsed

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