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US4764474A
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Method for detecting a tagging compound
Assignee: ATK Launch Systems LLC
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Filing: 1987-07-24
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Granted: 1988-08-16
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Expires: 2007-07-24
Abstract
Abstract Tagging compounds (which function as both dyes and markers) having the following structures: ##STR1## wherein x is an integer between 0 and 3 inclusive, y is an integer between 1 and 3 inclusive, z is 0 or 1, and R is a straight or branched chain hydrocarbon having from 1 to 5 carbon atoms are disclosed. These compounds can be dissolved in a diluent at a concentration of from about 10 percent to about 30 percent, forming a concentrate which can be further dispersed in an organic liquid to form a final concentration of from about 1 ppm to about 15 ppm of said tagging compound in said liquid. Methods for detecting the presence of a tagged compound in an organic liquid are also disclosed.
Inventors
- 👤 Richard B. Orelup
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-29 19:46
CPC Classifications
C; C10; C10L; C10L1/00; C10L1/003; C09; C09B; C09B1/00; C09B1/50; C09B1/51; C09B1/515; C10L1/10; C10L1/14; C10L1/22; C10L1/222; C10L1/223; C10L1/2235; G; G01; G01N; G01N33/00; G01N33/26; G01N33/28; G01N33/2835; G01N33/2882; Y; Y10; Y10T; Y10T436/00; Y10T436/13; Y10T436/17; Y10T436/173845; Y10T436/21; Y10T436/212
Claims Analysis
Total Claims: 4
Claim 1
Independent Claim
165 words
A method for detecting a tagging compound having a structure selected from the group consisting of: ##STR5## wherein x is an integer between 0 and 3 inclusive, y is an integer between 1 and 3 inclusive, and z is 0 or 1, and ##STR6## wherein R is selected from linear or branched hydrocarbons having from 1 to about 5 carbon atoms, comprising the steps of: A. providing a sample suspected to contain said tagging compound; B. contacting said sample with a reagent comprising: i. from about 20 weight percent to about 60 weight percent glycerine; ii. from about 20 weight percent to about 40 weight percent water; and iii. from about 10 weight percent to about 50 weight percent of an organic primary amine to form an admixture therewith; C. allowing the admixture to form a sample phase and a reagent phase; and D. determining whether said reagent phase develops a substantially bluish red or red color, thereby indicating the presence of said tagging compounds.
Claim 2
Independent Claim
165 words
A method for detecting a tagging compound having a structure selected from the group consisting of: ##STR5## wherein x is an integer between 0 and 3 inclusive, y is an integer between 1 and 3 inclusive, and z is 0 or 1, and ##STR6## wherein R is selected from linear or branched hydrocarbons having from 1 to about 5 carbon atoms, comprising the steps of: A. providing a sample suspected to contain said tagging compound; B. contacting said sample with a reagent comprising: i. from about 20 weight percent to about 60 weight percent glycerine; ii. from about 20 weight percent to about 40 weight percent water; and iii. from about 10 weight percent to about 50 weight percent of an organic primary amine to form an admixture therewith; C. allowing the admixture to form a sample phase and a reagent phase; and D. determining whether said reagent phase develops a substantially bluish red or red color, thereby indicating the presence of said tagging compounds.
Claim 3
Independent Claim
141 words
A method for detecting a tagging oompound having a structure selected from a group consisting of: ##STR7## wherein x is an integer between 0 and 3 inclusive, y is an integer between 1 and 3 inclusive, and z is 0 or 1 and ##STR8## wherein R is selected from linear or branched hydrocarbons having from 1 to about 5 carbon atoms, and mixtures thereof, comprising the steps of: A. providing a sample of an organic liquid suspected to contain said tagging compound; B. passing said sample through an activated alumina chromatographic column; C. washing said organic liquid from said column with a solvent therefor; D. washing the natural colors of said organic liquid from said column with a solvent therefor; and E. determining whether a substantially purple zone is formed in said column, thereby indicating the presence of said tagging compounds.
Claim 4
Independent Claim
141 words
A method for detecting a tagging oompound having a structure selected from a group consisting of: ##STR7## wherein x is an integer between 0 and 3 inclusive, y is an integer between 1 and 3 inclusive, and z is 0 or 1 and ##STR8## wherein R is selected from linear or branched hydrocarbons having from 1 to about 5 carbon atoms, and mixtures thereof, comprising the steps of: A. providing a sample of an organic liquid suspected to contain said tagging compound; B. passing said sample through an activated alumina chromatographic column; C. washing said organic liquid from said column with a solvent therefor; D. washing the natural colors of said organic liquid from said column with a solvent therefor; and E. determining whether a substantially purple zone is formed in said column, thereby indicating the presence of said tagging compounds.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1991-08-16 | 1992-02-15 | 1992-08-16 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1995-08-16 | 1996-02-15 | 1996-08-16 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1999-08-16 | 2000-02-15 | 2000-08-16 | $7700.00 | Window Closed / Lapsed |