Patent US4041180A successfully refreshed from Google Patents.
US4041180A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Introducing gases into fermentation liquids
Assignee: Brewing Patents Ltd
•
Filing: 1976-03-05
•
Granted: 1977-08-09
•
Expires: 1996-03-05
Abstract
Abstract The bubbling of poorly soluble gases into fermentation liquids either for the replenishment of dissolved oxygen or for removal of excess super-saturated CO 2 can lead to severe foaming problems, particularly in deep fermentation vessels. The present invention overcomes this problem by dissolving the gas in an aqueous medium, usually water, under superatmospheric conditions and injecting the gas solution into the fermentation liquid in controlled quantities under conditions such that the gas is either retained in solution in the fermentation liquid or, at most, the gas is released from solution in the form of microbubbles of much smaller size than can be obtained by passing gas through a porous diffuser. Microbubbles may be released from the gas solution by injecting the pressurized gas solution into the fermentation liquid under conditions of high shear rate.
Inventors
- 👤 Richard John Hugh Wilson
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-30 21:38
CPC Classifications
C; C12; C12C; C12C11/00; C12C11/003; C12M; C12M29/00; C12M29/14; C12M29/20; Y; Y10; Y10S; Y10S435/00; Y10S435/812
Claims Analysis
Total Claims: 12
Claim 1
Independent Claim
126 words
A method of oxygenating brewers' wort during fermentation which consists of introducing into said wort a solution of oxygen or air in an aqueous carrier liquid selected from the group consisting of water, brewers' wort and beer, said solution being introduced into said wort at a predetermined depth, at a higher pressure than the pressure at said predetermined depth and under conditions such that the oxygen or air is retained in solution in the wort, said solution being super-saturated with oxygen or air at the temperature and under the pressure of the wort at said predetermined depth, the volume of said oxygen or air solution introduced during a single fermentation being not more than about 5% of the bulk volume of said wort in said fermentor.
Claim 2
Independent Claim
126 words
A method of oxygenating brewers' wort during fermentation which consists of introducing into said wort a solution of oxygen or air in an aqueous carrier liquid selected from the group consisting of water, brewers' wort and beer, said solution being introduced into said wort at a predetermined depth, at a higher pressure than the pressure at said predetermined depth and under conditions such that the oxygen or air is retained in solution in the wort, said solution being super-saturated with oxygen or air at the temperature and under the pressure of the wort at said predetermined depth, the volume of said oxygen or air solution introduced during a single fermentation being not more than about 5% of the bulk volume of said wort in said fermentor.
Claim 3
Independent Claim
143 words
A method of degassing brewers' wort during fermentation or degassing fermented beer, said wort or beer being supersaturated with carbon dioxide, which method comprises 1. dissolving a gas selected from the group consisting of oxygen, nitrogen, carbon dioxide and a mixture thereof in an aqueous carrier liquid selected from the group consisting of water, brewers' wort and beer to form a solution which is saturated with said gas at a superatmospheric pressure, and 2. introducing said solution into said wort or beer at a predetermined depth, under conditions leading to a high degree of shear thereby causing said gas to be liberated from said supersaturated solution as a multitude of microbubbles, said multitude of microbubbles being characterized by a distinctive milky appearance, said solution becoming supersaturated with said gas under the temperature and pressure of said wort or beer at said predetermined depth.
Claim 4
Independent Claim
143 words
A method of degassing brewers' wort during fermentation or degassing fermented beer, said wort or beer being supersaturated with carbon dioxide, which method comprises 1. dissolving a gas selected from the group consisting of oxygen, nitrogen, carbon dioxide and a mixture thereof in an aqueous carrier liquid selected from the group consisting of water, brewers' wort and beer to form a solution which is saturated with said gas at a superatmospheric pressure, and 2. introducing said solution into said wort or beer at a predetermined depth, under conditions leading to a high degree of shear thereby causing said gas to be liberated from said supersaturated solution as a multitude of microbubbles, said multitude of microbubbles being characterized by a distinctive milky appearance, said solution becoming supersaturated with said gas under the temperature and pressure of said wort or beer at said predetermined depth.
Claim 5
Dependent Claim
16 words
A method according to claim 1, wherein said solution is a solution of oxygen in water.
Claim 6
Dependent Claim
41 words
A method according to claim 1, wherein said solution is mixed with a portion of said wort at a pressure higher than the pressure at said predetermined depth, and the resultant mixture is then introduced into the bulk of the wort.
Claim 7
Dependent Claim
51 words
A method according to claim 4, wherein a stream of the wort is withdrawn from the bulk of said wort, said wort stream is mixed with a stream of said solution, and a stream of the resultant mixture is then introduced into the bulk of said wort at said predetermined depth.
Claim 8
Dependent Claim
14 words
A method according to claim 1, wherein said wort is supersaturated with carbon dioxide.
Claim 9
Dependent Claim
37 words
A method according to claim 1, wherein said gas is oxygen and/or nitrogen, and said gas is dissolved in said carrier liquid under a pressure of at least 3 atmospheres and at a temperature below 25° C.
Claim 10
Dependent Claim
27 words
A method according to claim 7, wherein said gas is dissolved in said carrier liquid under a pressure of 5-10 atmospheres and a temperature of 2°-18° C.
Claim 11
Dependent Claim
26 words
A method according to claim 1, wherein said solution is injected intermittently into said wort or beer to control the number of nuclei-forming microbubbles generated therein.
Claim 12
Dependent Claim
32 words
A method according to claim 1, wherein the volume of said solution introduced into said wort or beer is not more than about 1% of the volume of said wort or beer.
References Cited (Backward Citations)
US3123475A
Cited
US3041250A
Cited
US3345179A
Cited
US3506460A
Cited
US3723255A
Cited
US3698913A
Cited
US3850753A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1980-08-08 | 1981-02-07 | 1981-08-09 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1984-08-08 | 1985-02-07 | 1985-08-09 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1988-08-08 | 1989-02-07 | 1989-08-09 | $7700.00 | Window Closed / Lapsed |