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US4269944A Expired / Lapsed US ⏱️ 0.0 years remaining

Composition for forming an intumescent material

Assignee: Dixon International Ltd
•
Filing: 1980-05-16
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Granted: 1981-05-26
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Expires: 2000-05-16
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Abstract

Abstract An improvement in intumescent compositions is provided comprising, in part, melamine formaldehyde resin, a cross-linking agent, and a hydrophilic setting agent. The composition chemically absorbs water to yield an intumescent material with reduced cracking properties which decomposes into gas and a solid foam residue upon heating.

Inventors

  • 👤 Cyril A. Redfarn

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-08 20:45
CPC Classifications
C; C09; C09K; C09K21/00; C09K21/14; C08; C08L; C08L61/00; C08L61/20; C08L61/26; C08L61/28; C09D; C09D5/00; C09D5/18; C09D5/185; Y; Y10; Y10S; Y10S521/00; Y10S521/907

Claims Analysis

Total Claims: 15
Claim 1
Independent Claim 64 words
An intumescent material upon heating decomposes into gas and a solid foam residue comprising: cured hydrophobic melamine formaldehyde resin in which the curing agent is selected from the group consisting of guanidine and dicyandiamide; a hydrated inorganic setting agent, said setting agent having chemically absorbed water to make the intumescent material coherent; an ammonium phosphate; polyvinyl acetate; a polyhydroxy compound; and reinforcing fibrous material.
Claim 2
Dependent Claim 64 words
An intumescent material upon heating decomposes into gas and a solid foam residue comprising: cured hydrophobic melamine formaldehyde resin in which the curing agent is selected from the group consisting of guanidine and dicyandiamide; a hydrated inorganic setting agent, said setting agent having chemically absorbed water to make the intumescent material coherent; an ammonium phosphate; polyvinyl acetate; a polyhydroxy compound; and reinforcing fibrous material.
Claim 3
Dependent Claim 47 words
An intumescent material which upon heating decomposes into gas and an expanded solid foam residue comprising: cured hydrophobic melamine formaldehyde resin in which the curing agent is selected from the group consisting of dicyandiamide and guanadine calcium sulphate dihydrate; monoammonium diphosphate; polyvinyl acetate; pentaerythritol; and wood flour.
Claim 4
Dependent Claim 47 words
An intumescent material which upon heating decomposes into gas and an expanded solid foam residue comprising: cured hydrophobic melamine formaldehyde resin in which the curing agent is selected from the group consisting of dicyandiamide and guanadine calcium sulphate dihydrate; monoammonium diphosphate; polyvinyl acetate; pentaerythritol; and wood flour.
Claim 5
Dependent Claim 28 words
The composition as recited in claim 1 wherein said inorganic setting agent is selected from the group consisting of calcium sulphate dihydrate, Portland cement, and high alumina cement.
Claim 6
Dependent Claim 24 words
The intumescent material as recited in claim 1 wherein said ammonium phosphate is selected from the group consisting of monoammonium diphosphate and diammonium phosphate.
Claim 7
Dependent Claim 15 words
The intumescent material as recited in claim 1 wherein said polyhydroxy compound is a sugar.
Claim 8
Dependent Claim 14 words
The intumescent material as recited in claim 1 wherein said polyhydroxy compound is pentaerythritol.
Claim 9
Dependent Claim 30 words
The intumescent material as recited in claim 1, wherein said reinforcing fibrous material is selected from the group consisting of wood flour, hammer milled glass fibers and disintegrated nylon fibers.
Claim 10
Dependent Claim 140 words
The intumescent material as recited in claim 1 comprising: said cured hydrophobic melamine formaldehyde resin, the cured resin being formed from prepolymer residues of 90 to 110 parts by weight of water-dispersible melamine formaldehyde prepolymer and 45 to 55 parts by weight of said curing agent; 90 to 110 parts by weight of said inorganic setting agent; 90 to 110 parts by weight of said ammonium phosphate; 3.6 to 4.4 parts by weight of said polyvinyl acetate; 3.6 to 4.4 parts by weight of said polyvinyl acetate; 18 to 22 parts by weight of said polyhydroxy compound; and 4.5 to 5.5 parts by weight of said reinforcing fibrous material, these parts by weight being based upon an amount of the intumescent material obtained from a total of 150 parts by weight of the melamine formaldehyde prepolymer and the curing agent.
Claim 11
Independent Claim 87 words
A method for making an intumescent material which upon heating decomposes into gas and an expanded solid foam residue, said method comprising the steps of combining as a mixture water-dispersible melamine formaldehyde prepolymer resin an inorganic hydrophilic setting agent selected from the group consisting of dicyandiamide and guanidine, an ammonium phosphate, polyvinyl acetate, a polyhydroxy compound, and reinforcing fibrous material; adding water to said mixture to form a paste or slurry; and holding said paste or slurry mixture at room temperature for a predetermined period of time.
Claim 12
Independent Claim 87 words
A method for making an intumescent material which upon heating decomposes into gas and an expanded solid foam residue, said method comprising the steps of combining as a mixture water-dispersible melamine formaldehyde prepolymer resin an inorganic hydrophilic setting agent selected from the group consisting of dicyandiamide and guanidine, an ammonium phosphate, polyvinyl acetate, a polyhydroxy compound, and reinforcing fibrous material; adding water to said mixture to form a paste or slurry; and holding said paste or slurry mixture at room temperature for a predetermined period of time.
Claim 13
Dependent Claim 35 words
A method according to claim 9, wherein the slurry is poured into a container before being held at room temperature for said predetermined period of time, whereby the intumescent material is formed within the container.
Claim 14
Dependent Claim 26 words
A method according to claim 9, wherein the paste is applied to a surface before being held at room temperature for said predetermined period of time.
Claim 15
Dependent Claim 30 words
A method of curing the melamine formaldehyde prepolymer of claim 9, which consists of holding the mixture between room temperature and 40° C. cross-linked by the dicyandiamide or the guanadine.

References Cited (Backward Citations)

US2566964A Cited
US2684953A Cited
US3037951A Cited
US4013599A Cited
US4043950A Cited
US3979341A Cited
US4210725A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1984-05-25 1984-11-24 1985-05-26 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1988-05-25 1988-11-24 1989-05-26 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1992-05-25 1992-11-24 1993-05-26 $7700.00 Window Closed / Lapsed

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