Patent US4308155A successfully refreshed from Google Patents.
US4308155A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Rubber or plastic magnet and magnetic powder for making the same
Assignee: TDK Corp
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Filing: 1979-10-29
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Granted: 1981-12-29
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Expires: 1999-10-29
Abstract
Abstract A rubber or plastic magnet of high magnetic properties is produced by incorporating a magnetoplumbite type magnetic powder into a rubber or thermoplastic or thermosetting matrix at a high concentration with a high degree of orientation of the magnetic particles. Such high concentration and orientation can be obtained by using a magnetoplumbite type magnetic powder having a compressed density in the range between 3.30 g/cm 3 and about 3.55 g/cm 3 and an average particle size of about 1.00 and 1.50μ, said particles being prepared by dry crushing process from coarse sintered particles and having predominantly single crystal structure.
Inventors
- 👤 Takeo Tada
- 👤 Katsuji Honda
- 👤 Masami Oguriyama
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-30 01:36
CPC Classifications
H; H01; H01F; H01F1/00; H01F1/01; H01F1/03; H01F1/032; H01F1/10; H01F1/11; H01F1/113; H01F1/117
Claims Analysis
Total Claims: 14
Claim 1
Independent Claim
180 words
A process of producing a magnetic powder for use in a plastic or rubber magnet wherein said powder is filled in a plastic or rubber matrix and magnetically oriented comprising: (a) firing a starting composition capable of forming when fired a ferrite selected from the group consisting of barium ferrite, strontium ferrite and lead plumbite ferrite at a temperature above 1200° C. to produce a sintered body of magnetic material; (b) coarse-crushing said sintered body to obtain coarse particles; (c) pulverizing said coarse particles together with about 0.1% by weight of about 10% by weight based on the weight of said coarse particles of a lower alcohol having three or less carbon atoms until a fine powder is obtained, said fine powder having an average particle size in the range between about 1.00μ and about 1.50μ measured with a Fisher Sub-Sieve Sizer and having a compressed density in the range of about 3.30 g/cm 3 and about 3.55 g/cm 3 when compressed under a pressure of 1 ton/cm 2 ; and (d) annealing said fine powder at an elevated temperature.
Claim 2
Dependent Claim
180 words
A process of producing a magnetic powder for use in a plastic or rubber magnet wherein said powder is filled in a plastic or rubber matrix and magnetically oriented comprising: (a) firing a starting composition capable of forming when fired a ferrite selected from the group consisting of barium ferrite, strontium ferrite and lead plumbite ferrite at a temperature above 1200° C. to produce a sintered body of magnetic material; (b) coarse-crushing said sintered body to obtain coarse particles; (c) pulverizing said coarse particles together with about 0.1% by weight of about 10% by weight based on the weight of said coarse particles of a lower alcohol having three or less carbon atoms until a fine powder is obtained, said fine powder having an average particle size in the range between about 1.00μ and about 1.50μ measured with a Fisher Sub-Sieve Sizer and having a compressed density in the range of about 3.30 g/cm 3 and about 3.55 g/cm 3 when compressed under a pressure of 1 ton/cm 2 ; and (d) annealing said fine powder at an elevated temperature.
Claim 3
Dependent Claim
12 words
A process according to claim 1 wherein said ferrite is barium ferrite.
Claim 4
Dependent Claim
16 words
A process according to claim 1 wherein said coarse particles are pulverized in a ball mill.
Claim 5
Dependent Claim
16 words
A process according to claim 1 wherein said coarse particles are pulverized in a vibration mill.
Claim 6
Dependent Claim
27 words
A process according to claim 1 wherein said alcohol is selected from the group consisting of methanol, ethanol, propanol, ispropanol, mixtures thereof, and ethanol denatured with methanol.
Claim 7
Dependent Claim
181 words
A magnetic powder for use in a plastic or rubber magnet wherein said powder is filled in a plastic or rubber matrix and magnetically oriented, said powder being made according to the following steps: (a) firing a starting composition capable of forming when fired a ferrite selected from the group consisting of barium ferrite, strontium ferrite and lead plumbite ferrite at a temperature above 1200° C. to produce a sintered body of magnetic material; (b) coarse-crushing said sintered body to obtain coarse particles; (c) pulverizing said coarse particles together with about 0.1% by weight to about 10% by weight based on the weight of said coarse particles of a lower alcohol having three or less carbon atoms until a fine powder is obtained, said fine powder having an average particle size in the range between 1.00μ and 1.50μ measured with a Fisher Sub-Sieve Sizer having a compressed density in the range of about 3.30 g/cm 3 and about 3.55 g/cm 3 when compressed under a pressure of 1 ton/cm 2 ; and (d) annealing said fine powder at an elevated temperature.
