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US4441968A
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Method of manufacture of an electric humidity detecting sensing element
Assignee: Charles University
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Filing: 1981-12-01
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Granted: 1984-04-10
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Expires: 2001-12-01
Abstract
Abstract Electric humidity detecting sensing element on the basis of a layer of porous aluminum oxide, treated by sealing in boiling water, passivation and tempering at 70° to 110° C., achieving thereby a substantial reduction of subsequent variations of calibrating curves. The time of tempering may range from 2 to 24 hours. A preferred average time of tempering is 8 hours, with a practical upper limit of 12 hours.
Inventors
- 👤 Ivan Emmer
- 👤 Zdenek Hajek
- 👤 Petr Repa
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-28 11:53
CPC Classifications
G; G01; G01N; G01N27/00; G01N27/02; G01N27/04; G01N27/12; G01N27/121
Claims Analysis
Total Claims: 6
Claim 1
Independent Claim
144 words
In a method of manufacturing an electric humidity detecting sensing element by anodically oxidizing a polished aluminum surface by alternating current of a density of about 12 mA/sq.cm using an electrolyte of 50% sulphuric acid at a temperature of 33° C. for 25 minutes to provide a porous layer of aluminum oxide and sealing the porous layer in boiling water, the improvement in combination therewith which comprises prior to preparing an upper electrode, tempering said layer for a time ranging from 2 to 24 hours at a temperature of from 70° to 110° C. in an atmosphere which is chemically inert relative to said aluminum oxide layer, said atmosphere containing water vapor in an amount of from zero to that corresponding to the dew point of 65° C., thereby stabilizing surface properties of said layer with respect to a reversible absorption of water vapor.
Claim 2
Dependent Claim
144 words
In a method of manufacturing an electric humidity detecting sensing element by anodically oxidizing a polished aluminum surface by alternating current of a density of about 12 mA/sq.cm using an electrolyte of 50% sulphuric acid at a temperature of 33° C. for 25 minutes to provide a porous layer of aluminum oxide and sealing the porous layer in boiling water, the improvement in combination therewith which comprises prior to preparing an upper electrode, tempering said layer for a time ranging from 2 to 24 hours at a temperature of from 70° to 110° C. in an atmosphere which is chemically inert relative to said aluminum oxide layer, said atmosphere containing water vapor in an amount of from zero to that corresponding to the dew point of 65° C., thereby stabilizing surface properties of said layer with respect to a reversible absorption of water vapor.
Claim 3
Dependent Claim
14 words
A method as claimed in claim 1, wherein the said atmosphere is clean air.
Claim 4
Dependent Claim
14 words
A method as claimed in claim 1, wherein the tempering takes place in vacuo.
Claim 5
Dependent Claim
57 words
A method as claimed in claim 1, wherein the porous aluminum oxide layer, prior to tempering, is passivated by submerging it in an aqueous solution of NaH 2 PO 4 .2H 2 O having a concentration of from 0.01 to 2 mol, for from 10 to 60 minutes at a temperature of from 35° to 100° C.
Claim 6
Dependent Claim
53 words
A method as claimed in claim 1, wherein the porous aluminum oxide layer, prior to tempering, is passivated by submerging it in an aqueous solution of pure silicic acid having a concentration of from 0.01 to 2 mol, for from 10 to 60 minutes at a temperature of from 35° to 100° C.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1987-04-10 | 1987-10-10 | 1988-04-10 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1991-04-10 | 1991-10-10 | 1992-04-10 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1995-04-10 | 1995-10-10 | 1996-04-10 | $7700.00 | Window Closed / Lapsed |