Patent US3890209A successfully refreshed from Google Patents.
US3890209A
Expired / Lapsed
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Abrasion resistant mechanical member with composite nickel-plating layer having meshlike porous portion and a method for manufacture thereof
Assignee: Mazda Motor Corp
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Filing: 1973-06-01
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Granted: 1975-06-17
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Expires: 1993-06-01
Abstract
Abstract An abrasion resistant mechanical member haivng a composite nickel plating layer on the surface of the member, which is formed by electrolysis by the use of a nickel electroplating bath. To achieve the intended purpose, the nickel electroplating bath is added with tensile stress accelerating agent and compression stress accelerating agent in addition to ceramic powder. The electrodeposited member is subsequently subjected to reverse electrolysis for forming a porous portion in the composite nickel electroplating layer which exhibits an excellent oil retention together with abrasion resistance.
Inventors
- 👤 Toshihiko Shigeta
- 👤 Toshio Yamada
- 👤 Takao Sasame
- 👤 Yoshitaka Uebayashi
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-01 09:21
CPC Classifications
C; C25; C25D; C25D15/00; C25D15/02; Y; Y10; Y10T; Y10T428/00; Y10T428/12; Y10T428/12479; Y10T428/12493; Y10T428/12535; Y10T428/12625; Y10T428/12771; Y10T428/12861; Y10T428/12944
Claims Analysis
Total Claims: 8
Claim 1
Independent Claim
51 words
AN ABRASION-RESISTANT MECHANICAL MEMBER WHICH COMPRISES A COMPOSITE NICKEL-ELECTROPLATED LAYER ON THE SURFACE OF SAID MEMBER, SAID LAYER HAVING A MESH-LIKE POROUS PORTION WHICH CONTAINS THEREIN CERAMIC POWDER AS AN ABRASION RESISTANT ELEMENT, SAID POROUS PORTION BEING COMPOSED OF GROOVES OF APPROXIMATELY 0.01 TO 0.5 MM IN WIDTH AND PERCENT AT
Claim 2
Dependent Claim
51 words
AN ABRASION-RESISTANT MECHANICAL MEMBER WHICH COMPRISES A COMPOSITE NICKEL-ELECTROPLATED LAYER ON THE SURFACE OF SAID MEMBER, SAID LAYER HAVING A MESH-LIKE POROUS PORTION WHICH CONTAINS THEREIN CERAMIC POWDER AS AN ABRASION RESISTANT ELEMENT, SAID POROUS PORTION BEING COMPOSED OF GROOVES OF APPROXIMATELY 0.01 TO 0.5 MM IN WIDTH AND PERCENT AT
Claim 3
Independent Claim
221 words
A method for manufacturing an abrasion-resistant mechanical member having a composite nickel-electroplated layer on the surface of said member, said layer having a mesh-like porous portion which contains therein ceramic powder as an abrasion resistant element and is cOmposed of grooves of approximately 0.01 to 0.5 mm. in width and present at intervals of approximately 0.5 to 9 mm. thereby to provide an oil retention characteristic, which comprises a step of electrodepositing a workpiece in a nickel-plating bath containing therein a ceramic powder in an amount of 50 to 500 g/lit., said bath further containing a tensile stress accelerating agent in an amount of 0.05 to 5 g/lit. with respect to the total volume of said bath and a compression stress accelerating agent in an amount of 0.1 to 10 g/lit. with respect to the total volume of said bath, the amount of said compression stress accelerating agent being sufficient to permit the action of said tensile stress accelerating agent to overcome the action of said compression stress accelerating agent, thereby to form the nickel-electroplated layer having fine cracks developing in a mesh-like manner and caused by the presence of said tensile stress accelerating agent, and a step of subjecting the resultant member to reverse electrolysis thereby to impart the particular grooves of the particular size to said composite nickel-electroplated layer.
Claim 4
Independent Claim
221 words
A method for manufacturing an abrasion-resistant mechanical member having a composite nickel-electroplated layer on the surface of said member, said layer having a mesh-like porous portion which contains therein ceramic powder as an abrasion resistant element and is cOmposed of grooves of approximately 0.01 to 0.5 mm. in width and present at intervals of approximately 0.5 to 9 mm. thereby to provide an oil retention characteristic, which comprises a step of electrodepositing a workpiece in a nickel-plating bath containing therein a ceramic powder in an amount of 50 to 500 g/lit., said bath further containing a tensile stress accelerating agent in an amount of 0.05 to 5 g/lit. with respect to the total volume of said bath and a compression stress accelerating agent in an amount of 0.1 to 10 g/lit. with respect to the total volume of said bath, the amount of said compression stress accelerating agent being sufficient to permit the action of said tensile stress accelerating agent to overcome the action of said compression stress accelerating agent, thereby to form the nickel-electroplated layer having fine cracks developing in a mesh-like manner and caused by the presence of said tensile stress accelerating agent, and a step of subjecting the resultant member to reverse electrolysis thereby to impart the particular grooves of the particular size to said composite nickel-electroplated layer.
Claim 5
Dependent Claim
23 words
A method as claimed in claim 2, wherein said tensile stress accelerating agent is butyne-2-diol-1,4 and said compression stress accelerating agent is saccharin.
Claim 6
Dependent Claim
25 words
A method as claimed in claim 3, wherein the reverse electrolysis is carried by the use of a chromium acid bath of 1 to 50%.
Claim 7
Dependent Claim
53 words
A method as claimed in claim 2, wherein said nickel electroplating bath comprises a chloride bath and wherein the amount of said tensile stress accelerating agent is within the range of 0.05 to 2 g/lit. and the amount of said compression stress accelerating agent is within the range of 0.1 to 5 g/lit.
Claim 8
Dependent Claim
37 words
A method as claimed in claim 4 wherein the electrodepositing is carried out at a bath temperature of 40* to 75*C, a current density of 2 to 50 A/dm2 and a pH value of 3.5 to 5.3.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1978-06-16 | 1978-12-16 | 1979-06-17 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1982-06-16 | 1982-12-16 | 1983-06-17 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1986-06-16 | 1986-12-16 | 1987-06-17 | $7700.00 | Window Closed / Lapsed |