← Back to Patent Explorer
US4639326A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for the preparation of a powder detergent composition of high bulk density

Assignee: Lever Brothers Co
•
Filing: 1985-07-03
•
Granted: 1987-01-27
•
Expires: 2005-07-03
📄 Original PDF 🌐 Google Patents 🔄 Sync Now

Abstract

Abstract The invention relates to a process for the preparation of a nonionic surfactant-containing powder detergent composition wherein a spray-dried sodium sulphate-free base powder containing a portion of the nonionic surfactant is obtained and the remaining portion of the nonionic surfactant is in part sprayed onto the base powder and in part added subsequently in a form obtained by granulation with a carrier containing a mixture of zeolite and alkali metal perborate monhydrate and wherein the other detergent components are added subsequently to the base powder. A detergent composition prepared in this manner has a high bulk density despite its high AD content.

Inventors

  • 👤 Klaus Czempik
  • 👤 Gerd Stremmel

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-08 19:37
CPC Classifications
C; C11; C11D; C11D17/00; C11D17/06; C11D17/065; C11D1/00; C11D1/66; C11D1/72; C11D11/00; C11D11/02; C11D3/00; C11D3/02; C11D3/12; C11D3/124; C11D3/1246; C11D3/128; C11D3/39; C11D3/3942

Claims Analysis

Total Claims: 6
Claim 1
Independent Claim 210 words
A process for the preparation of a nonionic surfactant-containing powder detergent composition having a total surfactant content from 5 to 15% and of greater than 0.60 kg/l bulk density, comprising the steps of: (a) spray-drying a base powder comprising from about 4% to about 6% by weight of said detergent composition of a nonionic surfactant; (b) spraying onto said base powder a further amount of nonionic surfactant in an amount from about 4% up to not more than half of the total nonionic content by weight of said detergent composition; (c) subsequent to step (b) adding a final amount of nonionic surfactant obtained by granulation with a carrier, the amounts of said surfactant and carrier being from about 2.85 to 4.0% and being about 22%, respectively, by weight of said detergent composition; and (d) subsequently adding adjunct detergent components to the base powder, said base powder being essentially free of sodium sulfate and the carrier for the nonionic surfactant comprising a mixture of zeolite and alkali metal perborate monohydrate in the amount of about 3 to 4% and about 8.5%, respectively, by weight of said detergent composition; said base powder and nonionic containing granulated carrier being present from about 59% and about 26%, respectively, by weight of said detergent composition.
Claim 2
Dependent Claim 210 words
A process for the preparation of a nonionic surfactant-containing powder detergent composition having a total surfactant content from 5 to 15% and of greater than 0.60 kg/l bulk density, comprising the steps of: (a) spray-drying a base powder comprising from about 4% to about 6% by weight of said detergent composition of a nonionic surfactant; (b) spraying onto said base powder a further amount of nonionic surfactant in an amount from about 4% up to not more than half of the total nonionic content by weight of said detergent composition; (c) subsequent to step (b) adding a final amount of nonionic surfactant obtained by granulation with a carrier, the amounts of said surfactant and carrier being from about 2.85 to 4.0% and being about 22%, respectively, by weight of said detergent composition; and (d) subsequently adding adjunct detergent components to the base powder, said base powder being essentially free of sodium sulfate and the carrier for the nonionic surfactant comprising a mixture of zeolite and alkali metal perborate monohydrate in the amount of about 3 to 4% and about 8.5%, respectively, by weight of said detergent composition; said base powder and nonionic containing granulated carrier being present from about 59% and about 26%, respectively, by weight of said detergent composition.
Claim 3
Dependent Claim 35 words
A process according to claim 1, wherein the detergent composition comprises a mixture of nonionic and anionic surfactants in an amount from 5 to 15% and 3 to 12%, respectively, by weight of said composition.
Claim 4
Dependent Claim 14 words
A process according to claim 1, wherein the base powder contains about 5% zeolites.
Claim 5
Dependent Claim 43 words
A process according to claim 1, wherein the base powder contains less than one-half of the total quantity of nonionic surfactant and not more than one-half of the remaining portion of the total quantity of nonionic surfactant is sprayed onto the base powder.
Claim 6
Dependent Claim 30 words
A process according to claim 1, wherein about 1% of an anionic surfactant is sprayed onto the base powder together with about 4% of the nonionic surfactant in step (b).

References Cited (Backward Citations)

US3538004A Cited
US3700600A Cited
US3769222A Cited
US3886098A Cited
US3920586A Cited
US4136051A Cited
US4406808A Cited
US4288342A Cited
US4330424A Cited
US4311607A Cited
US4368134A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1990-01-26 1990-07-28 1991-01-27 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1994-01-26 1994-07-28 1995-01-27 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1998-01-26 1998-07-28 1999-01-27 $7700.00 Window Closed / Lapsed

Assigned Categories & Tags

No categories assigned to this patent yet.

Assign Category Tag