US3896031A
Expired / Lapsed
US
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Preparation of colloidal solid suspensions in aqueous solutions
Assignee: MI Drilling Fluids Co
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Filing: 1973-04-20
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Granted: 1975-07-22
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Expires: 1993-04-20
Abstract
Abstract The present invention relates to the preparation of colloidal suspensions of solids in aqueous solutions, e.g., water-base drilling fluids, in the absence of oil. Colloidal solid materials such as asphaltic solids are rendered directly dispersible in the aqueous solution by novel dispersing agents provided by this invention. Improved aqueous drilling fluids containing colloidal suspensions of asphaltic solids and novel additives for forming such colloidal suspensions in aqueous drilling fluids are also provided by the present invention.
Inventors
- 👤 Leroy L Carney
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-07 11:25
CPC Classifications
C; C09; C09K; C09K8/00; C09K8/02; C09K8/04; C09K8/14; C09K8/18; C09K8/22; Y; Y10; Y10S; Y10S516/00; Y10S516/01; Y10S516/03; Y10S516/05
Claims Analysis
Total Claims: 13
Claim 1
Independent Claim
124 words
AN ADDITIVE FOR FORMING A COLLOIDAL SUSPENSION OF ASPHALTIC SOLIDS IN AN AQUEOUS SOLUTION IN THE ABSENCE OF OIL WHICH COMPRISES: COLLOIDAL ASPHALTIC SOLIDS, AND A DISPERSANT PRESENT IN SAID ADDITIVE IN AN AMOUNT IN THE RANGE OF FROM ABOUT 1% TO ABOUT 50% BY WEIGHT THEREOF CONSISTING OF A MIXTURE OF WASTE LIGNIN LIQUOR PRESENT IN AN AMOUNT IN THE RANGE OF FROM ABOUT 25% TO ABOUT 75% BY WEIGHT OF SAID MIXTURE AND AN AMIDE PRESENT IN AN AMOUNT IN THE RANGE OF FROM ABOUT 25% TO ABOUT 75% BY WEIGHT OF SAID MIXTURE, SAID AMIDE BEING FORMED BY REACTING A SATURATED OR UNSATURATED FATTY ACID HAVING IN THE RANGE OF FROM ABOUT 14 TO ABOUT 18 CARBON ATOMS WITH N-METHYL TAURINE.
Claim 2
Dependent Claim
124 words
AN ADDITIVE FOR FORMING A COLLOIDAL SUSPENSION OF ASPHALTIC SOLIDS IN AN AQUEOUS SOLUTION IN THE ABSENCE OF OIL WHICH COMPRISES: COLLOIDAL ASPHALTIC SOLIDS, AND A DISPERSANT PRESENT IN SAID ADDITIVE IN AN AMOUNT IN THE RANGE OF FROM ABOUT 1% TO ABOUT 50% BY WEIGHT THEREOF CONSISTING OF A MIXTURE OF WASTE LIGNIN LIQUOR PRESENT IN AN AMOUNT IN THE RANGE OF FROM ABOUT 25% TO ABOUT 75% BY WEIGHT OF SAID MIXTURE AND AN AMIDE PRESENT IN AN AMOUNT IN THE RANGE OF FROM ABOUT 25% TO ABOUT 75% BY WEIGHT OF SAID MIXTURE, SAID AMIDE BEING FORMED BY REACTING A SATURATED OR UNSATURATED FATTY ACID HAVING IN THE RANGE OF FROM ABOUT 14 TO ABOUT 18 CARBON ATOMS WITH N-METHYL TAURINE.
Claim 3
Dependent Claim
11 words
The additive of claim 1 wherein the amide is oleyl amide.
Claim 4
Dependent Claim
26 words
The additive of claim 2 wherein the dispersant is further characterized to be a substantially dry solid prepared by drying the oleyl amide-waste lignin liquor mixture.
Claim 5
Dependent Claim
23 words
The additive of claim 3 wherein the dry dispersant is present in said additive in an amount of about 4% by weight thereof.
Claim 6
Dependent Claim
50 words
The additive of claim 4 wherein the oleyl amide is present in said dispersant in an amount of about 50% by weight thereof and the waste lignin liquor is waste sulfite liquor present in the dispersant prior to drying in an amount of about 50% by weight of the dispersant.
