US3888816A
Expired / Lapsed
US
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Process for producing bound aggregate building material
Assignee: Qo Chemicals Inc
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Filing: 1973-06-18
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Granted: 1975-06-10
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Expires: 1993-06-18
Abstract
Abstract A process for producing a bound aggregate building material composition comprising: (a) forming a monomeric binder mixture of specified amounts of monomeric furfuryl alcohol and a silane coupling agent of the general formula: X-R''-Si(OR'''')3 wherein R'' is a short chain alkylene radical; R'''' is aryl, substituted aryl, alkyl, or heteroalkyl; and X is amino, mercapto, epoxy, or glycidoxy; (b) forming a mixture of specified amounts of aggregate and acidic catalyst; (c) admixing specified amounts of the monomeric binder with specified amounts of the aggregate-acidic catalyst mixture.
Inventors
- 👤 Lloyd H Brown
- 👤 Daniel S P Eftax
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-09 14:08
CPC Classifications
C; C08; C08L; C08L71/00; C08L71/08; C08L71/14; C04; C04B; C04B26/00; C04B26/02; C04B26/10; C04B26/105
Claims Analysis
Total Claims: 19
Claim 1
Independent Claim
51 words
A PROCESS FPR MATERIAL COMPOSITION CONSISTING ESSENTIALLY OF THE STEPS OF: A. FORMING A FIRST MIXTURE COMPRISING A MONOMERIC BINDER MIXTURE OF FROM 99.5 PERCENT TO 99.9875 PERCENT BY WEIGHT MONOMERIC FURFURYL ACHOLOL, AND FROM 0.5 PERCENT TO 0.125 PERCENT BY WEIGHT OF A SILANE COUPLING AGENT OR THE GENERAL FORMULA:
Claim 2
Dependent Claim
51 words
A PROCESS FPR MATERIAL COMPOSITION CONSISTING ESSENTIALLY OF THE STEPS OF: A. FORMING A FIRST MIXTURE COMPRISING A MONOMERIC BINDER MIXTURE OF FROM 99.5 PERCENT TO 99.9875 PERCENT BY WEIGHT MONOMERIC FURFURYL ACHOLOL, AND FROM 0.5 PERCENT TO 0.125 PERCENT BY WEIGHT OF A SILANE COUPLING AGENT OR THE GENERAL FORMULA:
Claim 3
Dependent Claim
39 words
A process as in claim 1 wherein said first mixture includes from 2 percent to 10 percent by weight of aqueous urea-formaldehyde mixture and said aqueous urea-formaldehyde mixture contains from 5 percent to about 25 percent by weight water.
Claim 4
Dependent Claim
15 words
The process as in claim 1 in which said acidic catalyst is toluene sulfonic acid.
Claim 5
Dependent Claim
12 words
The process of claim 1 wherein said silane coupling agent is gamma-aminopropyltriethoxysilane.
Claim 6
Dependent Claim
12 words
The process of claim 1 wherein said silane coupling agent is gamma-mercaptopropyltrimethoxysilane.
Claim 7
Dependent Claim
12 words
The process of claim 1 wherein said silane coupling agent is N-beta-(aminoethyl)-gamma-aminopropyltrimethoxysilane.
Claim 8
Dependent Claim
12 words
The process of claim 1 wherein said silane coupling agent is beta-(3,4-epoxycyclohexyl)ethyltrimethoxysilane.
Claim 9
Dependent Claim
12 words
The process of claim 1 wherein said silane coupling agent is gamma-glycidoxypropyltrimethoxysilane.
Claim 10
Dependent Claim
12 words
The process of claim 1 wherein said silane coupling agent is gamma-aminopropyltriphenoxysilane.
Claim 11
Dependent Claim
12 words
The process of claim 1 wherein said silane coupling agent is gamma-aminopropyltribenzyloxysilane.
Claim 12
Dependent Claim
12 words
The process of claim 1 wherein said silane coupling agent is gamma-aminopropyltrifurfuroxysilane.
Claim 13
Dependent Claim
12 words
The process of claim 1 wherein said silane coupling agent is gamma-aminopropyltri(o-chlorophenoxy)silane.
Claim 14
Dependent Claim
12 words
The process of claim 1 wherein said silane coupling agent is gamma-aminopropyltri(p-chlorophenoxy)silane.
Claim 15
Dependent Claim
12 words
The process of claim 1 wherein said silane coupling agent is gamma-aminopropyltri(tetrahydrofurfuroxy)silane.
