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US5227211A Expired / Lapsed US ⏱️ 0.0 years remaining

Magnetic recording disk medium comprising a magnetic thin film and a carbon overcoat having surface nitrogen atoms, a specified carbon structure, and oxygen atoms

Assignee: WD Media LLC
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Filing: 1991-03-05
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Granted: 1993-07-13
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Expires: 2011-03-05
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Abstract

Abstract A thin film magnetic disc having a carbon overcoat which is characterized by (a) a thickness of less than about 500 Å and (b) surface nitrogen atoms having a nitrogen (1s) electron principle binding energy, as determined by electron spectroscopy for chemical analysis (ESCA), of about 399.4 eV. The nitrogen atoms enhance lubricant adhesion to the overcoat. In a preferred embodiment, the overcoat is formed by sputtering under an argon/hydrocarbon/nitrogen gas atmosphere to produce long resistance-to-erosion times, and high lubricity properties.

Inventors

  • 👤 Atef H. Eltoukhy
  • 👤 Yassin Mehmandoust

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-28 07:11
CPC Classifications
C; C23; C23C; C23C14/00; C23C14/06; C23C14/0605; C23C14/22; C23C14/54; G; G01; G01N; G01N3/00; G01N3/56; Y; Y10; Y10S; Y10S428/00; Y10S428/90; Y10T; Y10T428/00; Y10T428/12; Y10T428/12493; Y10T428/12771; Y10T428/12806; Y10T428/12826; Y10T428/12847; Y10T428/12854; Y10T428/26; Y10T428/263; Y10T428/264; Y10T428/265; Y10T428/30; Y10T428/31504; Y10T428/3154; Y10T428/31544

Claims Analysis

Total Claims: 10
Claim 1
Independent Claim 94 words
A thin film magnetic medium comprising a substrate disc, a magnetic thin-film formed on the substrate disc, and formed on the magnetic thin-film, a carbon overcoat having a thickness less than about 500 Å, and characterized by (i) a nitrogen (1s) electron principle binding energy, as determined by electron spectrosopy for chemical analysis (ESCA), of about 399.4 eV, and (ii) a carbon structure, characterized by a carbon (1s) principle binding energy of about 284.8 eV, and oxygen atoms having an oxygen (1s) principle binding energy of about 532.5 eV, also as determined by ESCA.
Claim 2
Dependent Claim 94 words
A thin film magnetic medium comprising a substrate disc, a magnetic thin-film formed on the substrate disc, and formed on the magnetic thin-film, a carbon overcoat having a thickness less than about 500 Å, and characterized by (i) a nitrogen (1s) electron principle binding energy, as determined by electron spectrosopy for chemical analysis (ESCA), of about 399.4 eV, and (ii) a carbon structure, characterized by a carbon (1s) principle binding energy of about 284.8 eV, and oxygen atoms having an oxygen (1s) principle binding energy of about 532.5 eV, also as determined by ESCA.
Claim 3
Dependent Claim 25 words
The medium of claim 1, wherein the carbon overcoat has an oxygen abundance of no more than about 10 atom percent, as determined by ESCA.
Claim 4
Dependent Claim 32 words
The medium of claim 2, wherein the carbon overcoat includes at least about 2 atom percent nitrogen atoms, and which further includes a layer of perfluoropolyether lubricant film on the carbon overcoat.
Claim 5
Dependent Claim 77 words
An article comprising a substrate; and formed on the substrate, a carbon overcoat having (i) surface nitrogen atoms characterized by a nitrogen (1s) electron principle binding energy, as determined by electron spectrosopy for chemical analysis (ESCA), of about 399.4 eV, and (ii) a carbon structure characterized by a carbon (1s) principle binding energy of about 284.8 eV, and (iii) oxygen atoms having an oxygen (1s) principle binding energy of about 532.5 eV, also as determined by ESCA.
Claim 6
Dependent Claim 77 words
An article comprising a substrate; and formed on the substrate, a carbon overcoat having (i) surface nitrogen atoms characterized by a nitrogen (1s) electron principle binding energy, as determined by electron spectrosopy for chemical analysis (ESCA), of about 399.4 eV, and (ii) a carbon structure characterized by a carbon (1s) principle binding energy of about 284.8 eV, and (iii) oxygen atoms having an oxygen (1s) principle binding energy of about 532.5 eV, also as determined by ESCA.
Claim 7
Dependent Claim 29 words
The article of claim 4, wherein the carbon overcoat has a thickness of less than about 500 Å, and contains at least about 2 atom percent surface nitrogen atoms.
Claim 8
Dependent Claim 21 words
The article of claim 4, wherein the carbon overcoat has an oxygen abundance of no more than about 10 atom percent.
Claim 9
Dependent Claim 18 words
The article of claim 6, which further includes a layer of perfluoropolyether lubricant film on the carbon overcoat.
Claim 10
Dependent Claim 17 words
The article of claim 7, wherein the lubricant film has a thickness of between about 15-40 Å.

References Cited (Backward Citations)

US4664976A Cited
US4717622A Cited
US4833031A Cited
US4861662A Cited
US5013579A Cited
US4960609A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1996-07-12 1997-01-11 1997-07-13 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 2000-07-12 2001-01-11 2001-07-13 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2004-07-12 2005-01-11 2005-07-13 $7700.00 Window Closed / Lapsed

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