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US6562117B2 Expired / Lapsed US ⏱️ 0.0 years remaining

Process for producing pigment dispersion

Assignee: Seiko Epson Corp
•
Filing: 2001-09-13
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Granted: 2003-05-13
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Expires: 2021-09-13
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Abstract

Abstract There is provided a method for regulating the average particle diameter of a pigment for an ink composition possessing excellent anti-clogging properties and ejection stability. The method comprises the steps of: dispersing the pigment in a solvent to prepare a stock pigment dispersion; and subjecting the stock pigment dispersion to crossflow membrane filtration.

Inventors

  • 👤 Tsuyoshi Sano
  • 👤 Teruhito Kojima

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-30 22:29
CPC Classifications
C; C09; C09D; C09D11/00; C09D11/30; C09D11/32; C09D11/322; C09D17/00; C09D17/002

Claims Analysis

Total Claims: 37
Claim 1
Independent Claim 84 words
An ink composition produced by a process comprising the steps of: dispersing a pigment that is suitable as a colorant for the ink composition in a solvent to prepare a stock pigment dispersion; subjecting the stock pigment dispersion to crossflow membrane filtration to recover a liquid, which is passed through a filtration membrane, or a liquid, which is not passed through the filtration membrane, as a pigment dispersion, and mixing the pigment dispersion with water and, optionally other components to form the ink composition.
Claim 2
Dependent Claim 84 words
An ink composition produced by a process comprising the steps of: dispersing a pigment that is suitable as a colorant for the ink composition in a solvent to prepare a stock pigment dispersion; subjecting the stock pigment dispersion to crossflow membrane filtration to recover a liquid, which is passed through a filtration membrane, or a liquid, which is not passed through the filtration membrane, as a pigment dispersion, and mixing the pigment dispersion with water and, optionally other components to form the ink composition.
Claim 3
Dependent Claim 15 words
The composition according to claim 1 , wherein the membrane filtration is microfiltration or ultrafiltration.
Claim 4
Dependent Claim 26 words
The composition according to claim 1 , wherein the membrane used in the membrane filtration has an average pore diameter of 1 nm to 1 μm.
Claim 5
Dependent Claim 22 words
The composition according to claim 1 , wherein the pigment is dispersed with the aid of a polymeric dispersant or a surfactant.
Claim 6
Dependent Claim 125 words
A process for producing a dispersion of a pigment having a regulated average particle diameter, said pigment being suitable as a colorant in an ink composition, said process comprising the steps of: dispersing the pigment in a solvent to prepare a stock pigment dispersion; subjecting the stock pigment dispersion to first-stage crossflow membrane filtration to recover a liquid, which is passed through a first filtration membrane; and subjecting said liquid to second-stage crossflow membrane filtration to recover a liquid, which is not passed through a second filtration membrane, as a pigment dispersion, the average pore diameter of the first membrane used in the first-stage crossflow membrane filtration being larger than the average pore diameter of the second membrane used in the second-stage crossflow membrane filtration.
Claim 7
Dependent Claim 125 words
A process for producing a dispersion of a pigment having a regulated average particle diameter, said pigment being suitable as a colorant in an ink composition, said process comprising the steps of: dispersing the pigment in a solvent to prepare a stock pigment dispersion; subjecting the stock pigment dispersion to first-stage crossflow membrane filtration to recover a liquid, which is passed through a first filtration membrane; and subjecting said liquid to second-stage crossflow membrane filtration to recover a liquid, which is not passed through a second filtration membrane, as a pigment dispersion, the average pore diameter of the first membrane used in the first-stage crossflow membrane filtration being larger than the average pore diameter of the second membrane used in the second-stage crossflow membrane filtration.
Claim 8
Dependent Claim 20 words
The process according to claim 5 , wherein each of the first and second-stage membrane filtrations is microfiltration or ultrafiltration.
Claim 9
Dependent Claim 46 words
The process according to claim 5 , wherein the average pore diameter of the membrane used in the first-stage crossflow membrane filtration is 0.05 to 1 μm, and the average pore diameter of the membrane used in the second-stage crossflow membrane filtration is 0.001 to 0.1μm.
Claim 10
Dependent Claim 22 words
The process according to claim 5 , wherein the pigment is dispersed with the aid of a polymeric dispersant or a surfactant.
Claim 11
Dependent Claim 30 words
