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US3909287A Expired / Lapsed US ⏱️ 0.0 years remaining

Recovery of sugar from clarifier scum by countercurrent extraction

Assignee: Tate and Lyle PLC
•
Filing: 1974-05-07
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Granted: 1975-09-30
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Expires: 1994-05-07
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Abstract

Abstract In the phosphatation-flotation process of sugar refining, sugar is recovered from the clarifier scum by a multi-stage reflotation process involving at least two consecutive stages of countercurrent aqueous extraction, using an organic polymeric flocculating agent. The residual sugar loss can typically be reduced to about 0.05% or less of the total sugar input to the refinery, without the need for filtration or centrifugation of the scum.

Inventors

  • 👤 John Trethowan Rundell
  • 👤 Raymond George Bennett
  • 👤 Colin Vesty Rich
  • 👤 Paul Richmond Pottage

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-09 14:23
CPC Classifications
C; C13; C13B; C13B20/00; C13B20/12; C13B20/126

Claims Analysis

Total Claims: 12
Claim 1
Independent Claim 193 words
A CONTINUOUS PROCESS FOR RECOVERING SUGAR FROM THE CLARIFIER SCUM PRODCED BY PHOSPHATION-FLOATION IN SURGAR REFINING, WHICH PROCESS COMPRISES: SUBJECTING THE SCUM TO AT LEAST TWO CONSEUTIVE STAGES OF COUNTER-CURRENT AQUEOUS EXTRACTION, WHEREIN EACH EXTRACTION STAGE COMPRISES THE SUCCESSIVE STEPS OF A. DISPERSING THE SCUM IN DESWEETENING WATER, TO GIVE A HOMOGENEOUS MIXTURE, AND AERATING THE MIXTURE, B. DISTRIBUTING AN ANIONIC ORGANIC POLYMERIC FLOCCULANT UNIFORMLY THROUGHOUT THE AERATED MIXTURE, TO FLOCULATE THE SCUM THEREIN, C. PASSING THE MIXTURE, WITHOUT FURTHER AGITATION, TO A CLARIFIER, D. ALLOWING THE FLOCULATED SCUM TO SEGREATE FROM THE MIXTURE BY FLOATATION IN THE CLARIFIER, AND E. SEPARATELY REMOVING A CLARIFIED DILUTE SURGAR SOLUTION AND FLOCCULATED SCUM FROM THE CLARIFIER, PASSING THE FLOCULATED SCUM FROM THE STEP (E) OF EACH EXCEPT THE LAST EXTRACTION STAGE (A) OF THE NEXT EXRACTION STAGE, PASSING THE DILUTE SUGAR SOLUTION FROM STEP (E) OF EACH EXCEPT THE FIRST EXTRACTION STAGE (A) OF THE I MEDIATELAY PRECEDING EXTRACTION STAGE, FOR USE AS DESWEETENING WATER THEREIN, DISCHARGIING THE FLOCCULATED SCUM FROM STEP (E) OF THE LAST EXTRACTION STAGE, AS DESWEETENED SCUM, AND RECOVERING THE DILUTE SUGAR SOLUTION FROM STEP (E) OF THE FIRST EXRACTION STAGE.
Claim 2
Dependent Claim 193 words
A CONTINUOUS PROCESS FOR RECOVERING SUGAR FROM THE CLARIFIER SCUM PRODCED BY PHOSPHATION-FLOATION IN SURGAR REFINING, WHICH PROCESS COMPRISES: SUBJECTING THE SCUM TO AT LEAST TWO CONSEUTIVE STAGES OF COUNTER-CURRENT AQUEOUS EXTRACTION, WHEREIN EACH EXTRACTION STAGE COMPRISES THE SUCCESSIVE STEPS OF A. DISPERSING THE SCUM IN DESWEETENING WATER, TO GIVE A HOMOGENEOUS MIXTURE, AND AERATING THE MIXTURE, B. DISTRIBUTING AN ANIONIC ORGANIC POLYMERIC FLOCCULANT UNIFORMLY THROUGHOUT THE AERATED MIXTURE, TO FLOCULATE THE SCUM THEREIN, C. PASSING THE MIXTURE, WITHOUT FURTHER AGITATION, TO A CLARIFIER, D. ALLOWING THE FLOCULATED SCUM TO SEGREATE FROM THE MIXTURE BY FLOATATION IN THE CLARIFIER, AND E. SEPARATELY REMOVING A CLARIFIED DILUTE SURGAR SOLUTION AND FLOCCULATED SCUM FROM THE CLARIFIER, PASSING THE FLOCULATED SCUM FROM THE STEP (E) OF EACH EXCEPT THE LAST EXTRACTION STAGE (A) OF THE NEXT EXRACTION STAGE, PASSING THE DILUTE SUGAR SOLUTION FROM STEP (E) OF EACH EXCEPT THE FIRST EXTRACTION STAGE (A) OF THE I MEDIATELAY PRECEDING EXTRACTION STAGE, FOR USE AS DESWEETENING WATER THEREIN, DISCHARGIING THE FLOCCULATED SCUM FROM STEP (E) OF THE LAST EXTRACTION STAGE, AS DESWEETENED SCUM, AND RECOVERING THE DILUTE SUGAR SOLUTION FROM STEP (E) OF THE FIRST EXRACTION STAGE.
