US4353709A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Granulation process
Assignee: Mitsui Toatsu Chemicals Inc
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Filing: 1980-11-18
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Granted: 1982-10-12
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Expires: 2000-11-18
Abstract
Abstract There is disclosed a process of granulation comprising dropping as liquid droplets the melt of a substance solidifiable by cooling or drying through a zone having a sufficient vertical distance to allow solidification of the droplets, forming a fluidized bed of the solidified droplets on the bottom of the said zone, spraying the same or a different melt from the above mentioned substance as fine liquid grains along with a gas stream into the fluidized bed thereby forming a spouted bed of the solidified droplets in the fluidized bed, coating and enlarging the solidified droplets with the fine liquid grains inside the spouted bed, and discharging the obtained large sized granules from the fluidized bed. There is also disclosed an apparatus for practicing the process.
Inventors
- 👤 Susumu Nioh
- 👤 Hiroshi Hirayama
- 👤 Tetsuzo Honda
- 👤 Takashi Nagahama
- 👤 Masaki Naruo
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-31 10:40
CPC Classifications
C; C05; C05C; C05C9/00; C05C9/005; B; B01; B01J; B01J2/00; B01J2/16
Claims Analysis
Total Claims: 5
Claim 1
Independent Claim
200 words
A process for producing substantially spherical granules having a diameter larger than about 2 mm, which comprises the steps of: (a) dropping as liquid droplets the melt of a substance solidifiable by cooling or drying through a cooling zone having a sufficient height to solidify said liquid droplets, said melt containing up to 40% by weight of water; (b) countercurrently contacting said liquid droplets with a gas stream for cooling or drying, thereby forming solidified prills having diameter smaller than about 2 mm; (c) fluidizing said prills with a gas stream at the bottom of said cooling zone to form a fluidized bed; (d) spraying as fine liquid grains the melt of substance solidifiable by cooling or drying upwardly into said fluidized bed along with a gas stream to form a sprouted bed of said prills in said fluidized bed, while coating and enlarging said prills with said liquid grains, thereby forming granules having a diameter of up to 5 times greater than the diameter of said prills, the weight ratio of the melt dropped as liquid droplets to the melt sprayed as fine liquid grains ranging from 1:4 to 4:1, and (e) discharging said granules from said fluidized bed.
Claim 2
Dependent Claim
200 words
A process for producing substantially spherical granules having a diameter larger than about 2 mm, which comprises the steps of: (a) dropping as liquid droplets the melt of a substance solidifiable by cooling or drying through a cooling zone having a sufficient height to solidify said liquid droplets, said melt containing up to 40% by weight of water; (b) countercurrently contacting said liquid droplets with a gas stream for cooling or drying, thereby forming solidified prills having diameter smaller than about 2 mm; (c) fluidizing said prills with a gas stream at the bottom of said cooling zone to form a fluidized bed; (d) spraying as fine liquid grains the melt of substance solidifiable by cooling or drying upwardly into said fluidized bed along with a gas stream to form a sprouted bed of said prills in said fluidized bed, while coating and enlarging said prills with said liquid grains, thereby forming granules having a diameter of up to 5 times greater than the diameter of said prills, the weight ratio of the melt dropped as liquid droplets to the melt sprayed as fine liquid grains ranging from 1:4 to 4:1, and (e) discharging said granules from said fluidized bed.
Claim 3
Dependent Claim
36 words
A process as claimed in claim 1, wherein said melt dropped as liquid droplets and said melt sprayed as fine liquid grains are both urea and said granules are urea granules having diameters of 3-5 mm.
Claim 4
Dependent Claim
18 words
A process as claimed in claim 1, wherein said prills have a diameter between 1 and 2 mm.
Claim 5
Dependent Claim
21 words
A process as claimed in claim 1 wherein at least one of said melts is a melt of a fertilizer substance.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1985-10-11 | 1986-04-12 | 1986-10-12 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1989-10-11 | 1990-04-12 | 1990-10-12 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1993-10-11 | 1994-04-12 | 1994-10-12 | $7700.00 | Window Closed / Lapsed |