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US4610944A Expired / Lapsed US ⏱️ 0.0 years remaining

Production of toner

Assignee: Canon Inc
•
Filing: 1984-01-03
•
Granted: 1986-09-09
•
Expires: 2004-01-03
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Abstract

Abstract A process for producing a toner, comprising the steps of suspending a molten mixture of starting materials of a binder containing a compound having a hydrocarbon chain and a colorant in an aqueous dispersing medium in the presence of a hardly water-soluble fine powdery inorganic dispersant, cooling the dispersed particles, and recovering the cooled particles.

Inventors

  • 👤 Toru Matsumoto
  • 👤 Masuo Yamazaki
  • 👤 Katsutoshi Wakamiya

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-09 13:54
CPC Classifications
G; G03; G03G; G03G9/00; G03G9/08; G03G9/087; G03G9/08784; G03G9/08786; G03G9/0802; G03G9/0804; G03G9/097; G03G9/09708; G03G9/09725

Claims Analysis

Total Claims: 42
Claim 1
Independent Claim 94 words
A process for producing a toner and having a controlled and more uniform particle size distribution, comprising the steps of: melting a mixture of a long-chain binder compound having a melting point above room temperature, and a colorant; adding the molten mixture to a heated aqueous dispersing medium in the presence of a substantially water-insoluble fine powdery inorganic dispersant; stirring the added molten mixture and said aqueous dispersing medium to form suspended particles of said molten mixture dispersed in the aqueous dispersing medium; cooling the dispersed particles of said mixture; recovering the cooled particles.
Claim 2
Dependent Claim 94 words
A process for producing a toner and having a controlled and more uniform particle size distribution, comprising the steps of: melting a mixture of a long-chain binder compound having a melting point above room temperature, and a colorant; adding the molten mixture to a heated aqueous dispersing medium in the presence of a substantially water-insoluble fine powdery inorganic dispersant; stirring the added molten mixture and said aqueous dispersing medium to form suspended particles of said molten mixture dispersed in the aqueous dispersing medium; cooling the dispersed particles of said mixture; recovering the cooled particles.
Claim 3
Dependent Claim 45 words
A process according to claim 1, wherein the long-chain binder compound is selected from the group consisting of hydrocarbons, fatty acids, esters, metal soaps, metal salts or chlorides of fatty acids, fatty alcohols, polyhydric alcohols, fluorides, amides, and bisamides containing 12 to 50 carbon atoms,
Claim 4
Dependent Claim 56 words
A process according to claim 1, wherein the fine powdery inorganic dispersant is fine particles selected from the group consisting of BaSO 4 , CaSO 4 , BaCO 3 , CaCO 3 , MgCO 3 , Ca 3 (PO 4 ) 2 , talc, bentonite, silicic acid, diatomaceous earth, clay, aluminum oxide and SiO 2 .
Claim 5
Dependent Claim 19 words
A process according to claim 1, wherein the aqueous dispersing medium is heated to about 60° to 99° C.
Claim 6
Dependent Claim 106 words
A process for producing a toner, comprising the steps of: melting a mixture of a long-chain binder compound having a melting point above room temperature and a colorant, said mixture being chargeable either cationically or anionically; adding the molten mixture to a heated aqueous dispersing medium in the presence of a substantially water-insoluble fine powdery inorganic dispersant, said dispersant being chargeable to a polarity opposite to that of said mixture; stirring the added molten mixture and said aqueous dispersing medium to form suspended particles of said molten mixture dispersed in the aqueous dispersing medium; cooling the dispersed particles of said mixture; and recovering the cooled particles.
Claim 7
Dependent Claim 106 words
A process for producing a toner, comprising the steps of: melting a mixture of a long-chain binder compound having a melting point above room temperature and a colorant, said mixture being chargeable either cationically or anionically; adding the molten mixture to a heated aqueous dispersing medium in the presence of a substantially water-insoluble fine powdery inorganic dispersant, said dispersant being chargeable to a polarity opposite to that of said mixture; stirring the added molten mixture and said aqueous dispersing medium to form suspended particles of said molten mixture dispersed in the aqueous dispersing medium; cooling the dispersed particles of said mixture; and recovering the cooled particles.
