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US4643920A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for incorporating antimicrobials into fibers

Assignee: ATK Launch Systems LLC
•
Filing: 1986-03-06
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Granted: 1987-02-17
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Expires: 2006-03-06
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Abstract

Abstract A lower temperature technique for incorporating antimicrobial agents into fibers following the melt step in fiber manufacturing processes results in several advantages when contrasted with incorporation during the molten state.

Inventors

  • 👤 Thomas C. McEntee
  • 👤 Lawrence J. Guilbault
  • 👤 James F. Brophy
  • 👤 Judith L. Koob

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-01 13:14
CPC Classifications
D; D06; D06M; D06M16/00; Y; Y10; Y10S; Y10S428/00; Y10S428/907; Y10T; Y10T428/00; Y10T428/29; Y10T428/2913; Y10T428/2933; Y10T428/294; Y10T428/2964; Y10T428/2967; Y10T428/2969; Y10T428/2971

Claims Analysis

Total Claims: 24
Claim 1
Independent Claim 81 words
A method for incorporating an antimicrobial agent into a fiber, comprising: treating a fiber which does not contain an antimicrobial agent by passing said fiber into a liquid medium containing a solution of an antimicrobial agent in a concentration sufficient to cause an effective amount of said agent to be exhausted into the fiber and to be incorporated in an essentially homogeneously cross-sectional distribution throughout said fiber; said effective amount being sufficient to provide protection against microbial attack of said fiber.
Claim 2
Independent Claim 81 words
A method for incorporating an antimicrobial agent into a fiber, comprising: treating a fiber which does not contain an antimicrobial agent by passing said fiber into a liquid medium containing a solution of an antimicrobial agent in a concentration sufficient to cause an effective amount of said agent to be exhausted into the fiber and to be incorporated in an essentially homogeneously cross-sectional distribution throughout said fiber; said effective amount being sufficient to provide protection against microbial attack of said fiber.
Claim 3
Dependent Claim 26 words
The method of claim 1, wherein: said fiber is a member selected from the group consisting of synthetic fibers, semisynthetic fibers, natural fibers, and blends thereof.
Claim 4
Dependent Claim 10 words
The method of claim 2, wherein: said fiber is nylon.
Claim 5
Dependent Claim 11 words
The method of claim 3, wherein: said antimicrobial agent is 10,10'-oxybisphenoxarsine.
Claim 6
Dependent Claim 23 words
The method of claim 4, wherein: a bath volume of fiber weight ratio from about 100:1 to 1:1 is utilized during the process.
Claim 7
Dependent Claim 14 words
The method of claim 5, wherein: said ratio is from about 30:1 to 10:1.
Claim 8
Dependent Claim 21 words
The method of claim 4, wherein: said concentration of 10,10'-oxybisphenoxarsine in said medium is from about 1 ppm to 120 ppm.
Claim 9
Dependent Claim 20 words
The method of claim 7, wherein: said 10,10'-oxybisphenoxarsine concentration in said medium is from about 15 ppm to 40 ppm.
Claim 10
Dependent Claim 21 words
The method of claim 4, wherein: from about 10 ppm to 3300 ppm of 10,10'-oxybisphenoxarsine is exhausted into said nylon fiber.
Claim 11
Dependent Claim 21 words
The method of claim 9, wherein: from about 250 pm to 500 ppm of 10,10'-oxybisphenoxarsine is exhausted into said nylon fiber.
Claim 12
Dependent Claim 22 words
The method of claim 1, wherein: said antimicrobial agent is a member selected from the group consisting of 10,10'-oxybisphenoxarsine and bis(tri-n-butyl tin)oxide.
Claim 13
Dependent Claim 11 words
The method of claim 11, wherein: said antimicrobial agent is 10,10'-oxybisphenoxarsine.
Claim 14
Dependent Claim 31 words
The method of claim 1, wherein: said antimicrobial agent is 10,10'-oxybisphenoxarsine, said fiber is nylon and the concentration of said agent is said liquid medium is from about 0.001% to 1%.
Claim 15
Dependent Claim 29 words
The method of claim 1, wherein: said medium comprises an aqueous dyeing medium which also serves as to dye said fiber during passage of said fiber through the medium.
Claim 16
Dependent Claim 13 words
The method of claim 14, wherein: said medium is a beck dye bath.
Claim 17
Dependent Claim 42 words
The method of claim 1, wherein: said antimicrobial agent is a member of the group consisting of phenoxarsines, phenarsazines, maleimides, isoindole dicarboximides having a sulfur atom bonded to the nitrogen atom of the dicarboximide group, halogenated aryl alkanols, isothazolinones, and organotin compounds.
Claim 18
Dependent Claim 11 words
The method of claim 1, wherein: said antimicrobial agent is n-(2-methylnaphthyl)maleimide.
Claim 19
Dependent Claim 11 words
The method of claim 1, wherein: said antimicrobial agent is bis-n-[(1,1,2,2-tetrachloroethyl)]-4-cyclohexene-1,2-dicarboximide.
Claim 20
Dependent Claim 11 words
The method of claim 1, wherein: said antimicrobial agent is n-trichloromethylthio-4-cyclohexene-1,2-dicarboximide.
Claim 21
Dependent Claim 12 words
The method of claim 1, wherein: said antimicrobial agent is n-trichloromethylthio phthalimide.
Claim 22
Dependent Claim 12 words
The method of claim 1, wherein: said antimicrobial agent is 2,4-dichlorobenzyl alcohol.
Claim 23
Dependent Claim 11 words
The method of claim 1, wherein: said antimicrobial agent is 2-(n-octyl-4-isothiazolin-3-one.
Claim 24
Dependent Claim 11 words
The method of claim 1, wherein: said antimicrobial agent is bis(tri-n-butyltin)oxide.

References Cited (Backward Citations)

USRE21197E Cited
US3197430A Cited
US3198765A Cited
US3198764A Cited
US3282878A Cited
US3284395A Cited
US3959556A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1990-02-16 1990-08-18 1991-02-17 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1994-02-16 1994-08-18 1995-02-17 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1998-02-16 1998-08-18 1999-02-17 $7700.00 Window Closed / Lapsed

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