Claim 7
Dependent Claim
81 words
An additive for forming a colloidal suspension of asphaltic solids in an aqueous solution in the absence of oil which comprises: colloidal asphaltic solids; and a dispersant present in said additive in an amount in the range of from about 1% to about 50% by weight of said additive, said dispersant being prepared by mixing in about equal amounts by weight the oleyl amide formed by reacting oleic acid with N-methyl taurine and waste sulfite liquor, and then drying said mixture.
Claim 8
Dependent Claim
81 words
An additive for forming a colloidal suspension of asphaltic solids in an aqueous solution in the absence of oil which comprises: colloidal asphaltic solids; and a dispersant present in said additive in an amount in the range of from about 1% to about 50% by weight of said additive, said dispersant being prepared by mixing in about equal amounts by weight the oleyl amide formed by reacting oleic acid with N-methyl taurine and waste sulfite liquor, and then drying said mixture.
Claim 9
Dependent Claim
21 words
The additive of claim 6 wherein the dried dispersant is present therein in an amount of about 4% by weight thereof.
Claim 10
Dependent Claim
171 words
An improved aqueous drilling fluid containing a colloidal suspension of asphaltic solids in the absence of oil which comprises: water; an additive consisting of colloidal asphaltic solids and a dried mixture of an amide and waste lignin liquor, the amide being present in said mixture in an amount in the range of from about 25% to about 75% by weight and being formed by reacting a saturated or unsaturated fatty acid having in the range of from about 14 to about 18 carbon atoms with N-methyl taurine, the waste lignin liquor being present in said mixture in an amount in the range of from about 25% to about 75% by weight prior to drying, and the dried amide-waste lignin liquor mixture being present in said additive in an amount in the range of from about 1% to about 50% by weight of said additive; and said additive being present in said drilling fluid in an amount in the range of from about 0.5% to about 2% by weight of said water.
Claim 11
Dependent Claim
171 words
An improved aqueous drilling fluid containing a colloidal suspension of asphaltic solids in the absence of oil which comprises: water; an additive consisting of colloidal asphaltic solids and a dried mixture of an amide and waste lignin liquor, the amide being present in said mixture in an amount in the range of from about 25% to about 75% by weight and being formed by reacting a saturated or unsaturated fatty acid having in the range of from about 14 to about 18 carbon atoms with N-methyl taurine, the waste lignin liquor being present in said mixture in an amount in the range of from about 25% to about 75% by weight prior to drying, and the dried amide-waste lignin liquor mixture being present in said additive in an amount in the range of from about 1% to about 50% by weight of said additive; and said additive being present in said drilling fluid in an amount in the range of from about 0.5% to about 2% by weight of said water.
Claim 12
Dependent Claim
109 words
An improved aqueous drilling fluid containing a colloidal suspension of asphaltic solids in the absence of oil which comprises: water; an additive consisting of colloidal asphaltic solids and a Dispersant prepared by mixing oleyl amide with waste sulfite liquor in equal amounts by weight and then drying said mixture, the oleyl amide being formed by reacting oleic acid with N-methyl taurine, and the dispersant being present in said additive in an amount of about 4% by weight of said additive; and said additive being present in said drilling fluid in an amount in the range of from about 0.5% to about 2% by weight of the water present therein.
Claim 13
Dependent Claim
109 words
An improved aqueous drilling fluid containing a colloidal suspension of asphaltic solids in the absence of oil which comprises: water; an additive consisting of colloidal asphaltic solids and a Dispersant prepared by mixing oleyl amide with waste sulfite liquor in equal amounts by weight and then drying said mixture, the oleyl amide being formed by reacting oleic acid with N-methyl taurine, and the dispersant being present in said additive in an amount of about 4% by weight of said additive; and said additive being present in said drilling fluid in an amount in the range of from about 0.5% to about 2% by weight of the water present therein.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1978-07-21 | 1979-01-20 | 1979-07-22 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1982-07-21 | 1983-01-20 | 1983-07-22 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1986-07-21 | 1987-01-20 | 1987-07-22 | $7700.00 | Window Closed / Lapsed |