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Process for making pyridinethione salts

Assignee: Procter and Gamble Co
•
Filing: 1980-02-07
•
Granted: 1982-04-06
•
Expires: 2000-02-07
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Abstract

Abstract A process for producing heavy metal, magnesium or aluminum pyridinethione salt crystals involving reacting a water soluble salt of the desired metal with a water soluble pyridinethione salt or pyridinethione itself in an aqueous surfactant medium.

Inventors

  • 👤 Raymond E. Bolich, Jr.
  • 👤 Steven A. Shaya
  • 👤 Christian Steuri

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-06 23:19
CPC Classifications
C; C07; C07D; C07D213/00; C07D213/02; C07D213/89; A; A61; A61K; A61K8/00; A61K8/02; A61K8/18; A61K8/30; A61K8/49; A61K8/4906; A61K8/4933; A61Q; A61Q5/00; A61Q5/006; A61Q5/02; A61K2800/00; A61K2800/40; A61K2800/41; A61K2800/412

Claims Analysis

Total Claims: 12
Claim 1
Independent Claim 46 words
A process for making heavy metal, magnesium or aluminum N-hydroxy pyridinethione salts comprising reacting 1-hydroxy-2-pyridinethione or a water soluble salt thereof with a water soluble heavy metal, magnesium or aluminum salt in an aqueous surfactant medium, wherein the reaction temperature is at least about 20° C.
Claim 2
Dependent Claim 46 words
A process for making heavy metal, magnesium or aluminum N-hydroxy pyridinethione salts comprising reacting 1-hydroxy-2-pyridinethione or a water soluble salt thereof with a water soluble heavy metal, magnesium or aluminum salt in an aqueous surfactant medium, wherein the reaction temperature is at least about 20° C.
Claim 3
Dependent Claim 33 words
A process according to claim 1 wherein the pyridinethione compound is an alkali metal pyridinethione salt and the concentration of surfactant in the total reaction mixture is from about 1% to about 24%.
Claim 4
Dependent Claim 39 words
A process according to claim 2 wherein the metal salt is a heavy metal salt selected from the group consisting of zinc, tin, cadmium and zirconium salts and is present in an amount sufficient to provide a stoichiometric excess.
Claim 5
Dependent Claim 11 words
A process according to claim 3 wherein the surfactant is anionic.
Claim 6
Dependent Claim 15 words
A process according to claim 4 wherein the heavy metal salt is a zinc salt.
Claim 7
Dependent Claim 19 words
A process according to claim 5 wherein the reaction temperature is from about 60° C. to about 100° C.
Claim 8
Dependent Claim 18 words
A process according to claim 6 wherein the concentration of surfactant is from about 1% to about 8%.
Claim 9
Dependent Claim 15 words
A process according to claim 7 wherein the alkali metal pyridinetione salt is sodium pyridinethione.
Claim 10
Dependent Claim 13 words
A process according to claim 8 wherein the zinc salt is zinc sulfate.
Claim 11
Dependent Claim 14 words
A process according to claim 9 wherein the anionic surfactant is an alkyl sulfate.
Claim 12
Dependent Claim 14 words
A process according to claim 10 wherein the alkyl sulfate is sodium alkyl sulfate.

References Cited (Backward Citations)

US2286847A Cited
US2809971A Cited
US3037849A Cited
US3590035A Cited
US3773770A Cited
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US3836531A Cited
US4089945A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1985-04-05 1985-10-05 1986-04-06 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1989-04-05 1989-10-05 1990-04-06 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1993-04-05 1993-10-05 1994-04-06 $7700.00 Window Closed / Lapsed

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