Claim 8
Dependent Claim 45 words
A process according to claim 5, wherein the long-chain binder compound is selected from the group consisting of hydrocarbons, fatty acids, esters, metla soaps, metal salts or chlorides of fatty acids, fatty alcohols, polyhydric alcohols, fluorides, amides, and bisamides containing 12 to 50 carbon atoms.
Claim 9
Dependent Claim 56 words
A process according to claim 5, wherein the fine powdery inorganic dispersant is fine particles selected from the group consisting of BaSO 4 , CaSO 4 , BaCO 3 , CaCO 3 , MgCO 3 , Ca 3 (PO 4 ) 2 , talc, bentonite, silicic acid, diatomaceous earth, clay, aluminum oxide and SiO 2 .
Claim 10
Dependent Claim 19 words
A process according to claim 5, wherein the aqueous dispersing medium is heated to about 60° to 99° C.
Claim 11
Dependent Claim 30 words
A process according to claim 5 wherein the mixture contains a cationic compound or a substantially water-insoluble organic amine compound and is used in combination with an anionic inorganic dispersant.
Claim 12
Dependent Claim 14 words
A process according to claim 9, wherein the cationic compound is a cationic polymer.
Claim 13
Dependent Claim 21 words
A process according to claim 9, wherein the cationic compound is a cationic monomer graft polymerized onto the long-chain binder compound.
Claim 14
Dependent Claim 22 words
A process according to claim 9, wherein the anionic inorganic dispersant is selected from the group consisting of colloidal silica and bentonite.
Claim 15
Dependent Claim 23 words
A process according to claim 5, wherein the mixture contains an anionic compound and is used in combination with a cationic inorganic dispersant.
Claim 16
Dependent Claim 14 words
A process according to claim 13, wherein the anionic compound is an anionic polymer.
Claim 17
Dependent Claim 21 words
A process according to claim 13, wherein the anionic compound is an anionic monomer graft polymerized onto the long-chain binder compound.
Claim 18
Dependent Claim 15 words
A process according to claim 13, wherein the cationic inorganic dispersant comprises aluminum oxide particles.
Claim 19
Dependent Claim 92 words
A process for producing a toner, comprising the steps of: melting a mixture of a long-chain binder compound having a melting point above room temperature and a colorant; adding the molten mixture to a heated aqueous dispersing medium in the presence of a substantially water-insoluble fine powdery inorganic dispersant; stirring the added molten mixture and said aqueous dispersing medium to form suspended particles of said molten mixture dispersed in the aqueous dispersing medium; cooling the dispersed particles of said mixture; recovering the cooled particles; and coating the recovered particles with a resin.
Claim 20
Dependent Claim 92 words
A process for producing a toner, comprising the steps of: melting a mixture of a long-chain binder compound having a melting point above room temperature and a colorant; adding the molten mixture to a heated aqueous dispersing medium in the presence of a substantially water-insoluble fine powdery inorganic dispersant; stirring the added molten mixture and said aqueous dispersing medium to form suspended particles of said molten mixture dispersed in the aqueous dispersing medium; cooling the dispersed particles of said mixture; recovering the cooled particles; and coating the recovered particles with a resin.
Claim 21
Dependent Claim 45 words
A process according to claim 17, wherein the long-chain binder compound is selected from the group consisting of hydrocarbons, fatty acids, esters, metal soaps, metal salts or chlorides of fatty acids, fatty alcohols, polyhydric alcohols, fluorides, amides, and bisamides containing 12 to 50 carbon atoms.
Claim 22
Dependent Claim 56 words
A process according to claim 17, wherein the fine powdery inorganic dispersant is fine particles selected from the group consisting of BaSO 4 , CaSO 4 , BaCO 3 , CaCO 3 , MgCO 3 , Ca 3 (PO 4 ) 2 , talc, bentonite, silicic acid, diatomaceous earth, clay, aluminum oxide and SiO 2 .
Claim 23
Dependent Claim 19 words
A process according to claim 17, wherein the aqueous dispersing medium is heated to about 60° to 99° C.
Claim 24
Dependent Claim 21 words
A process according to claim 17, wherein the resin coating is applied on the recovered particles by the phase separation method.
Claim 25
Dependent Claim 28 words
A process according to claim 21, wherein the resin coating is carried out by dispersing the recovered particles in a resin solutin and spray drying the resultant dispersion.
