US4407747A
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US
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Continuous method for dissolving milk proteins containing casein and an apparatus for performing the method as well as water soluble milk protein products of a novel type
Assignee: STICHTING NEDERLANDS INSTITUUT VOOR VUIVELONDERZOEK (NIZO)
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Filing: 1980-10-28
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Granted: 1983-10-04
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Expires: 2000-10-28
Abstract
Abstract Continuous method for dissolving milk proteins containing water insoluble casein by passing said milk proteins together with one or more solubilizers and with water in a continuous stream through a closed reaction chamber by means of a positive displacement pump and converting the mixture within said reaction chamber under the influence of shearing forces into a solution having a dry solids content within the range of from 20 to 70% by weight. The solution can be removed from the reaction chamber as liquid jets which are dried while forming endless threads or films which can be cut or milled. Water soluble milk protein product having a particle density amounting to at least 90% of the specific density. Apparatus for performing said method containing a positive displacement pump and a closed reaction chamber connected to said pump by way of the discharge conduit of said pump, in which reaction chamber preferably a rotary means, such as a colloid mill or a serrated impeller, is provided.
Inventors
- 👤 Frank Lippe
- 👤 Henricus A. W. E. M. Ottenhof
- 👤 Rudolf De Boer
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-02 21:53
CPC Classifications
A; A23; A23J; A23J3/00; A23J3/04; A23J3/08; A23J3/10; Y; Y10; Y10S; Y10S530/00; Y10S530/827; Y10S530/832
Claims Analysis
Total Claims: 18
Claim 1
Independent Claim
103 words
A continuous method for dissolving milk proteins containing water insoluble casein comprising (a) simultaneously admixing said milk proteins with at least one solubilizer and with water, (b) passing the milk proteins, the solubilizer, and the water in a continuous stream through a closed reaction chamber by means of a positive displacement pump, and (c) converting the mixture within said reaction chamber under the influence of shearing forces at a temperature of at least 60° C. and at a final pH value of at least 6.5 into a solution having a dry solids content within the range of from 27 to 60% by weight.
Claim 2
Dependent Claim
103 words
A continuous method for dissolving milk proteins containing water insoluble casein comprising (a) simultaneously admixing said milk proteins with at least one solubilizer and with water, (b) passing the milk proteins, the solubilizer, and the water in a continuous stream through a closed reaction chamber by means of a positive displacement pump, and (c) converting the mixture within said reaction chamber under the influence of shearing forces at a temperature of at least 60° C. and at a final pH value of at least 6.5 into a solution having a dry solids content within the range of from 27 to 60% by weight.
Claim 3
Dependent Claim
17 words
The method of claim 1, wherein said pump is a volume pump having an added feeding screw.
Claim 4
Independent Claim
25 words
The method of claims 1 and 2, wherein the shearing forces within the reaction chamber are generated solely by friction with respect to stationary surfaces.
Claim 5
Independent Claim
36 words
The method of claims 1 or 2, wherein the shearing forces are intensified by the use of rotary means selected from the group consisting of a colloid mill and a serrated impeller, within said reaction chamber.
Claim 6
Dependent Claim
63 words
The method of claim 1 wherein said solubilizer has an alkaline reaction such that before arriving in the reaction chamber the milk proteins are admixed with an alkaline solubilizer until a pH-value of from 5.0 to 5.3 is reached whereupon within said reaction chamber such an amount of alkaline solubilizer is added that the pH-value of the mixture will be at least 6.5.
Claim 7
Dependent Claim
46 words
The method of claim 1, wherein the milk proteins before arriving in the reaction chamber are admixed with ammonium hydroxide up to a pH-value of from 5.0 to 5.3 whereupon within the reaction chamber calcium hydroxide is added up to a pH-value of at least 6.5.
Claim 8
Dependent Claim
19 words
The method of claim 5, wherein the mixture is kept at a temperature of from 70° to 80° C.
Claim 9
Independent Claim
22 words
The method of claims 1 or 2 wherein the temperature within the reaction chamber is adjusted by the direct injection of steam.
Claim 10
Dependent Claim
26 words
The method of claim 1 wherein the residence time, the temperature and the pressure within the reaction chamber are kept constant during the continuous dissolving operation.
Claim 11
Dependent Claim
40 words
The method of claim 1 wherein the mixture is kept at a temperature above 120° C. within the reaction chamber for a period of time such that micro-organisms, viruses and other undesirable substances of biological origin are killed or inactivated.
Claim 12
Dependent Claim
50 words
The method of claim 1 wherein the residence time and the temperature within the reaction chamber are adjusted in such a manner that the thermal deterioration of the proteins will be no more serious than that corresponding to a residence time of 120 seconds at a temperature of 80° C.
Claim 13
Independent Claim
24 words
The method of claims 1, or 2, wherein the solutions obtained are dried to a dry solids content of at least 90% by weight.
Claim 14
Independent Claim
52 words
The method of claims 1, or 2, wherein the solution obtained in the reaction chamber is discharged from said reaction chamber by means of at least one narrow discharge opening, whereupon the liquid jets forced through said opening are dried while forming endless threads or films which are then cut or milled.
Claim 15
Dependent Claim
40 words
The method of claim 5, wherein the alkaline solubilizer is added within said reaction chamber while the shearing forces are intensified by the use of rotary means selected from the group consisting of a colloid mill and a serrated impeller.
Claim 16
Dependent Claim
39 words
The method of claim 6, wherein calcium hydroxide is added within the reaction chamber, while the shearing forces are intensified by the use of rotary means selected from the group consisting of a colloid mill and a serrated impeller.
Claim 17
Dependent Claim
53 words
The water-soluble milk protein product which is prepared according to the method of claim 12 and then forced through narrow openings and dried to endless threads or films which can be processed into a powder having a particle density amounting to at least 90% of the specific density of the milk protein itself.
Claim 18
Dependent Claim
32 words
The water-soluble milk protein product prepared according to the method of claim 13 and having a particle density amounting to at least 90% of the specific density of the milk protein itself.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
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| 3.5 Years (Year 4) | 1986-10-03 | 1987-04-04 | 1987-10-04 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1990-10-03 | 1991-04-04 | 1991-10-04 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1994-10-03 | 1995-04-04 | 1995-10-04 | $7700.00 | Window Closed / Lapsed |