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US4301020A Expired / Lapsed US ⏱️ 0.0 years remaining

Process of slurrying and spray drying ceramic oxides with polyethyleneimine dispersants

Assignee: AT&T Inc
•
Filing: 1981-02-06
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Granted: 1981-11-17
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Expires: 2001-02-06
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Abstract

Abstract Many ceramics are produced with a processing sequence that includes spray drying or ball milling a slurry. To produce ceramics with the best properties and to facilitate ball milling or spray drying, a dispersant is normally added to the ceramic slurry. Ammonium citrate and polyethylenimine have been found to produce ceramic slurries with the desired characteristics. The dispersants appear especially well suited for use with ferrite slurries.

Inventors

  • 👤 David W. Johnson, Jr.
  • 👤 Eva M. Vogel

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-01 09:52
CPC Classifications
C; C04; C04B; C04B35/00; C04B35/01; C04B35/26; C04B35/2658; C04B35/2608; H; H01; H01F; H01F1/00; H01F1/01; H01F1/03; H01F1/12; H01F1/34; H01F1/36

Claims Analysis

Total Claims: 7
Claim 1
Independent Claim 70 words
A method of processing ceramics which comprises forming a slurry consisting of ceramic material and a dispersant; said ceramic material forming between 65 percent and 80 percent, by weight, of said material and being a mixture of metal oxides, and spray drying said slurry; characterized in that said dispersant consists essentially of at least one member selected from the group consisting of polyethylenimine and mixtures of polyethylenimine and ammonium citrate.
Claim 2
Independent Claim 70 words
A method of processing ceramics which comprises forming a slurry consisting of ceramic material and a dispersant; said ceramic material forming between 65 percent and 80 percent, by weight, of said material and being a mixture of metal oxides, and spray drying said slurry; characterized in that said dispersant consists essentially of at least one member selected from the group consisting of polyethylenimine and mixtures of polyethylenimine and ammonium citrate.
Claim 3
Dependent Claim 19 words
A method as recited in claim 1 in which said slurry has a solids content of approximately 75 percent.
Claim 4
Dependent Claim 22 words
A method as recited in claim 2 in which said ceramic material is a mixture of oxides suitable for forming a ferrite.
Claim 5
Dependent Claim 15 words
A method as recited in claim 3 in which said ferrite is a MnZn ferrite.
Claim 6
Dependent Claim 23 words
A method as recited in claim 3 in which said dispersant is polyethylenimine, said dispersant having a concentration greater than 0.25 weight percent.
Claim 7
Dependent Claim 18 words
A method as recited in claim 5 in which said concentration is between 0.75 and 1.00 weight percent.

References Cited (Backward Citations)

US3455718A Cited
US3597253A Cited
US3615811A Cited
GB1282307A Cited
US3663284A Cited
US4144083A Cited
US4267065A Cited
US4226843A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1984-11-16 1985-05-18 1985-11-17 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1988-11-16 1989-05-18 1989-11-17 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1992-11-16 1993-05-18 1993-11-17 $7700.00 Window Closed / Lapsed

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