The process according to claim 5 , wherein the average particle diameter of the pigment has been regulated so as to fall within the range of 10 to 300 nm.
Claim 12
Dependent Claim 16 words
An ink composition comprising the pigment dispersion produced by the process according to claim 5 .
Claim 13
Dependent Claim 125 words
A process for producing a dispersion of a pigment having a regulated average particle diameter, said pigment being suitable as a colorant in an ink composition, said process comprising the steps of: dispersing the pigment in a solvent to prepare a stock pigment dispersion; subjecting the stock pigment dispersion to first-stage crossflow membrane filtration to recover a liquid, which is not passed through a first filtration membrane; and subjecting said liquid to second-stage crossflow membrane filtration to recover a liquid, which is passed through a second filtration membrane, as a pigment dispersion, the average pore diameter of the first membrane used in the first-stage crossflow membrane filtration being smaller than the average pore diameter of the second membrane used in the second-stage crossflow membrane filtration.
Claim 14
Dependent Claim 125 words
A process for producing a dispersion of a pigment having a regulated average particle diameter, said pigment being suitable as a colorant in an ink composition, said process comprising the steps of: dispersing the pigment in a solvent to prepare a stock pigment dispersion; subjecting the stock pigment dispersion to first-stage crossflow membrane filtration to recover a liquid, which is not passed through a first filtration membrane; and subjecting said liquid to second-stage crossflow membrane filtration to recover a liquid, which is passed through a second filtration membrane, as a pigment dispersion, the average pore diameter of the first membrane used in the first-stage crossflow membrane filtration being smaller than the average pore diameter of the second membrane used in the second-stage crossflow membrane filtration.
Claim 15
Dependent Claim 47 words
The process according to claim 11 , wherein the average pore diameter of the membrane used in the first-stage crossflow membrane filtration is 0.001 to 0.1 μm, and the average pore diameter of the membrane used in the second-stage crossflow membrane filtration is 0.05 to 1 μm.
Claim 16
Dependent Claim 16 words
An ink composition comprising the pigment dispersion produced by the process according to claim 11 .
Claim 17
Dependent Claim 87 words
A process for producing an ink composition comprising at least a pigment, a dispersant, and a water-soluble organic solvent, said pigment being suitable as a colorant in an ink composition, said process comprising the steps of: preparing a stock ink comprising at least a pigment, a dispersant, and a water-soluble organic solvent; and subjecting the stock ink to crossflow membrane filtration to recover a liquid, which is passed through a filtration membrane, or a liquid, which is not passed through the filtration membrane, as an ink composition.
Claim 18
Dependent Claim 87 words
A process for producing an ink composition comprising at least a pigment, a dispersant, and a water-soluble organic solvent, said pigment being suitable as a colorant in an ink composition, said process comprising the steps of: preparing a stock ink comprising at least a pigment, a dispersant, and a water-soluble organic solvent; and subjecting the stock ink to crossflow membrane filtration to recover a liquid, which is passed through a filtration membrane, or a liquid, which is not passed through the filtration membrane, as an ink composition.
Claim 19
Dependent Claim 15 words
The process according to claim 14 , wherein the membrane filtration is microfiltration or ultrafiltration.
Claim 20
Dependent Claim 26 words
The process according to claim 14 , wherein the membrane used in the membrane filtration has an average pore diameter of 1 nm to 1 μm.
Claim 21
Dependent Claim 17 words
The process according to claim 14 , wherein the dispersant is a polymeric dispersant or a surfactant.
Claim 22
Dependent Claim 12 words
An ink composition produced by the process according to claim 7 .
Claim 23
Dependent Claim 132 words
A process for producing an ink composition comprising at least a pigment, a dispersant, and a water-soluble organic solvent, said pigment being suitable as a colorant in an ink composition, said process comprising the steps of: preparing a stock ink comprising at least a pigment, a dispersant, and a water-soluble organic solvent; subjecting the stock ink to first-stage crossflow membrane filtration to recover a liquid which is passed through a first filtration membrane; and subjecting said liquid to second-stage crossflow membrane filtration to recover a liquid, which is not passed through a second filtration membrane, as an ink composition, the average pore diameter of the first membrane used in the first-stage crossflow membrane filtration being larger than the average pore diameter of the second membrane used in the second-stage crossflow membrane filtration.
