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US3618618A Expired / Lapsed US ⏱️ 0.0 years remaining

Tobacco smoke filtering material

Assignee: ROBERT L STRICKMAN FOUNDATION Inc
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Filing: 1968-04-11
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Granted: 1971-11-09
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Expires: 1988-04-11
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Abstract

Abstract Filter materials for filtering aerosols, such as cigarette filters for filtering tobacco smoke, are provided comprising rigid polyurethane particles devoid of any cellular structure. Preferably the particles are granular and of jagged, spiny, cragged nature. The rigid polyurethane is produced from a polyol and a polyisocyanate. The particles are produced by first preparing a rigid polyurethane foam, preferably with the aid of a blowing agent, granulating the foam, treating the granules with hot water or steam to hydrolyze unreacted isocyanate and other free materials to render them inert, and then dried. Preferably, inorganic additives may be present during the preparation of the rigid polyurethane foam, such as the lower alkyl silicates, e.g., ethyl silicate, and water soluble salts of the acids of metals of groups VA and VIA of the Periodic Table, e.g., sodium tungstate. Inorganic additives may be added to the filter particles, such as an alkaline earth metal carbonate, silicate or hydroxide.

Inventors

  • 👤 Robert L Strickman

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-02 10:00
CPC Classifications
C; C08; C08J; C08J3/00; C08J3/12; A; A24; A24D; A24D3/00; A24D3/06; A24D3/08; B; B01; B01D; B01D39/00; B01D39/14; B01D39/16; B01D39/1638; B01D39/1653; B01D39/1669; B01D39/1676; C08J2375/00; C08J2375/04; Y; Y10; Y10S; Y10S264/00; Y10S264/17; Y10S521/00; Y10S521/918

Claims Analysis

Total Claims: 17
Claim 1
Independent Claim 13 words
A filtering material according to claim 1 wherein the polyisocyanate is tolylene diisocyanate.
Claim 2
Dependent Claim 22 words
A filter material according to claim 1 produced from a foam having a density of less than 3 pounds per cubic foot.
Claim 3
Dependent Claim 19 words
A filtering material according to claim 1 having the particles of a particle size of less than 750 microns.
Claim 4
Dependent Claim 21 words
A filtering material according to claim 1 having the particles of a particle size of between about 150 and 600 microns.
Claim 5
Dependent Claim 17 words
A filtering material according to claim 1 in which the particles are in the form of granules.
Claim 6
Dependent Claim 18 words
A filtering material according to claim 1 wherein the polyol has a hydroxyl number of at least 300.
Claim 7
Dependent Claim 35 words
A filtering material according to claim 1 wherein the amounts of polyisocyanate and polyol are such as to provide a ratio of reactive isocyanate groups to organic hydroxyl groups of between about 0.75 and 1.25.
Claim 8
Dependent Claim 25 words
A filtering material according to claim 1 wherein between about 40 and 150 parts by weight of polyisocyanate are employed for 100 parts of polyol.
Claim 9
Dependent Claim 25 words
A filtering material according to claim 1 further including a member selected from the group consisting of alkaline earth metal carbonates, silicates, oxides and hydroxides.
Claim 10
Dependent Claim 21 words
A filtering material according to claim 10, wherein said member is present in an amount not exceeding 25 percent by weight.
Claim 11
Dependent Claim 11 words
A filtering material according to claim 1 further including magnesium trisilicate.
Claim 12
Dependent Claim 11 words
A filtering material according to claim 1 further including magnesium hydroxide.
Claim 13
Dependent Claim 11 words
A filtering material according to claim 1 further including aluminum hydroxide
Claim 14
Dependent Claim 29 words
A filtering material according to claim 1 further including between about 3 and 15 percent by weight of an approximately equal parts mixture of aluminum hydroxide and magnesium trisilicate.
Claim 15
Dependent Claim 9 words
A filter unit containing particles in accordance with claim
Claim 16
Dependent Claim 11 words
A cigarette containing the filter unit in accordance with claim 1.
Claim 17
Dependent Claim 11 words
A filtering material according to claim 1 further including charcoal granules.

References Cited (Backward Citations)

US1950542A Cited
US2181614A Cited
US2770241A Cited
GB753203A Cited
US2820461A Cited
US2834354A Cited
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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1974-11-08 1975-05-10 1975-11-09 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1978-11-08 1979-05-10 1979-11-09 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1982-11-08 1983-05-10 1983-11-09 $7700.00 Window Closed / Lapsed

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