US4481077A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Process for preparing microfibrillated cellulose
Assignee: Rayonier Inc
•
Filing: 1983-03-28
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Granted: 1984-11-06
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Expires: 2003-03-28
Abstract
Abstract A process of preparing microfibrillated cellulose comprising adding to never-dried cellulosic pulp an additive compound capable of substantially inhibiting hydrogen bonding of the fibrils in the cellulose and then drying the pulp and additive. Microfibrillation of a suspension of the cellulosic pulp is carried out at considerably increased efficiency if the additive compound is present prior to drying the pulp. The resulting MFC product can be dried and redispersed without substantial loss of viscosity.
Inventors
- 👤 Franklin W. Herrick
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-29 05:03
CPC Classifications
D; D21; D21C; D21C9/00; D21C9/001; C; C08; C08L; C08L1/00; C08L1/02
Claims Analysis
Total Claims: 9
Claim 1
Independent Claim
122 words
A process of preparing microfibrillated cellulose comprising adding to never-dried cellulosic pulp an additive compound capable of substantially inhibiting hydrogen bonding of the fibrils in the cellulose, said additive compound being non-reactive with said cellulose and not having substantial volatility during drying, drying said cellulosic pulp and additive compound to a moisture content no greater than 15%, adding a liquid to said dried cellulosic pulp and additive compound to form a liquid suspension thereof and passing said liquid suspension through a high pressure homogenizer having a small diameter orifice in which said suspension is subjected to a pressure drop of at least 3000 psi followed by a high velocity decelerating impact against a solid surface to form a suspension of microfibrillated cellulose.
Claim 2
Dependent Claim
122 words
A process of preparing microfibrillated cellulose comprising adding to never-dried cellulosic pulp an additive compound capable of substantially inhibiting hydrogen bonding of the fibrils in the cellulose, said additive compound being non-reactive with said cellulose and not having substantial volatility during drying, drying said cellulosic pulp and additive compound to a moisture content no greater than 15%, adding a liquid to said dried cellulosic pulp and additive compound to form a liquid suspension thereof and passing said liquid suspension through a high pressure homogenizer having a small diameter orifice in which said suspension is subjected to a pressure drop of at least 3000 psi followed by a high velocity decelerating impact against a solid surface to form a suspension of microfibrillated cellulose.
Claim 3
Dependent Claim
40 words
The process of claim 1 in which the liquid suspension is repeatedly passed through the homogenizer until the suspension becomes a substantially stable suspension, said process requiring fewer passes through the homogenizer than would be necessary without said additive compound.
Claim 4
Dependent Claim
24 words
The process of claim 1 in which the additive compound is present at levels of at least one half the weight of the cellulose.
Claim 5
Dependent Claim
28 words
The process of claim 1 in which said additive compound is selected from the group consisting of a polyhydroxy compound, an alkali metal salt and an aprotic solvent.
Claim 6
Dependent Claim
24 words
The process of claim 4 in which said additive compound is selected from the group consisting of a carbohydrate, a glycol and derivatives thereof.
Claim 7
Dependent Claim
13 words
The process of claim 5 in which said additive compound is a carbohydrate.
Claim 8
Dependent Claim
26 words
The process of claim 6 in which the carbohydrate is sucrose in an amount of about one half to two times the weight of the cellulose.
Claim 9
Dependent Claim
13 words
The process of claim 1 in which the suspension of MFC is dried.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1987-11-06 | 1988-05-07 | 1988-11-06 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1991-11-06 | 1992-05-07 | 1992-11-06 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1995-11-06 | 1996-05-07 | 1996-11-06 | $7700.00 | Window Closed / Lapsed |