Claim 8
Dependent Claim
181 words
A magnetic powder for use in a plastic or rubber magnet wherein said powder is filled in a plastic or rubber matrix and magnetically oriented, said powder being made according to the following steps: (a) firing a starting composition capable of forming when fired a ferrite selected from the group consisting of barium ferrite, strontium ferrite and lead plumbite ferrite at a temperature above 1200° C. to produce a sintered body of magnetic material; (b) coarse-crushing said sintered body to obtain coarse particles; (c) pulverizing said coarse particles together with about 0.1% by weight to about 10% by weight based on the weight of said coarse particles of a lower alcohol having three or less carbon atoms until a fine powder is obtained, said fine powder having an average particle size in the range between 1.00μ and 1.50μ measured with a Fisher Sub-Sieve Sizer having a compressed density in the range of about 3.30 g/cm 3 and about 3.55 g/cm 3 when compressed under a pressure of 1 ton/cm 2 ; and (d) annealing said fine powder at an elevated temperature.
Claim 9
Dependent Claim
13 words
A magnetic powder according to claim 6 wherein said ferrite is barium ferrite.
Claim 10
Dependent Claim
17 words
A magnetic powder according to claim 6 wherein said powder is comprised predominantly of single crystal particles.
Claim 11
Dependent Claim
186 words
A plastic or rubber magnet comprising a magnetic powder uniformly dispersed in a plastic or rubber matrix, said powder being magnetically or mechanically oriented in said matrix, said powder being made according to the following steps: (a) firing a starting composition capable of forming when fired a ferrite selected from the group consisting of barium ferrite, strontium ferrite and lead plumbite ferrite at a temperature above 1200° C. to produce a sintered body of magnetic material; (b) coarse-crushing said sintered body to obtain coarse particles; (c) pulverizing said coarse particles together with about 0.1% by weight to about 10% by weight based on the weight of said coarse particles of a lower alcohol having three or less carbon atoms until a fine powder is obtained, said fine powder having an average particle size in the range between about 1.00μ and about 1.50μ measured with a Fisher Sub-Sieve Sizer and having a compressed density in the range of about 3.30 g/cm 3 and about 3.55 g/cm 3 when compressed under a pressure of 1 ton/cm 2 ; and (d) annealing said fine powder at an elevated temperature.
Claim 12
Dependent Claim
186 words
A plastic or rubber magnet comprising a magnetic powder uniformly dispersed in a plastic or rubber matrix, said powder being magnetically or mechanically oriented in said matrix, said powder being made according to the following steps: (a) firing a starting composition capable of forming when fired a ferrite selected from the group consisting of barium ferrite, strontium ferrite and lead plumbite ferrite at a temperature above 1200° C. to produce a sintered body of magnetic material; (b) coarse-crushing said sintered body to obtain coarse particles; (c) pulverizing said coarse particles together with about 0.1% by weight to about 10% by weight based on the weight of said coarse particles of a lower alcohol having three or less carbon atoms until a fine powder is obtained, said fine powder having an average particle size in the range between about 1.00μ and about 1.50μ measured with a Fisher Sub-Sieve Sizer and having a compressed density in the range of about 3.30 g/cm 3 and about 3.55 g/cm 3 when compressed under a pressure of 1 ton/cm 2 ; and (d) annealing said fine powder at an elevated temperature.
Claim 13
Dependent Claim
12 words
A magnet according to claim 9 wherein said ferrite is barium ferrite.
Claim 14
Dependent Claim
22 words
A magnet according to claim 9 wherein said plastic matrix is selected from the group consisting of thermoplastic materials and thermosetting materials.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1984-12-28 | 1985-06-29 | 1985-12-29 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1988-12-28 | 1989-06-29 | 1989-12-29 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1992-12-28 | 1993-06-29 | 1993-12-29 | $7700.00 | Window Closed / Lapsed |