US4072671A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Method for extracting phenols and oligosaccharides from vegetable tissues
Assignee: Eni SpA
•
Filing: 1976-02-20
•
Granted: 1978-02-07
•
Expires: 1996-02-20
Abstract
Abstract A method for stripping phenols and fermentable oligosaccharides from vegetable materials is disclosed, which consists in using a mixed solvent composed of a polar organic solvent formed by an alcohol, a ketone or an ester combined with an aqueous solution of an acidic electrolyte, the electrolyte is preferably an organic or inorganic acid or an acidic salt of these. The extraction temperature is from 4 DEG C to the temperature which is safe enough as not to experience protein denaturation. Certain critical ranges for the pH and solute to solvent ratios are also indicated.
Inventors
- 👤 Giancarlo Sodini
- 👤 Marco Canella
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-04 08:52
CPC Classifications
A; A23; A23J; A23J1/00; A23J1/14; A23J1/142; C; C13; C13K; C13K13/00
Claims Analysis
Total Claims: 12
Claim 1
Independent Claim
75 words
A method for the extraction of phenols and oligosaccharides from vegetable protein materials containing said phenols and oligosaccharides consisting in extracting said protein materials selected from the group consisting of flours, concentrates and isolates with an extracting amount of a polar solvent consisting of n-butyl alcohol in miscible combination with an aqueous solution of an electrolyte having an acidic nature selected from the group consisting of organic or inorganic acids and the acidic salts thereof.
Claim 2
Independent Claim
75 words
A method for the extraction of phenols and oligosaccharides from vegetable protein materials containing said phenols and oligosaccharides consisting in extracting said protein materials selected from the group consisting of flours, concentrates and isolates with an extracting amount of a polar solvent consisting of n-butyl alcohol in miscible combination with an aqueous solution of an electrolyte having an acidic nature selected from the group consisting of organic or inorganic acids and the acidic salts thereof.
Claim 3
Dependent Claim
34 words
A method for the extraction of phenols and oligosaccharides according to claim 1 characterized in that the extraction is carried out with a total protein material to solvent ratio ranging from 1:5 to 1:240.
Claim 4
Dependent Claim
28 words
A method for extracting phenols and oligosaccharides according to claim 1 characterized in that the pH of the aqueous solution of the electrolyte ranges from 2.0 to 6.0.
Claim 5
Dependent Claim
38 words
A method for extracting phenols and oligosaccharides according to claim 1 characterized in that the extraction is carried out at temperatures in the range from 4° C to the temperature at which the denaturation of the proteins begins.
Claim 6
Dependent Claim
22 words
A method for the extraction of phenols and oligosaccharides according to claim 1 characterized in that the electrolyte is an inorganic acid.
Claim 7
Dependent Claim
21 words
A method for the extraction of phenols and oligosaccharides according to claim 5 characterized in that the acid is hydrochloric acid.
Claim 8
Dependent Claim
36 words
A method for the extraction of phenols and oligosaccharides according to claim 1 characterized in that the extraction is carried out on a substrate selected from the group consisting of sunflowerseed flour, cottonseed flour and soybeanflour.
Claim 9
Independent Claim
51 words
A method for the extraction of phenols and oligosaccharides from a substrate selected from the group consisting of soy flour, sunflower seed flour and cottonseed flour which comprises contacting said substrate with an extracting amount of a miscible mixture of n-butanol, water and hydrochloric acid to extract said phenols and oligosaccharides.
Claim 10
Independent Claim
51 words
A method for the extraction of phenols and oligosaccharides from a substrate selected from the group consisting of soy flour, sunflower seed flour and cottonseed flour which comprises contacting said substrate with an extracting amount of a miscible mixture of n-butanol, water and hydrochloric acid to extract said phenols and oligosaccharides.
Claim 11
Dependent Claim
16 words
The method of claim 8 wherein the flour to solvent ratio is from 1:5 to 1:240.
Claim 12
Dependent Claim
18 words
The method of claim 8 wherein the pH of the water-hydrochloric acid mixture ranges from 2.0 to 6.0.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1981-02-06 | 1981-08-08 | 1982-02-07 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1985-02-06 | 1985-08-08 | 1986-02-07 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1989-02-06 | 1989-08-08 | 1990-02-07 | $7700.00 | Window Closed / Lapsed |