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US3962403A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for separation of nahcolite from oil shale

Assignee: ExxonMobil Oil Corp
•
Filing: 1974-01-14
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Granted: 1976-06-08
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Expires: 1994-01-14
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Abstract

Abstract Nahcolite-bearing oil shale ore is heated to produce a distinct color change in the nahcolite, differentiating the nahcolite from the host oil shale for optical sorting, and such sorting is then accomplished by optical sorting means.

Inventors

  • 👤 Dagobert M. Wyslouzil

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-02 19:48
CPC Classifications
C; C01; C01D; C01D7/00; B; B07; B07C; B07C5/00; B07C5/34; B07C5/342; B07C5/3425; B07C5/3427; C01D7/12; C01D7/123

Claims Analysis

Total Claims: 13
Claim 1
Independent Claim 63 words
A process for separation of nahcolite from nahcolite-bearing oil shale ore, comprising the steps of: heating said nahcolite-bearing oil shale ore at a temperature of from about 100°C to about 1000°C for a time sufficient to convert at least some of the surface of said nahcolite to a lighter-colored product; and optically sorting to separate said lighter-colored product from the remaining oil shale.
Claim 2
Dependent Claim 63 words
A process for separation of nahcolite from nahcolite-bearing oil shale ore, comprising the steps of: heating said nahcolite-bearing oil shale ore at a temperature of from about 100°C to about 1000°C for a time sufficient to convert at least some of the surface of said nahcolite to a lighter-colored product; and optically sorting to separate said lighter-colored product from the remaining oil shale.
Claim 3
Dependent Claim 42 words
The process of claim 1 wherein said nahcolite-bearing oil shale ore is in the form of particles of from about 1/4 inch to about 3/4 inch in size and said heating is at a temperature of from about 150°C to about 200°C.
Claim 4
Dependent Claim 21 words
The process of claim 2 wherein said heating is for a time of from about 15 minutes to about 30 minutes.
Claim 5
Dependent Claim 16 words
The process of claim 1 wherein said optical sorting includes at least two stages of sorting.
Claim 6
Dependent Claim 12 words
The process of claim 1 wherein said optical sorting comprises area sorting.
Claim 7
Dependent Claim 17 words
The process of claim 1 wherein substantially all of said nahcolite is converted to said lighter-colored product.
Claim 8
Dependent Claim 83 words
A process for separation of nahcolite from nahcolite-bearing oil shale ore, comprising the steps of: heating said nahcolite-bearing oil shale ore at a temperature of from about 100°C to about 1000°C for a time sufficient to convert at least some of the surface of said nahcolite to sodium carbonate having a distinctly lighter color than the surface of the remaining oil shale; and optically sorting said heated nahcolite-bearing oil shale ore to separate a lighter-colored converted nahcolite fraction from the remaining oil shale.
Claim 9
Dependent Claim 83 words
A process for separation of nahcolite from nahcolite-bearing oil shale ore, comprising the steps of: heating said nahcolite-bearing oil shale ore at a temperature of from about 100°C to about 1000°C for a time sufficient to convert at least some of the surface of said nahcolite to sodium carbonate having a distinctly lighter color than the surface of the remaining oil shale; and optically sorting said heated nahcolite-bearing oil shale ore to separate a lighter-colored converted nahcolite fraction from the remaining oil shale.
Claim 10
Dependent Claim 42 words
The process of claim 7 wherein said nahcolite-bearing oil shale ore is in the form of particles of from about 1/4 inch to about 3/4 inch in size and said heating is at a temperature of from about 150°C to about 200°C.
Claim 11
Dependent Claim 35 words
The process of claim 8 wherein said heating is for a time of from about 15 minutes to about 30 minutes and substantially all of the surface of said nahcolite is converted to sodium carbonate.
Claim 12
Dependent Claim 16 words
The process of claim 7 wherein said optical sorting comprises a plurality of area sorting stages.
Claim 13
Dependent Claim 23 words
The process of claim 7 wherein said heating is for a time sufficient to convert substantially all of said nahcolite to sodium carbonate.

References Cited (Backward Citations)

US3133010A Cited
US3097744A Cited
US3479133A Cited
US3821353A Cited
US3819805A Cited
US3795310A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1979-06-08 1979-12-08 1980-06-08 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1983-06-08 1983-12-08 1984-06-08 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1987-06-08 1987-12-08 1988-06-08 $7700.00 Window Closed / Lapsed

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