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EP0179589A2 Expired / Lapsed EP ⏱️ 0.0 years remaining

Densification of ceramic materials

Assignee: Babcock and Wilcox Co
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Filing: 1985-10-07
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Granted: —
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Expires: 2005-10-07
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Abstract

Abstract Supercritical fluids may be used to carry ceramic precursor materials into the pores of ceramic host. Reducing the solubility of a ceramic precursor in the supercritical fluid will assist deposition of the ceramic precursor in the pores or void spaces of the ceramic host to accomplish densification of the ceramic host material.

Inventors

  • 👤 Philip L. Berneburg
  • 👤 Val J. Krukonis

Bibliographic Details

Application Number —
Jurisdiction EP
Data Source google_patents
Last Synchronized 2026-10-30 20:17
CPC Classifications
C; C04; C04B; C04B41/00; C04B41/009; C04B35/00; C04B35/515; C04B35/56; C04B35/565; C04B35/571; C04B35/58; C04B35/584; C04B35/589; C04B35/71; C04B35/78; C04B35/80; C04B41/45; C04B41/50; C04B41/5025; C04B41/5053; C04B41/80; C04B41/81; C04B41/85; C04B41/87

Claims Analysis

Total Claims: 14
Claim 1
Independent Claim 55 words
A process for increasing the density of a ceramic material characterised by:- a. dissolving a ceramic precursor in a supercritical fluid; b. infiltrating the ceramic material with the ceramic precursor-laden fluid; and c. reducing the solubility of the ceramic precursor in the fluid to deposit the ceramic precursor in void spaces of the ceramic material.
Claim 2
Dependent Claim 55 words
A process for increasing the density of a ceramic material characterised by:- a. dissolving a ceramic precursor in a supercritical fluid; b. infiltrating the ceramic material with the ceramic precursor-laden fluid; and c. reducing the solubility of the ceramic precursor in the fluid to deposit the ceramic precursor in void spaces of the ceramic material.
Claim 3
Dependent Claim 33 words
A process according to claim 1, wherein the supercritical fluid is one selected from the group consisting of methane, ethylene, carbon dioxide, ethane, nitrous oxide, propane, butane, and chloro-, fluoro-, and chloro fluoro-hydrocarbons.
Claim 4
Dependent Claim 58 words
A process for increasing the density of a silicon nitride material characterised by:- a. dissolving a ceramic precursor in a supercritical fluid; b. infiltrating the silicon nitride material with the ceramic precursor-laden fluid; and c. reducing the solubility of the ceramic precursor in the fluid to deposit the ceramic precursor in void spaces of the silicon nitride material.
Claim 5
Dependent Claim 58 words
A process for increasing the density of a silicon nitride material characterised by:- a. dissolving a ceramic precursor in a supercritical fluid; b. infiltrating the silicon nitride material with the ceramic precursor-laden fluid; and c. reducing the solubility of the ceramic precursor in the fluid to deposit the ceramic precursor in void spaces of the silicon nitride material.
Claim 6
Dependent Claim 17 words
A process according to claim 3, wherein the silicon nitride is a porous reaction sintered silicon nitride.
Claim 7
Dependent Claim 22 words
A process according to claim 3, wherein the ceramic precursor is a silicon-containing polymeric material which acts as a silicon nitride precursor.
Claim 8
Dependent Claim 59 words
A process for increasing the density of a silicon carbide material characterised by:- a. dissolving a ceramic precursor in a supercritical fluid; b. infiltrating the silicon carbide material with the ceramic precursor-laden fluid; and c. reducing the solubility of the ceramic precursor in the supercritical fluid to deposit the ceramic precursor in void spaces of the silicon carbide material.
Claim 9
Dependent Claim 59 words
A process for increasing the density of a silicon carbide material characterised by:- a. dissolving a ceramic precursor in a supercritical fluid; b. infiltrating the silicon carbide material with the ceramic precursor-laden fluid; and c. reducing the solubility of the ceramic precursor in the supercritical fluid to deposit the ceramic precursor in void spaces of the silicon carbide material.
Claim 10
Dependent Claim 22 words
A process according to claim 6, wherein the ceramic precursor is a silicon-containing polymeric material which acts as a silicon carbide precursor.
Claim 11
Dependent Claim 20 words
A process according to claim 6, wherein the silicon-containing polymeric material which acts as a silicon carbide precursor is polysilane.
Claim 12
Dependent Claim 59 words
A process for increasing the density of an aluminum borosilicate material characterised by:- a. dissolving a ceramic precursor in a supercritical fluid; b. infiltrating the aluminum borosilicate material with the ceramic precursor-laden fluid; and c. reducing the solubility of the ceramic precursor in the supercritical fluid to deposit the ceramic precursor in void spaces of the aluminum borosilicate material.
Claim 13
Dependent Claim 59 words
A process for increasing the density of an aluminum borosilicate material characterised by:- a. dissolving a ceramic precursor in a supercritical fluid; b. infiltrating the aluminum borosilicate material with the ceramic precursor-laden fluid; and c. reducing the solubility of the ceramic precursor in the supercritical fluid to deposit the ceramic precursor in void spaces of the aluminum borosilicate material.
Claim 14
Dependent Claim 13 words
A process according to claim 7, wherein the ceramic precursor is aluminum isopropoxide.

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