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US4380503A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for preparing oil-in-water emulsion

Assignee: TH GOLDSCHIDT AG
•
Filing: 1981-06-03
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Granted: 1983-04-19
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Expires: 2001-06-03
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Abstract

Abstract The invention relates to a process for the preparation of fine-particulate, stable emulsions of the oil-in-water type, in which the quantity of emulsifier required to achieve a stable emulsion is distributed in about 0.5 to 3 times the amount of water by weight, based upon the weight of the emulsifier, the emulsifying amount of the oleic phase is introduced into the foregoing dispersion, homogenization is performed under the effect of high shear stresses until a uniform gel is obtained, the gel so obtained is forced through a slotted disk comprising a plurality of holes less than 10 mm in diameter and into the residual amount of water, and the emulsion so generated is stirred while avoiding high shear stresses until the gel particles are completely dissolved. The process makes it possible to obtain fine-particulate, storage-stable and dilutable oil-in-water emulsions using only very small quantities of emulsifier.

Inventors

  • 👤 Gotz Koerner
  • 👤 Gerd Sanger
  • 👤 Hans-Ferdi Fink
  • 👤 Friedhelm Grassmann

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-30 22:49
CPC Classifications
B; B01; B01F; B01F23/00; B01F23/40; B01F23/43; B01F23/41; B01F23/4105; B01F25/00; B01F25/40; B01F25/45; B01F25/452; B01F25/4521; B01F33/00; B01F33/80; B01F33/834; C; C09; C09K; C09K23/00; C09K23/42; C10; C10L; C10L1/00; C10L1/32; C10L1/328; Y; Y10; Y10S; Y10S516/00; Y10S516/924; Y10S516/926

Claims Analysis

Total Claims: 4
Claim 1
Independent Claim 118 words
A process for the preparation of fine-particulate, stable emulsions of the oil-in-water type, which comprises (a) distributing the quantity of emulsifier required to achieve a stable emulsion in about 0.5 to 3 times the amount of water by weight, based upon the emulsifier weight, (b) introducing the oleic phase to be emulsified into the foregoing dispersion and homogenizing it under the effect of high shear stresses until a uniform gel is formed, (c) forcing the gel so obtained through a slotted disk, provided with a plurality of holes less than 10 mm in diameter, into the remaining amount of water, and stirring the emulsion so obtained while avoiding high shear stresses until the gel particles are completely dissolved.
Claim 2
Dependent Claim 118 words
A process for the preparation of fine-particulate, stable emulsions of the oil-in-water type, which comprises (a) distributing the quantity of emulsifier required to achieve a stable emulsion in about 0.5 to 3 times the amount of water by weight, based upon the emulsifier weight, (b) introducing the oleic phase to be emulsified into the foregoing dispersion and homogenizing it under the effect of high shear stresses until a uniform gel is formed, (c) forcing the gel so obtained through a slotted disk, provided with a plurality of holes less than 10 mm in diameter, into the remaining amount of water, and stirring the emulsion so obtained while avoiding high shear stresses until the gel particles are completely dissolved.
Claim 3
Dependent Claim 16 words
A process according to claim 1 including performing process steps (a) and (b) at elevated temperatures.
Claim 4
Dependent Claim 29 words
A process according to claim 1 or claim 2 including using a slotted disk in process step (c) of which the holes are 1 to 3 mm in diameter.

References Cited (Backward Citations)

US3361680A Cited
US3635834A Cited
US3709664A Cited
US4026817A Cited
US4000086A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1986-04-18 1986-10-18 1987-04-19 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1990-04-18 1990-10-18 1991-04-19 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1994-04-18 1994-10-18 1995-04-19 $7700.00 Window Closed / Lapsed

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