US3897365A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Hydrotreating catalyst and process therefor
Assignee: Wyeth Holdings LLC
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Filing: 1973-09-20
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Granted: 1975-07-29
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Expires: 1993-09-20
Abstract
Abstract There is disclosed a hydrotreating catalyst consisting of a support of molybdenum oxide-inorganic oxide gel and carried thereon nickel oxide and molybdenum oxide so as to provide an active catalyst having an increased content of molybdenum oxide over prior catalysts and the process of preparation thereof.
Inventors
- 👤 Irvin Ralph Feins
- 👤 Robert Murphy Yarrington
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-05 23:43
CPC Classifications
C; C10; C10G; C10G45/00; C10G45/02; C10G45/04; C10G45/06; C10G45/08; B; B01; B01J; B01J23/00; B01J23/70; B01J23/76; B01J23/84; B01J23/85; B01J23/88; B01J23/883; B01J27/00; B01J27/14; B01J27/186; B01J27/188; B01J27/19
Claims Analysis
Total Claims: 6
Claim 1
Independent Claim
212 words
A PROCESS FOR PREPARING A PRE-CRACKING HYDROTREATING CATALYST WHICH COMPRISES: (I) UNIFORMLY ADMIXING AN AQUEOUS AMMONIUM MOLYBDATE SOLUTION WITH AN INORGANIC OXIDE GEL CONSISTING OF AT LEAST 50 WEIGHT PERCENT ALUMINA, UP TO ABOUT 50 WEIGHT PERCENT SILICA, AND UP TO A TOTAL 10 WEIGHT PERCENT OF TITANIA, ZIRCONIA, OR VANADIA, SAID GEL PERCENTAGES TOTALING 100, THE AMOUNT OF AMMONIUM MOLYBDATE SOLUTION ADMIXED BEING SUFFICIENT TO POVIDE FROM ABOUT 5 TO 15 WEIGHT PERCENT MOLYBDENUM OXIDE BASED ON THE TOTAL CALCINED WEIGHT OF MOLYBDENUM OXIDE AND INORGANIC OXIDE GEL: (II) FORMING THE RESULTING MIXTURE INTO A CATALYST SUPPORT: (III) DRYING AND CALCINING THE FORMED SUPPORT, (IV) IMPREGNATING THE CALCINED SUPPORT WITH AN AQUEOUS ORTHOPHOSPHORIC ACID SOLUTION OF A NICKLE SOURCE AN A MOLYBDENUM SOURCE SO AS TO PROVIDE ON SAID SUPPORT FROM ABOUT 1.0 TO 3.5 WEIGHT PERCENT PHOSPHORUS, FROM ABOUT 1 TO 6 WEIGHT PERCENT NICKEL OXIDE, AND FROM ABOUT 1/ TO 2/ WEIGHT PERCENT MOLYBDENUM OXIDE, SAID PERCENTAGES BEING BASED ON THE TOTAL CALCINED WEIGHT OF SAID CATALYST AND THE TOTAL PERCENTAGE OF MOLYBDENUM OXIDE RESULTING FROM SAID SUPPORT AND IMPREGNATION BEING GREATER THAN 20 WEIGHT PERCENT AND LESS THAN ABOUT 35 WEIGHT PERCENT BASED ON THE WEIGHT OF THE CALCINED CATALYST, AND (V) DRYING AND CALCINING THE IMPREGNATED SUPPORT.
Claim 2
Dependent Claim
212 words
A PROCESS FOR PREPARING A PRE-CRACKING HYDROTREATING CATALYST WHICH COMPRISES: (I) UNIFORMLY ADMIXING AN AQUEOUS AMMONIUM MOLYBDATE SOLUTION WITH AN INORGANIC OXIDE GEL CONSISTING OF AT LEAST 50 WEIGHT PERCENT ALUMINA, UP TO ABOUT 50 WEIGHT PERCENT SILICA, AND UP TO A TOTAL 10 WEIGHT PERCENT OF TITANIA, ZIRCONIA, OR VANADIA, SAID GEL PERCENTAGES TOTALING 100, THE AMOUNT OF AMMONIUM MOLYBDATE SOLUTION ADMIXED BEING SUFFICIENT TO POVIDE FROM ABOUT 5 TO 15 WEIGHT PERCENT MOLYBDENUM OXIDE BASED ON THE TOTAL CALCINED WEIGHT OF MOLYBDENUM OXIDE AND INORGANIC OXIDE GEL: (II) FORMING THE RESULTING MIXTURE INTO A CATALYST SUPPORT: (III) DRYING AND CALCINING THE FORMED SUPPORT, (IV) IMPREGNATING THE CALCINED SUPPORT WITH AN AQUEOUS ORTHOPHOSPHORIC ACID SOLUTION OF A NICKLE SOURCE AN A MOLYBDENUM SOURCE SO AS TO PROVIDE ON SAID SUPPORT FROM ABOUT 1.0 TO 3.5 WEIGHT PERCENT PHOSPHORUS, FROM ABOUT 1 TO 6 WEIGHT PERCENT NICKEL OXIDE, AND FROM ABOUT 1/ TO 2/ WEIGHT PERCENT MOLYBDENUM OXIDE, SAID PERCENTAGES BEING BASED ON THE TOTAL CALCINED WEIGHT OF SAID CATALYST AND THE TOTAL PERCENTAGE OF MOLYBDENUM OXIDE RESULTING FROM SAID SUPPORT AND IMPREGNATION BEING GREATER THAN 20 WEIGHT PERCENT AND LESS THAN ABOUT 35 WEIGHT PERCENT BASED ON THE WEIGHT OF THE CALCINED CATALYST, AND (V) DRYING AND CALCINING THE IMPREGNATED SUPPORT.
Claim 3
Dependent Claim
25 words
The process of claim 1 wherein in step (I) the amount of ammonium molybdate solution employed is sufficient to provide 6-12 weight percent molybdenum oxide.
Claim 4
Dependent Claim
23 words
The process of claim 1 wherein in step (IV) the amount of nickel source is sufficient to provide 2-5 weight percent nickel oxide.
Claim 5
Dependent Claim
24 words
The process of claim 1 wherein in step (IV) the amount of orthophosphoric acid is sufficient to provide 1.5 to 3.0 weight percent phosphorus.
Claim 6
Dependent Claim
30 words
The process of claim 1 wherein the amounts of ammonium molybdate in step (I) and of molybdenum source in step (IV) are sufficient to provide 22-28 weight percent molybdenum oxide.
References Cited (Backward Citations)
US3114701A
Cited
US3287280A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1978-07-28 | 1979-01-27 | 1979-07-29 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1982-07-28 | 1983-01-27 | 1983-07-29 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1986-07-28 | 1987-01-27 | 1987-07-29 | $7700.00 | Window Closed / Lapsed |