US4639326A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Process for the preparation of a powder detergent composition of high bulk density
Assignee: Lever Brothers Co
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Filing: 1985-07-03
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Granted: 1987-01-27
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Expires: 2005-07-03
Abstract
Abstract The invention relates to a process for the preparation of a nonionic surfactant-containing powder detergent composition wherein a spray-dried sodium sulphate-free base powder containing a portion of the nonionic surfactant is obtained and the remaining portion of the nonionic surfactant is in part sprayed onto the base powder and in part added subsequently in a form obtained by granulation with a carrier containing a mixture of zeolite and alkali metal perborate monhydrate and wherein the other detergent components are added subsequently to the base powder. A detergent composition prepared in this manner has a high bulk density despite its high AD content.
Inventors
- 👤 Klaus Czempik
- 👤 Gerd Stremmel
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-08 19:37
CPC Classifications
C; C11; C11D; C11D17/00; C11D17/06; C11D17/065; C11D1/00; C11D1/66; C11D1/72; C11D11/00; C11D11/02; C11D3/00; C11D3/02; C11D3/12; C11D3/124; C11D3/1246; C11D3/128; C11D3/39; C11D3/3942
Claims Analysis
Total Claims: 6
Claim 1
Independent Claim
210 words
A process for the preparation of a nonionic surfactant-containing powder detergent composition having a total surfactant content from 5 to 15% and of greater than 0.60 kg/l bulk density, comprising the steps of: (a) spray-drying a base powder comprising from about 4% to about 6% by weight of said detergent composition of a nonionic surfactant; (b) spraying onto said base powder a further amount of nonionic surfactant in an amount from about 4% up to not more than half of the total nonionic content by weight of said detergent composition; (c) subsequent to step (b) adding a final amount of nonionic surfactant obtained by granulation with a carrier, the amounts of said surfactant and carrier being from about 2.85 to 4.0% and being about 22%, respectively, by weight of said detergent composition; and (d) subsequently adding adjunct detergent components to the base powder, said base powder being essentially free of sodium sulfate and the carrier for the nonionic surfactant comprising a mixture of zeolite and alkali metal perborate monohydrate in the amount of about 3 to 4% and about 8.5%, respectively, by weight of said detergent composition; said base powder and nonionic containing granulated carrier being present from about 59% and about 26%, respectively, by weight of said detergent composition.
Claim 2
Dependent Claim
210 words
A process for the preparation of a nonionic surfactant-containing powder detergent composition having a total surfactant content from 5 to 15% and of greater than 0.60 kg/l bulk density, comprising the steps of: (a) spray-drying a base powder comprising from about 4% to about 6% by weight of said detergent composition of a nonionic surfactant; (b) spraying onto said base powder a further amount of nonionic surfactant in an amount from about 4% up to not more than half of the total nonionic content by weight of said detergent composition; (c) subsequent to step (b) adding a final amount of nonionic surfactant obtained by granulation with a carrier, the amounts of said surfactant and carrier being from about 2.85 to 4.0% and being about 22%, respectively, by weight of said detergent composition; and (d) subsequently adding adjunct detergent components to the base powder, said base powder being essentially free of sodium sulfate and the carrier for the nonionic surfactant comprising a mixture of zeolite and alkali metal perborate monohydrate in the amount of about 3 to 4% and about 8.5%, respectively, by weight of said detergent composition; said base powder and nonionic containing granulated carrier being present from about 59% and about 26%, respectively, by weight of said detergent composition.
Claim 3
Dependent Claim
35 words
A process according to claim 1, wherein the detergent composition comprises a mixture of nonionic and anionic surfactants in an amount from 5 to 15% and 3 to 12%, respectively, by weight of said composition.
Claim 4
Dependent Claim
14 words
A process according to claim 1, wherein the base powder contains about 5% zeolites.
Claim 5
Dependent Claim
43 words
A process according to claim 1, wherein the base powder contains less than one-half of the total quantity of nonionic surfactant and not more than one-half of the remaining portion of the total quantity of nonionic surfactant is sprayed onto the base powder.
Claim 6
Dependent Claim
30 words
A process according to claim 1, wherein about 1% of an anionic surfactant is sprayed onto the base powder together with about 4% of the nonionic surfactant in step (b).
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1990-01-26 | 1990-07-28 | 1991-01-27 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1994-01-26 | 1994-07-28 | 1995-01-27 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1998-01-26 | 1998-07-28 | 1999-01-27 | $7700.00 | Window Closed / Lapsed |