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Carbodiimide catalysts and processes

Assignee: 3M Co
•
Filing: 1973-06-08
•
Granted: 1975-01-28
•
Expires: 1993-06-08
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Abstract

Abstract Phosphine oxides are prepared from terpenes and are found to be valuable as catalysts in the condensation of isocyanates to yield carbodiimides.

Inventors

  • 👤 Robert L Hansen

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-30 18:27
CPC Classifications
C; C07; C07F; C07F9/00; C07F9/02; C07F9/28; C07F9/50; C07F9/53

Claims Analysis

Total Claims: 10
Claim 1
Independent Claim 28 words
A BICYCLE TERPENE ALKYL OR HYDROCARBYL ARYL PHOSPHINE OXIDE WHEREIN ALKYL IS OF 1 TO 10 CARBON ATOMS AND HYDROCARBYL ARYL IS OF 6 TO 10 CARBON ATOMS.
Claim 2
Dependent Claim 28 words
A BICYCLE TERPENE ALKYL OR HYDROCARBYL ARYL PHOSPHINE OXIDE WHEREIN ALKYL IS OF 1 TO 10 CARBON ATOMS AND HYDROCARBYL ARYL IS OF 6 TO 10 CARBON ATOMS.
Claim 3
Dependent Claim 4 words
Camphene phenyl phosphine oxide.
Claim 4
Dependent Claim 4 words
Camphene phenyl phosphine oxide.
Claim 5
Dependent Claim 4 words
Pinene phenyl phosphine oxide.
Claim 6
Dependent Claim 4 words
Pinene phenyl phosphine oxide.
Claim 7
Dependent Claim 43 words
A process for the production of alkyl or hydrocarbyl aryl phosphine oxide comprising condensing a bicyclic C10H16 terpene with 1 to 10 carbon atom alkyl phosphine dihalide or 6 to 10 carbon atom hydrocarbyl aryl phosphine dihalide in the presence of Friedel-Crafts catalyst.
Claim 8
Dependent Claim 43 words
A process for the production of alkyl or hydrocarbyl aryl phosphine oxide comprising condensing a bicyclic C10H16 terpene with 1 to 10 carbon atom alkyl phosphine dihalide or 6 to 10 carbon atom hydrocarbyl aryl phosphine dihalide in the presence of Friedel-Crafts catalyst.
Claim 9
Dependent Claim 11 words
The process according to claim 4 wherein the terpene is camphene.
Claim 10
Dependent Claim 13 words
The process according to claim 4 wherein the phosphine dihalide is phenyl dichlorophosphine.

References Cited (Backward Citations)

US2663737A Cited
US2663739A Cited
US3331873A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1978-01-27 1978-07-29 1979-01-28 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1982-01-27 1982-07-29 1983-01-28 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1986-01-27 1986-07-29 1987-01-28 $7700.00 Window Closed / Lapsed

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