Claim 26
Dependent Claim 113 words
A process for producing a toner, comprising the steps of: melting a mixture of a long-chain binder compound having a melting point above room temperature and a colorant, said mixture being chargeable either cationically or anionically; adding the molten mixture to a heated aqueous dispersing medium in the presence of a substantially water-insoluble fine powdery inorganic dispersant, said dispersant being chargeable to a polarity opposite to that of said mixture; stirring the added molten mixture and said aqueous dispersing medium to form suspended particles of said molten mixture dispersed in the aqueous dispersing medium; cooling the dispersed particles of said mixture; recovering the cooled particles; and coating the recovered particles with a resin.
Claim 27
Dependent Claim 113 words
A process for producing a toner, comprising the steps of: melting a mixture of a long-chain binder compound having a melting point above room temperature and a colorant, said mixture being chargeable either cationically or anionically; adding the molten mixture to a heated aqueous dispersing medium in the presence of a substantially water-insoluble fine powdery inorganic dispersant, said dispersant being chargeable to a polarity opposite to that of said mixture; stirring the added molten mixture and said aqueous dispersing medium to form suspended particles of said molten mixture dispersed in the aqueous dispersing medium; cooling the dispersed particles of said mixture; recovering the cooled particles; and coating the recovered particles with a resin.
Claim 28
Dependent Claim 45 words
A process according to claim 23, wherein the long-chain binder compound is selected from the group consisting of hydrocarbons, fatty acids, esters, metal soaps, metal salts or chlorides of fatty acids, fatty alcohols, polyhydric alcohols, fluorides, amides, and bisamides containing 12 to 50 carbon atoms.
Claim 29
Dependent Claim 56 words
A process according to claim 23, wherein the fine powdery inorganic dispersant is fine particles selected from the group consisting of BaSO 4 , CaSO 4 , BaCO 3 , CaCO 3 , MgCO 3 , Ca 3 (PO 4 ) 2 , talc, bentonite, silicic acid, diatomaceous earth, clay, aluminum oxide and SiO 2 .
Claim 30
Dependent Claim 19 words
A process according to claim 23, wherein the aqueous dispersing medium is heated to about 60° to 99° C.
Claim 31
Dependent Claim 30 words
A process according to claim 23 wherein the mixture contains a cationic compound or a substantially water-insoluble organic amine compound and is used in combination with an anionic inorganic dispersant.
Claim 32
Dependent Claim 14 words
A process according to claim 27, wherein the cationic compound is a cationic polymer.
Claim 33
Dependent Claim 21 words
A process according to claim 27, wherein the cationic compound is a cationic monomer graft polymerized onto the long-chain binder compound.
Claim 34
Dependent Claim 22 words
A process according to claim 27, wherein the anionic inorganic dispersant is selected from the group consisting of colloidal silica and bentonite.
Claim 35
Dependent Claim 23 words
A process according to claim 23, wherein the mixture contains an anionic compound and is used in combination with a cationic inorganic dispersant.
Claim 36
Dependent Claim 14 words
A process according to claim 31, wherein the anionic compound is an anionic polymer.
Claim 37
Dependent Claim 21 words
A process according to claim 31, wherein the anionic compound is an anionic monomer graft polymerized onto the long-chain binder compound.
Claim 38
Dependent Claim 15 words
A process according to claim 31, wherein the cationic inorganic dispersant comprises aluminum oxide particles.
Claim 39
Dependent Claim 9 words
Toner produced according to the process of claim 1.
Claim 40
Dependent Claim 9 words
Toner produced according to the process of claim 5.
Claim 41
Dependent Claim 9 words
Toner produced according to the process of claim 17.
Claim 42
Dependent Claim 9 words
Toner produced according to the process of claim 23.

References Cited (Backward Citations)

US2221776A Cited
US2618552A Cited
US2874063A Cited
GB1520047A Cited
US4329415A Cited
JPS56130761A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1989-09-08 1990-03-10 1990-09-09 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1993-09-08 1994-03-10 1994-09-09 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1997-09-08 1998-03-10 1998-09-09 $7700.00 Window Closed / Lapsed

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