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US4692354A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for preparing ceramic membrane for separation of condensed component

Assignee: Mitsubishi Heavy Industries Ltd
•
Filing: 1986-08-12
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Granted: 1987-09-08
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Expires: 2006-08-12
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Abstract

Abstract A method for preparing a ceramic membrane for the separation of a condensed component which is characterized by comprising the steps of impregnating pores of a ceramic porous material with an alumina sol produced by hydrolyzing an aluminum alcoholate or an aluminum chelate; immersing the ceramic porous material into an aqueous sodium silicate solution; and subjecting the ceramic porous material to a water vapor treatment in a high-temperature water vapor.

Inventors

  • 👤 Masashi Asaeda
  • 👤 Kazutaka Mori
  • 👤 Hiroshi Makihara

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-09 12:54
CPC Classifications
C; C04; C04B; C04B41/00; C04B41/80; C04B41/81; C04B41/89; B; B01; B01D; B01D67/00; B01D67/0039; B01D67/0048; B01D71/00; B01D71/02; B01D71/05; C04B41/009; C04B41/45; C04B41/52; B01D2323/00; B01D2323/08

Claims Analysis

Total Claims: 7
Claim 1
Independent Claim 71 words
A method for preparing a ceramic membrane for the separation of a condensed component which is characterized by comprising the steps of impregnating pores of a ceramic porous material with an alumina sol produced by hydrolyzing an aluminum alcoholate or an aluminum chelate; immersing said ceramic porous material into an aqueous sodium silicate solution; and subjecting said ceramic porous material to a water vapor treatment in a high temperature water vapor.
Claim 2
Independent Claim 71 words
A method for preparing a ceramic membrane for the separation of a condensed component which is characterized by comprising the steps of impregnating pores of a ceramic porous material with an alumina sol produced by hydrolyzing an aluminum alcoholate or an aluminum chelate; immersing said ceramic porous material into an aqueous sodium silicate solution; and subjecting said ceramic porous material to a water vapor treatment in a high temperature water vapor.
Claim 3
Dependent Claim 82 words
A method for preparing ceramic membrane for the separation of a condensed component according to claim 1 which is characterized by comprising the steps of impregnating pores of a ceramic porous material with an alumina sol produced by hydrolyzing an aluminum alcoholate or an aluminum chelate; immersing said ceramic porous material into a 0.01 to 0.5 mol/l aqueous sodium silicate solution; and subjecting said ceramic porous material to a water vapor treatment at 95° to 100° C. for 0.5 to 5 hours.
Claim 4
Dependent Claim 40 words
A method according to claim 1 wherein said ceramic porous material is an optionally shaped porous material having relatively large pores (a pore diameter of which usually is 1,000 Å or more) such as foamed silica, sintered alumina or mullite.
Claim 5
Dependent Claim 21 words
A method according to claim 1 wherein said aluminum alcoholate is at least one compound selected from aluminum isopropoxide and aluminum-2-butyrate.
Claim 6
Dependent Claim 21 words
A method according to claim 1 wherein said aluminum chelate is at least one compound selected from aluminum tris(ethylacetoacetate) and ethylacetoacetate-aluminum-diisopropylate.
Claim 7
Dependent Claim 30 words
A method according to claim 2 wherein after said water vapor treatment, said ceramic porous material is immersed into boiling water in order to wash and remove alkaline components therefrom.

References Cited (Backward Citations)

US2372285A Cited
US3214287A Cited
US3539379A Cited
US3748157A Cited
US3752689A Cited
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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1990-09-07 1991-03-09 1991-09-08 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1994-09-07 1995-03-09 1995-09-08 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1998-09-07 1999-03-09 1999-09-08 $7700.00 Window Closed / Lapsed

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