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US3965086A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for producing protein concentrate (case) 1 using air classification

Assignee: Procter and Gamble Co
•
Filing: 1975-01-03
•
Granted: 1976-06-22
•
Expires: 1995-01-03
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Abstract

Abstract A process for concentrating oilseed protein which comprises the steps of fine grinding and air-classifying the initial protein source and washing the ground protein source with water at a pH of about 4 to 6 or with a 20% to 80% by weight alcohol solution.

Inventors

  • 👤 Ronald Bruce Swain
  • 👤 David Evans O'Connor

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-29 23:34
CPC Classifications
A; A23; A23J; A23J1/00; A23J1/14; A23J1/142

Claims Analysis

Total Claims: 19
Claim 1
Independent Claim 104 words
A process for producing a protein concentrate which comprises the steps of: a. fine grinding an oilseed meal so that 90% of the particles obtained thereby are less than 100 microns in diameter and air-classifying the resulting ground meal into a fraction which is characterized by its relatively high protein content and relatively low water-insoluble carbohydrate content; and b. washing said fraction either in water or in a 20% to 80% by weight aqueous alcohol solution wherein the alcohol component of said solution is selected from the group consisting of methanol, ethanol, and isopropanol and separating the protein containing residue from the liquid supernatant.
Claim 2
Dependent Claim 104 words
A process for producing a protein concentrate which comprises the steps of: a. fine grinding an oilseed meal so that 90% of the particles obtained thereby are less than 100 microns in diameter and air-classifying the resulting ground meal into a fraction which is characterized by its relatively high protein content and relatively low water-insoluble carbohydrate content; and b. washing said fraction either in water or in a 20% to 80% by weight aqueous alcohol solution wherein the alcohol component of said solution is selected from the group consisting of methanol, ethanol, and isopropanol and separating the protein containing residue from the liquid supernatant.
Claim 3
Dependent Claim 45 words
The process of claim 1 wherein subsequent to the grinding and air-classifying step and prior to the washing step there is inserted a heat-denaturing step such that the protein component of said air-classified fraction is substantially insoluble in water at a pH of about 7.
Claim 4
Dependent Claim 26 words
The process of claim 1 wherein the oilseed meal is selected from the group consisting of soy, cottonseed, sunflower, peanut, safflower, rapeseed, or sesame seed meals.
Claim 5
Dependent Claim 21 words
The process of claim 1 wherein the meal is washed in water at a pH of about 4 to about 6.
Claim 6
Dependent Claim 26 words
The process of claim 1 wherein the oilseed meal is soy meal and said meal is water-washed at a pH of about 4 to about 5.
Claim 7
Dependent Claim 25 words
The process of claim 1 wherein the oilseed meal is cottonseed and said meal is water-washed at a pH of about 4.5 to about 5.5.
Claim 8
Dependent Claim 27 words
The process of claim 1 wherein the oilseed meal is finely ground such that 90% of the particles obtained thereby are less than 60 microns in diameter.
Claim 9
Dependent Claim 93 words
The process of producing a protein concentrate which comprises the steps of: a. fine grinding an oilseed meal so that 90% of the particles obtained thereby are less than 60 microns in diameter and air-classifying the resulting ground meal into at least two fractions of which at least one fraction is characterized by its relatively high protein content and relatively low water-insoluble carbohydrate content; b. washing said fraction either in water or in a 20% to 80% by weight aqueous alcohol solution; and c. separating the protein containing residue from the liquid supernatant.
Claim 10
Dependent Claim 93 words
The process of producing a protein concentrate which comprises the steps of: a. fine grinding an oilseed meal so that 90% of the particles obtained thereby are less than 60 microns in diameter and air-classifying the resulting ground meal into at least two fractions of which at least one fraction is characterized by its relatively high protein content and relatively low water-insoluble carbohydrate content; b. washing said fraction either in water or in a 20% to 80% by weight aqueous alcohol solution; and c. separating the protein containing residue from the liquid supernatant.
Claim 11
Dependent Claim 45 words
The process of claim 8 wherein subsequent to the grinding and air-classifying step and prior to the washing step there is inserted a heat-denaturing step such that the protein component of said air-classified fraction is substantially insoluble in water at a pH of about 7.
Claim 12
Dependent Claim 26 words
The process of claim 8 wherein the oilseed meal is selected from the group consisting of soy, cottonseed, sunflower, peanut, safflower, rapeseed, or sesame seed meals.
Claim 13
Dependent Claim 21 words
The process of claim 8 wherein the meal is washed in water at a pH of about 4 to about 6.
Claim 14
Dependent Claim 26 words
The process of claim 8 wherein the oilseed meal is soy meal and said meal is water-washed at a pH of about 4 to about 5.
Claim 15
Dependent Claim 25 words
The process of claim 8 wherein the oilseed meal is cottonseed and said meal is water-washed at a pH of about 4.5 to about 5.5.
Claim 16
Dependent Claim 26 words
The process of claim 8 wherein the alcohol component of the aqueous alcohol washing step is selected from the group consisting of methanol, ethanol, and isopropanol.
Claim 17
Dependent Claim 112 words
The process for concentrating the protein material of an oilseed meal which comprises the steps of: a. washing said meal either in water or in a 20% to 80% by weight aqueous alcohol solution; b. separating the insoluble portion of said washed meal from the liquid supernatant; c. drying the insoluble portion of said washed meal; d. fine grinding the insoluble portion of said oilseed meal so that 90% of the particles obtained thereby are less than 60 microns in diameter and air-classifying the resulting ground meal into at least two fractions of which at least one fraction is characterized by its relatively high protein content and relatively low water-insoluble carbohydrate content.
Claim 18
Dependent Claim 112 words
The process for concentrating the protein material of an oilseed meal which comprises the steps of: a. washing said meal either in water or in a 20% to 80% by weight aqueous alcohol solution; b. separating the insoluble portion of said washed meal from the liquid supernatant; c. drying the insoluble portion of said washed meal; d. fine grinding the insoluble portion of said oilseed meal so that 90% of the particles obtained thereby are less than 60 microns in diameter and air-classifying the resulting ground meal into at least two fractions of which at least one fraction is characterized by its relatively high protein content and relatively low water-insoluble carbohydrate content.
Claim 19
Dependent Claim 24 words
The process of claim 12 wherein the alcohol component in the water-washing step is selected from the group consisting of methanol, ethanol, and isopropanol.

References Cited (Backward Citations)

US2355547A Cited
US2635094A Cited
US2881076A Cited
US3218307A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1979-06-22 1979-12-22 1980-06-22 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1983-06-22 1983-12-22 1984-06-22 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1987-06-22 1987-12-22 1988-06-22 $7700.00 Window Closed / Lapsed

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