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US4400412A Expired / Lapsed US ⏱️ 0.0 years remaining

Thermochromic vanadium oxide coated glass

Assignee: PPG Industries Inc
•
Filing: 1982-02-01
•
Granted: 1983-08-23
•
Expires: 2002-02-01
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Abstract

Abstract A method is disclosed for producing a thermochromic window comprising a glass substrate and a coating containing VO 2 by chemical vapor deposition employing vanadium n-propylate in an oxidizing atmosphere.

Inventors

  • 👤 J. Kevin Scanlon
  • 👤 Charles B. Greenberg

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-30 13:25
CPC Classifications
C; C03; C03C; C03C17/00; C03C17/22; C03C17/23; C03C17/245; C03C2217/00; C03C2217/20; C03C2217/21; C03C2217/218; C03C2218/00; C03C2218/10; C03C2218/15; C03C2218/152

Claims Analysis

Total Claims: 6
Claim 1
Independent Claim 104 words
A method for making a thermochromic window comprising the steps of: a. heating a glass substrate to a sufficient temperature to convert vanadium n-propylate to vanadium oxide; b. vaporizing vanadium n-propylate; c. conveying the vaporized vanadium n-propylate to said substrate in an atmosphere sufficiently oxidizing to form a thermochromic film comprising VO 2 but insufficiently oxidizing to form a film which is not thermochromic as a result of the proportion of V 2 O 5 ; d. contacting a surface of said heated glass substrate with said vapor of vanadium n-propylate in said oxidizing atmosphere to deposit thereupon a film containing VO 2 .
Claim 2
Independent Claim 104 words
A method for making a thermochromic window comprising the steps of: a. heating a glass substrate to a sufficient temperature to convert vanadium n-propylate to vanadium oxide; b. vaporizing vanadium n-propylate; c. conveying the vaporized vanadium n-propylate to said substrate in an atmosphere sufficiently oxidizing to form a thermochromic film comprising VO 2 but insufficiently oxidizing to form a film which is not thermochromic as a result of the proportion of V 2 O 5 ; d. contacting a surface of said heated glass substrate with said vapor of vanadium n-propylate in said oxidizing atmosphere to deposit thereupon a film containing VO 2 .
Claim 3
Dependent Claim 31 words
The method according to claim 1, wherein the glass substrate is heated to a temperature of at least 400° C. and said atmosphere comprises a mixture of inert gas and oxygen.
Claim 4
Dependent Claim 30 words
The method according to claim 2, wherein the glass substrate is heated to a temperature of at least 500° C. and said atmosphere comprises a mixture of nitrogen and oxygen.
Claim 5
Dependent Claim 21 words
The method according to claim 3, wherein said atmosphere comprises 90 percent by volume nitrogen and 10 percent by volume oxygen.
Claim 6
Dependent Claim 23 words
The method according to claim 1, wherein the film containing VO 2 is deposited to a thickness of about 100 to 1,500 Angstroms.

References Cited (Backward Citations)

US3483110A Cited
US4307942A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1986-08-22 1987-02-21 1987-08-23 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1990-08-22 1991-02-21 1991-08-23 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1994-08-22 1995-02-21 1995-08-23 $7700.00 Window Closed / Lapsed

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