US4765870A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Method of manufacture of an electric moisture-content sensor
Assignee: MATEMATICKO-FYZIKALNI FAKULTA UNIVERSITY KARLOVY PRAHA 2 CZECHOSLOVAKIA
•
Filing: 1987-05-08
•
Granted: 1988-08-23
•
Expires: 2007-05-08
Abstract
Abstract The present invention relates to a method of manufacture of an electric moisture-content sensor comprising a porous layer of alumuniumoxihydroxide, the so-called boehmite, obtained by hydration of an aluminium substrate in boiling redistilled water and subsequent passivating tempering. This method, due to its simplicity, results in a larger yield in manufacture, reduced variations of parameters of individual sensors and a higher stability of their calibration curves. Due to the extraordinary prolonged stability of sensors manufactured according to this method, they can be for example applied for measuring of the moisture content of stored goods, for air-conditioning systems, for drying plants, in meteorology and also for microelectronics and in medicine.
Inventors
- 👤 Ivan Emmer
- 👤 Zdenek Hajek
- 👤 Petr Repa
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-30 00:02
CPC Classifications
C; C23; C23C; C23C22/00; C23C22/05; C23C22/06; C23C22/07; C23C22/08; C23C22/18; G; G01; G01N; G01N27/00; G01N27/02; G01N27/04; G01N27/12; G01N27/121
Claims Analysis
Total Claims: 7
Claim 1
Independent Claim
123 words
A method of manufacturing an electric moisture-content sensor comprising the steps of on a pure aluminium substrate, creating a layer of aluminiumoxihydroxide by hydratation in boiling redistilled water for 5 to 60 minutes, and passivating said layer by soaking in an aqueous solution of sodium dihydrogenphosphate of a concentration of 0.01 to 2 mol/liter at a temperature of 35 to 100 degrees C. for a time of 5 to 60 minutes; where the passivated layer of aluminiumoxihydroxide is tempered in a gaseous medium which is chemically inert to said layer, at a temperature between 70 to 110 degrees C. for 2 to 24 hours, said medium containing water vapors of a lower pressure than the tension of water vapors at the tempering temperature.
Claim 2
Independent Claim
123 words
A method of manufacturing an electric moisture-content sensor comprising the steps of on a pure aluminium substrate, creating a layer of aluminiumoxihydroxide by hydratation in boiling redistilled water for 5 to 60 minutes, and passivating said layer by soaking in an aqueous solution of sodium dihydrogenphosphate of a concentration of 0.01 to 2 mol/liter at a temperature of 35 to 100 degrees C. for a time of 5 to 60 minutes; where the passivated layer of aluminiumoxihydroxide is tempered in a gaseous medium which is chemically inert to said layer, at a temperature between 70 to 110 degrees C. for 2 to 24 hours, said medium containing water vapors of a lower pressure than the tension of water vapors at the tempering temperature.
Claim 3
Dependent Claim
18 words
The method as claimed in claim 1, where the pure aluminium substrate is a compact aluminium, polished sheet.
Claim 4
Dependent Claim
14 words
The method as claimed in claim 2, where the polished sheet is electrochemically polished.
Claim 5
Dependent Claim
14 words
The method as claimed in claim 2, where the polished sheet is chemically polished.
Claim 6
Dependent Claim
36 words
The method as claimed in claim 1, where the pure aluminium substrate is formed as a thin layer of aluminium, by vacuum evaporation on a support of silicon covered by an insulating layer of silicon dioxide.
Claim 7
Dependent Claim
35 words
The method as claimed in claim 1, where the pure aluminium substrate is formed as a thin layer of aluminium, by sputtering on a support of silicon covered by an insulating layer of silicon dioxide.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1991-08-23 | 1992-02-22 | 1992-08-23 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1995-08-23 | 1996-02-22 | 1996-08-23 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1999-08-23 | 2000-02-22 | 2000-08-23 | $7700.00 | Window Closed / Lapsed |