Claim 24
Dependent Claim 132 words
A process for producing an ink composition comprising at least a pigment, a dispersant, and a water-soluble organic solvent, said pigment being suitable as a colorant in an ink composition, said process comprising the steps of: preparing a stock ink comprising at least a pigment, a dispersant, and a water-soluble organic solvent; subjecting the stock ink to first-stage crossflow membrane filtration to recover a liquid which is passed through a first filtration membrane; and subjecting said liquid to second-stage crossflow membrane filtration to recover a liquid, which is not passed through a second filtration membrane, as an ink composition, the average pore diameter of the first membrane used in the first-stage crossflow membrane filtration being larger than the average pore diameter of the second membrane used in the second-stage crossflow membrane filtration.
Claim 25
Dependent Claim 47 words
The process according to claim 19 , wherein the average pore diameter of the membrane used in the first-stage crossflow membrane filtration is 0.05 to 1 μm, and the average pore diameter of the membrane used in the second-stage crossflow membrane filtration is 0.001 to 0.1 μm.
Claim 26
Dependent Claim 30 words
The process according to claim 19 , wherein the average particle diameter of the pigment has been regulated so as to fall within the range of 10 to 300 nm.
Claim 27
Dependent Claim 17 words
The process according to claim 19 , wherein the dispersant is a polymeric dispersant or a surfactant.
Claim 28
Dependent Claim 12 words
An ink composition produced by the process according to claim 19 .
Claim 29
Dependent Claim 132 words
A process for producing an ink composition comprising at least a pigment, a dispersant, and a water-soluble organic solvent, said pigment being suitable as a colorant in an ink composition, said process comprising the steps of: preparing a stock ink comprising at least a pigment, a dispersant, and a water-soluble organic solvent; subjecting the stock ink to first-stage crossflow membrane filtration to recover a liquid which is not passed through a first filtration membrane; and subjecting said liquid to second-stage crossflow membrane filtration to recover a liquid, which is passed through a second filtration membrane, as an ink composition, the average pore diameter of the first membrane used in the first-stage crossflow membrane filtration being smaller than the average pore diameter of the second membrane used in the second-stage crossflow membrane filtration.
Claim 30
Dependent Claim 132 words
A process for producing an ink composition comprising at least a pigment, a dispersant, and a water-soluble organic solvent, said pigment being suitable as a colorant in an ink composition, said process comprising the steps of: preparing a stock ink comprising at least a pigment, a dispersant, and a water-soluble organic solvent; subjecting the stock ink to first-stage crossflow membrane filtration to recover a liquid which is not passed through a first filtration membrane; and subjecting said liquid to second-stage crossflow membrane filtration to recover a liquid, which is passed through a second filtration membrane, as an ink composition, the average pore diameter of the first membrane used in the first-stage crossflow membrane filtration being smaller than the average pore diameter of the second membrane used in the second-stage crossflow membrane filtration.
Claim 31
Dependent Claim 20 words
The process according to claim 19 , wherein each of the first-stage and second-stage membrane filtrations is microfiltration or ultrafiltration.
Claim 32
Dependent Claim 47 words
The process according to claim 24 , wherein the average pore diameter of the membrane used in the first-stage crossflow membrane filtration is 0.001 to 0.1 μm, and the average pore diameter of the membrane used in the second-stage crossflow membrane filtration is 0.05 to 1 μm.
Claim 33
Dependent Claim 12 words
An ink composition produced by the process according to claim 15 .
Claim 34
Dependent Claim 32 words
A method for ink jet printing comprising (a) providing the ink composition of claim 1 ; (b) ejecting droplets of the ink composition onto a recording medium to produce an image thereon.
Claim 35
Dependent Claim 32 words
A method for ink jet printing comprising (a) providing the ink composition of claim 13 ; (b) ejecting droplets of the ink composition onto a recording medium to produce an image thereon.
Claim 36
Dependent Claim 32 words
A method for ink jet printing comprising (a) providing the ink composition of claim 18 ; (b) ejecting droplets of the ink composition onto a recording medium to produce an image thereon.
Claim 37
Dependent Claim 32 words
A method for ink jet printing comprising (a) providing the ink composition of claim 23 ; (b) ejecting droplets of the ink composition onto a recording medium to produce an image thereon.

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