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US4018791A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for the preparation of highly pure halogenated phthalocyanine pigment

Assignee: Hoechst AG
•
Filing: 1973-12-21
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Granted: 1977-04-19
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Expires: 1993-12-21
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Abstract

Abstract A process for the preparation of highly pure organic pigments which comprises converting organic dyestuffs having various degrees of purity into dyestuff salts capable of being isolated by means of suitable acids which dissolve the impurities contained in the dyestuff, separating them from the acid, recovering the dyestuffs in pure form from the dyestuff salts by the action of water and subjecting the isolated dyestuff in aqueous organic or aqueous-organic medium to a mechanical fine dispersion. By this process the dyestuff formed by the decomposition of the dyestuff sulfate is obtained in highly pure form and can extremely well be brought into a finely dispersed form so that it can be brought into pigment form already by short-time grinding. During the preparation and isolation of the dyestuff sulfate the sulfuric acid is obtained in such a high concentration that it can be regenerated in an economical manner and any ecological charge is avoided.

Inventors

  • 👤 Ernst Spietschka
  • 👤 Siegfried Schiessler
  • 👤 Wolfgang Tronich

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-07 17:34
CPC Classifications
C; C09; C09B; C09B67/00; C09B67/0001; C09B67/0017

Claims Analysis

Total Claims: 3
Claim 1
Independent Claim 68 words
A process for the preparation of a highly pure, acid-stable highly halogenated copper phthalocyanine pigment which consists of the steps of: converting the crude, highly halogenated copper phthalocyanine by means of concentrated sulfuric acid or oleum into the sulfate, isolating the sulfate, hydrolizing the sulfate, isolating the highly halogenated copperphthalocyanine and grinding it in a mixture of water and an alcohol having from 4 to 6 carbon atoms.
Claim 2
Dependent Claim 68 words
A process for the preparation of a highly pure, acid-stable highly halogenated copper phthalocyanine pigment which consists of the steps of: converting the crude, highly halogenated copper phthalocyanine by means of concentrated sulfuric acid or oleum into the sulfate, isolating the sulfate, hydrolizing the sulfate, isolating the highly halogenated copperphthalocyanine and grinding it in a mixture of water and an alcohol having from 4 to 6 carbon atoms.
Claim 3
Dependent Claim 24 words
A process as claimed in claim 1, wherein the grinding medium is an aqueous solution of an alcohol of 4 to 6 carbon atoms.

References Cited (Backward Citations)

US2225302A Cited
US2284685A Cited
US2549842A Cited
US2556727A Cited
US2900390A Cited
US3004986A Cited
US2982666A Cited
US3127412A Cited
US3137704A Cited
US3351481A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1980-04-18 1980-10-18 1981-04-19 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1984-04-18 1984-10-18 1985-04-19 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1988-04-18 1988-10-18 1989-04-19 $7700.00 Window Closed / Lapsed

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