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Catalysts

Assignee: Lever Brothers Co
•
Filing: 1969-12-30
•
Granted: 1972-06-27
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Expires: 1989-12-30
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Abstract

Abstract In a process for the preparation of a nickel-on-silica catalyst, the use of an intimate mixture of an organic base, which base is substantially insoluble in the suspension of silica in aqueous nickel salt solution, as a means of withdrawing hydrogen ions from the solution and causing precipitation of nickel from the solution on to the silica carrier.

Inventors

  • 👤 Bastiaan Gerardus Linsen
  • 👤 Theo Jan Osinga

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-29 22:31
CPC Classifications
C; C09; C09K; C09K5/00; C09K5/02; C09K5/04; C09K5/041; B; B01; B01J; B01J23/00; B01J23/70; B01J23/74; B01J23/755; B01J35/00; B01J35/60; B01J21/00; B01J21/06; B01J21/08; B01J35/61; B01J35/615; B01J35/64; B01J35/647; B01J37/00; B01J37/02; B01J37/03; B01J37/031; B01J37/16; B01J37/18; Y; Y10; Y10S; Y10S502/00; Y10S502/506; Y10S502/509

Claims Analysis

Total Claims: 9
Claim 1
Independent Claim 33 words
A process as claimed in claim 1 in which the organic base is selected from primary and secondary alkyl amines containing in the alkyl groups a total of at least 8 carbon atoms.
Claim 2
Dependent Claim 29 words
A process as claimed in claim 2 in which the organic base comprises a mixture of t-alkyl amines, the t-alkyl groups of which contain 12 to 14 carbon atoms.
Claim 3
Dependent Claim 30 words
A process as claimed in claim 2 in which the organic basee comprises a mixture of t-alkyl amines, the t-alkyl groups of which contain contain 18 to 22 carbon atoms.
Claim 4
Dependent Claim 39 words
A process as claimed in claim 1 in which the organic base is dissolved in an organic solvent that is substantially insoluble in the aqueous salt solution and that does not react with it under the reaction conditions employed.
Claim 5
Dependent Claim 13 words
A process as claimed in claim 5 in which the solvent comprises chloroform.
Claim 6
Dependent Claim 35 words
A process as claimed in claim 1 in which the nickel salt comprises nickel sulphate and in which the concentration calculated as NiSO4.6 H2O in the aqueous solution is 1 to 5 percent by weight.
Claim 7
Dependent Claim 25 words
A process as claimed in claim 1 in which the silica containing carrier material comprises silica with a specific surface of 5 to 750 m2/g.
Claim 8
Dependent Claim 26 words
A process as claimed in claim 8 in which the silica has a significant part of its pores with a diameter of more than 25 A.
Claim 9
Dependent Claim 29 words
A process as claimed in claim 1 in which the solid material before drying is washed with a water miscible organic solvent having a boiling point below 100* C.

References Cited (Backward Citations)

US1232830A Cited
US1280314A Cited
US1375368A Cited
US1695666A Cited
US1783662A Cited
US2381198A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1975-06-27 1975-12-27 1976-06-27 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1979-06-27 1979-12-27 1980-06-27 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1983-06-27 1983-12-27 1984-06-27 $7700.00 Window Closed / Lapsed

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