Claim 16
Dependent Claim
219 words
A process for producing a bound aggregate building material composition comprising the steps of: a. forming a first package comprising a monomeric binder mixture of from 99 1/2 percent to 99 7/8 percent by weight monomeric furfuryl alcohol and from 1/2 percent to 1/8 percent by weight of a silane coupling agent of the general formula: X-R''-Si-(OR'''')3 wherein R'' is a short chain alkylene containing between about 3 and 6 carbon atoms; R'''' is a radical selected from the group consisting of aryl, alkyl, substituted aryl, and heteroalkyl; and X is a reactive member selected from thE group consisting of amino, mercapto, epoxy, and glycidoxy; b. forming a second package comprising a mixture of aggregate and acidic catalyst, said aggregate and said acidic catalyst being mixed in a proportion such that when from 2 percent to 20 percent by weight monomeric binder is mixed with from 98 percent to 80 percent by weight of the aggregate-acidic catalyst mixture, the acidic catalyst is present in an amount of from 5 percent to 50 percent by weight of the monomeric binder; and c. admixing said first package and said second package in an amount such that the first package contributes from 2 percent to 20 percent by weight and said second package contributes from 98 percent to 80 percent by weight.
Claim 17
Dependent Claim
219 words
A process for producing a bound aggregate building material composition comprising the steps of: a. forming a first package comprising a monomeric binder mixture of from 99 1/2 percent to 99 7/8 percent by weight monomeric furfuryl alcohol and from 1/2 percent to 1/8 percent by weight of a silane coupling agent of the general formula: X-R''-Si-(OR'''')3 wherein R'' is a short chain alkylene containing between about 3 and 6 carbon atoms; R'''' is a radical selected from the group consisting of aryl, alkyl, substituted aryl, and heteroalkyl; and X is a reactive member selected from thE group consisting of amino, mercapto, epoxy, and glycidoxy; b. forming a second package comprising a mixture of aggregate and acidic catalyst, said aggregate and said acidic catalyst being mixed in a proportion such that when from 2 percent to 20 percent by weight monomeric binder is mixed with from 98 percent to 80 percent by weight of the aggregate-acidic catalyst mixture, the acidic catalyst is present in an amount of from 5 percent to 50 percent by weight of the monomeric binder; and c. admixing said first package and said second package in an amount such that the first package contributes from 2 percent to 20 percent by weight and said second package contributes from 98 percent to 80 percent by weight.
Claim 18
Dependent Claim
223 words
A process of producing a bound aggregate building material composition comprising the steps of: a. forming a first package consisting essentially of a monomeric binder mixture of from 99 1/2 percent to 99 7/8 percent by weight monomeric furfuryl alcohol and from 1/2 percent to 1/8 percent by weight of a silane coupling agent of the general formula: X-R''-Si-(OR'''')3 wherein R'' is a short chain alkylene containing between about 3 and 6 carbon atoms; R'''' is a radical selected from the group consisting of aryl, alkyl, substituted aryl, and heteroalkyl; and X is a reactive member selected from the group consisting of amino, mercapto, epoxy, and glycidoxy; b. forming a second package consisting essentially of a mixture of aggregate and acidic catalyst, said aggregate and said acidic catalyst being mixed in a proportion such that when from 2 percent to 20 percent by weight monomeric binder is mixed with from 98 percent to 80 percent by weight of the aggregate-acidic catalyst mixture, the acidic catalyst is present in an amount of from 5 percent to 50 percent by weight of the monomeric binder; and c. admixing said first package and said second package in an amount such that the first package contributes from 2 percent to 20 percent by weight and said second package contributes from 98 percent to 80 percent by weight.
Claim 19
Dependent Claim
223 words
A process of producing a bound aggregate building material composition comprising the steps of: a. forming a first package consisting essentially of a monomeric binder mixture of from 99 1/2 percent to 99 7/8 percent by weight monomeric furfuryl alcohol and from 1/2 percent to 1/8 percent by weight of a silane coupling agent of the general formula: X-R''-Si-(OR'''')3 wherein R'' is a short chain alkylene containing between about 3 and 6 carbon atoms; R'''' is a radical selected from the group consisting of aryl, alkyl, substituted aryl, and heteroalkyl; and X is a reactive member selected from the group consisting of amino, mercapto, epoxy, and glycidoxy; b. forming a second package consisting essentially of a mixture of aggregate and acidic catalyst, said aggregate and said acidic catalyst being mixed in a proportion such that when from 2 percent to 20 percent by weight monomeric binder is mixed with from 98 percent to 80 percent by weight of the aggregate-acidic catalyst mixture, the acidic catalyst is present in an amount of from 5 percent to 50 percent by weight of the monomeric binder; and c. admixing said first package and said second package in an amount such that the first package contributes from 2 percent to 20 percent by weight and said second package contributes from 98 percent to 80 percent by weight.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1978-06-09 | 1978-12-09 | 1979-06-10 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1982-06-09 | 1982-12-09 | 1983-06-10 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1986-06-09 | 1986-12-09 | 1987-06-10 | $7700.00 | Window Closed / Lapsed |