Claim 3
Dependent Claim 18 words
The process according to claim 1, wherein there are two of the said consecutive stages of counter-current extraction.
Claim 4
Dependent Claim 18 words
The process according to claim 1, wherein there are three Of the said consecutive stages of counter-current extraction.
Claim 5
Dependent Claim 55 words
The process according to claim 1, wherein, in step (a) of at least one of the said stages of counter-current extraction, the homogeneous dispersion of the scum and aeration of the mixture are simultaneously performed in a mixing tank provided with an external recirculation loop which includes a power-driven aerator, with injection of compressed air.
Claim 6
Dependent Claim 28 words
The process according to claim 4, wherein the mean residence time of the mixture in the mixing tank is in the range of from 2 to 10 minutes.
Claim 7
Dependent Claim 46 words
The process according to claim 4, wherein from 1% to 5% by volume of air is introduced into said mixture, on the basis of the mixture volume, and the recirculation rate in said loop is from 1 to 10 times the throughput in said mixing tank.
Claim 8
Dependent Claim 45 words
The process according to claim 1, wherein, in step (b) of each of the said stages of counter-current extraction, there are distributed from 0.1 to 5.0 parts by weight of said flocculant per million parts by weight of melt sugar solids throughput in the refinery.
Claim 9
Dependent Claim 45 words
The process according to claim 1, wherein, in step (b) of each of the said stages of counter-current extraction, there are distributed from 0.5 to 2.0 parts by weight of said flocculant per million parts by weight of melt sugar solids throughput in the refinery.
Claim 10
Dependent Claim 36 words
The process according to claim 1, wherein said flocculant is added to said aerated mixture in the form of an aqueous solution having a concentration in the range of from 0.25 to 5.0 grams per liter.
Claim 11
Dependent Claim 33 words
The process according to claim 1, wherein said flocculant is added to said aerated mixture in the form of an aqueous solution having a concentration of from 0.5 to 2.0 grams per liter.
Claim 12
Dependent Claim 46 words
The process according to claim 1, wherein said flocculant is an anionic polyacrylamide flocculating agent having a molecular weight of at least one million and containing up to 20 mole percent of anionic units selected from the group consisting of acrylic acid and sodium acrylate units.

References Cited (Backward Citations)

US2431634A Cited
US3166442A Cited
US3508965A Cited
US3698951A Cited
US3853616A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-09-29 1979-03-31 1979-09-30 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-09-29 1983-03-31 1983-09-30 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-09-29 1987-03-31 1987-09-30 $7700.00 Window Closed / Lapsed

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