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US4034126A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for coating granular materials

Assignee: Takeda Pharmaceutical Co Ltd
•
Filing: 1975-10-10
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Granted: 1977-07-05
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Expires: 1995-10-10
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Abstract

Abstract A process for coating granular materials particularly applicable in coating granular materials each having a particle size within the range of 100 to 1,000 microns, wherein supply of a coating or binding liquid is effected in response to a specific measured electro-resistance of a fluidized means of the granular materials while supply of a coating powder is continuously effected in a predetermined variable rate. To this end, at least one electrode cooperates with a portion of the wall forming a coating apparatus to detect the specific electro-resistance which is in turn compared with a predetermined value in a comparison circuit.

Inventors

  • 👤 Yoshiro Funakoshi
  • 👤 Yoshihiko Matsumura
  • 👤 Masaki Yamamoto
  • 👤 Hiromu Komeda

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-03 09:21
CPC Classifications
B; B01; B01J; B01J2/00; B01J2/006; A; A61; A61K; A61K9/00; A61K9/48; A61K9/50; A61K9/5089

Claims Analysis

Total Claims: 10
Claim 1
Independent Claim 290 words
A process for coating granular material having granules with a particle size within the range of 100 to 1,000 microns in a coating apparatus of the type having a rotatable dish, which dish is mounted in a stationary vessel, said stationary vessel having a rising inner surface contiguous to the periphery of said dish and curved upwardly therefrom to define a steadily rising surface from said dish, which comprises charging said granular material into said vessel and onto said rotatable dish while said rotatable dish is rotated at a predetermined speed, intermittently supplying a binding solution to said vessel by measuring the specific electro-resistance of a mass of said granular material by means of a detector including at least one electrode which is spaced from a portion of the rising inner surface of the vessel, feeding a signal indicative of the detected specific electro-resistance to a comparision circuit, comparing said signal from said detector with a reference value fed from a reference signal generator, said comparision circuit generating a control pulse only when said detected specific electro-resistance exceeds the reference value and continuing the generation of such control pulse during a period in which said detected specific electro-resistance is in excess of said reference value, said binding solution spraying being effected under a predetermined pressure onto the fluidized mass of said granular material by means of an electromagnetic valve opened by said control pulse during the duration of said control pulse, the electro-magnetic valve being closed to discontinue spraying when the detected specific electro-resistance is less than the reference value and no control pulse is generated from said comparision circuit, and feeding coating powder continuously throughout the coating operation onto the fluidized mass of said granular material within said vessel.
Claim 2
Dependent Claim 290 words
A process for coating granular material having granules with a particle size within the range of 100 to 1,000 microns in a coating apparatus of the type having a rotatable dish, which dish is mounted in a stationary vessel, said stationary vessel having a rising inner surface contiguous to the periphery of said dish and curved upwardly therefrom to define a steadily rising surface from said dish, which comprises charging said granular material into said vessel and onto said rotatable dish while said rotatable dish is rotated at a predetermined speed, intermittently supplying a binding solution to said vessel by measuring the specific electro-resistance of a mass of said granular material by means of a detector including at least one electrode which is spaced from a portion of the rising inner surface of the vessel, feeding a signal indicative of the detected specific electro-resistance to a comparision circuit, comparing said signal from said detector with a reference value fed from a reference signal generator, said comparision circuit generating a control pulse only when said detected specific electro-resistance exceeds the reference value and continuing the generation of such control pulse during a period in which said detected specific electro-resistance is in excess of said reference value, said binding solution spraying being effected under a predetermined pressure onto the fluidized mass of said granular material by means of an electromagnetic valve opened by said control pulse during the duration of said control pulse, the electro-magnetic valve being closed to discontinue spraying when the detected specific electro-resistance is less than the reference value and no control pulse is generated from said comparision circuit, and feeding coating powder continuously throughout the coating operation onto the fluidized mass of said granular material within said vessel.
Claim 3
Dependent Claim 29 words
A process as claimed in claim 1, wherein the rate of continuous supply of the coating powder increases as the coating time passes in accordance with a predetermined program.
Claim 4
Dependent Claim 67 words
A process as claimed in claim 1, wherein said reference value is selected, in consideration of the rate of supply of the coating powder, such that the moisture content of said granular material being coated is a predetermined value within the range of 10 to 50% by weight relative to the total amount of the coating powder used to form each outermost layer on said granular material.
Claim 5
Dependent Claim 67 words
A process as claimed in claim 2, wherein said reference value is selected, in consideration of the rate of supply of the coating powder, such that the moisture content of said granular material being coated is a predetermined value within the range of 10 to 50% by weight relative to the total amount of the coating powder used to form each outermost layer on said granular material.
Claim 6
Dependent Claim 26 words
A process as claimed in claim 1, wherein said supply of the coating powder is initiated in response to the first generation of said control pulse.
Claim 7
Dependent Claim 31 words
A process as claimed in claim 1, further comprising a step of applying drying air continuously throughout the coating operation onto the fluidized mass of the granular material within said vessel.
Claim 8
Dependent Claim 31 words
A process as claimed in claim 2, further comprising a step of applying drying air continuously throughout the coating operation onto the fluidized mass of the granular material within said vessel.
Claim 9
Dependent Claim 31 words
A process as claimed in claim 3, further comprising a step of applying drying air continuously throughout the coating operation onto the fluidized mass of the granular material within said vessel.
Claim 10
Dependent Claim 31 words
A process as claimed in claim 4, further comprising a step of applying drying air continuously throughout the coating operation onto the fluidized mass of the granular material within said vessel.

References Cited (Backward Citations)

US2016920A Cited
US3141792A Cited
US3347701A Cited
US3711319A Cited
US3671296A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1980-07-04 1981-01-03 1981-07-05 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1984-07-04 1985-01-03 1985-07-05 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1988-07-04 1989-01-03 1989-07-05 $7700.00 Window Closed / Lapsed

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