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US4459762A Expired / Lapsed US ⏱️ 0.0 years remaining

Solvent dewatering coal

Assignee: SMC MINING Co C/O ZEIGLER COAL HOLDING
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Filing: 1982-11-18
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Granted: 1984-07-17
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Expires: 2002-11-18
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Abstract

Abstract Drying of wet coal is facilitated by the addition of a nonaqueous solvent, such as acetone, to the coal followed by application of heat to remove both solvent and water from the coal. The coal may be further upgraded by briquetting or pelletizing fine coal particles with waxes and resins extracted from the coal, or the waxes and resins may be left on the coal to reduce the tendency of the coal to reabsorb water. In addition, minerals such as sodium and potassium salts may be removed from the coal to reduce slagging and fouling behavior of the coal.

Inventors

  • 👤 Donald E. Hardesty
  • 👤 Herbert F. Buchholz

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-30 06:37
CPC Classifications
C; C10; C10L; C10L9/00; C10G; C10G1/00

Claims Analysis

Total Claims: 23
Claim 1
Independent Claim 93 words
A process for drying coal containing water and including fine coal particles, comprising, mixing a nonaqueous solvent of acetone and naphtha with the coal, the solvent having a lower heat of vaporization than the water and being miscible with the water and functioning to extract organics from the coal; applying heat to the coal sufficient to vaporize at least part of the solvent and water substantially free of the extracted organics; recovering the solvent from the vaporized solvent and water; and forming the fine coal particles and extracted organics into larger coal particles.
Claim 2
Dependent Claim 93 words
A process for drying coal containing water and including fine coal particles, comprising, mixing a nonaqueous solvent of acetone and naphtha with the coal, the solvent having a lower heat of vaporization than the water and being miscible with the water and functioning to extract organics from the coal; applying heat to the coal sufficient to vaporize at least part of the solvent and water substantially free of the extracted organics; recovering the solvent from the vaporized solvent and water; and forming the fine coal particles and extracted organics into larger coal particles.
Claim 3
Dependent Claim 13 words
The process of claim 1 wherein the extracted organics are waxes and resins.
Claim 4
Dependent Claim 18 words
The process of claim 2 wherein the fine coal particles are briquetted or pelletized with waxes and resins.
Claim 5
Dependent Claim 60 words
A process for water-proofing coal, comprising, mixing a nonaqueous solvent of acetone containing naphtha with the coal, the solvent functioning to extract organics from the coal; applying heat to the coal sufficient to vaporize at least part of the solvent which is substantially free of the extracted organics which remain as a coating on the coal; and recovering the solvent.
Claim 6
Dependent Claim 60 words
A process for water-proofing coal, comprising, mixing a nonaqueous solvent of acetone containing naphtha with the coal, the solvent functioning to extract organics from the coal; applying heat to the coal sufficient to vaporize at least part of the solvent which is substantially free of the extracted organics which remain as a coating on the coal; and recovering the solvent.
Claim 7
Dependent Claim 13 words
The process of claim 4 wherein the extracted organics are waxes and resins.
Claim 8
Dependent Claim 42 words
A process for reducing slagging and fouling behavior of coal by extracting minerals therefrom, comprising, mixing a nonaqueous solvent of tetrahydrofuran with the coal, the solvent functioning to extract minerals from the coal, and separating the solvent and minerals from the coal.
Claim 9
Dependent Claim 42 words
A process for reducing slagging and fouling behavior of coal by extracting minerals therefrom, comprising, mixing a nonaqueous solvent of tetrahydrofuran with the coal, the solvent functioning to extract minerals from the coal, and separating the solvent and minerals from the coal.
Claim 10
Dependent Claim 24 words
The process of claim 6 wherein the solvent is evaporated from the coal and the minerals are separated from the coal in a cyclone.
Claim 11
Dependent Claim 13 words
The process of claim 6 wherein the minerals are sodium and potassium salts.
Claim 12
Dependent Claim 115 words
A process for drying coal containing water and producing wax and resin from the coal, comprising mixing a nonaqueous solvent of acetone containing naphtha with the coal, the solvent having a lower heat of vaporization than the water and being miscible with the water and functioning to extract wax and resin from the coal; separating at least part of the solvent from the coal, the solvent containing wax and resin, and recovering the solvent from the wax and resin; applying heat to the coal to vaporize at least part of the solvent remaining with the coal and to vaporize at least part of the water; and recovering the solvent from the vaporized solvent and water.
Claim 13
Dependent Claim 115 words
A process for drying coal containing water and producing wax and resin from the coal, comprising mixing a nonaqueous solvent of acetone containing naphtha with the coal, the solvent having a lower heat of vaporization than the water and being miscible with the water and functioning to extract wax and resin from the coal; separating at least part of the solvent from the coal, the solvent containing wax and resin, and recovering the solvent from the wax and resin; applying heat to the coal to vaporize at least part of the solvent remaining with the coal and to vaporize at least part of the water; and recovering the solvent from the vaporized solvent and water.
Claim 14
Dependent Claim 31 words
A process for drying coal containing water, comprising, mixing acetone containing naptha with the coal; applying heat to the coal sufficient to vaporize at least part of the acetone and naptha.
Claim 15
Dependent Claim 31 words
A process for drying coal containing water, comprising, mixing acetone containing naptha with the coal; applying heat to the coal sufficient to vaporize at least part of the acetone and naptha.
Claim 16
Dependent Claim 39 words
A process for drying coal containing water, comprising, mixing tetrahydrofuran with the coal; applying heat to the coal sufficient to vaporize at least part of the tetrahydrofuran and water; and recovering the tetrahydrofuran from the vaporized tetrahydrofuran and water.
Claim 17
Dependent Claim 39 words
A process for drying coal containing water, comprising, mixing tetrahydrofuran with the coal; applying heat to the coal sufficient to vaporize at least part of the tetrahydrofuran and water; and recovering the tetrahydrofuran from the vaporized tetrahydrofuran and water.
Claim 18
Dependent Claim 73 words
A process for reducing oxidation of coal in order to enhance subsequent liquefaction of the coal, comprising, mixing a nonaqueous solvent of acetone containing naphtha with the coal, the solvent functioning to extract organics from the coal; applying heat to the coal sufficient to vaporize at least part of the solvent which is substantially free of the extracted organics which remain as a coating on the coal; and subjecting the coal to liquefaction.
Claim 19
Dependent Claim 73 words
A process for reducing oxidation of coal in order to enhance subsequent liquefaction of the coal, comprising, mixing a nonaqueous solvent of acetone containing naphtha with the coal, the solvent functioning to extract organics from the coal; applying heat to the coal sufficient to vaporize at least part of the solvent which is substantially free of the extracted organics which remain as a coating on the coal; and subjecting the coal to liquefaction.
Claim 20
Dependent Claim 71 words
A process for reducing oxidation of coal in order to enhance subsequent liquefaction of the coal, comprising, mixing a non-aqueous solvent of tetrahydrofuran with the coal, the solvent functioning to extract organics from the coal; applying heat to the coal sufficient to vaporize at least part of the solvent which is substantially free of the extracted organics which remain as a coating on the coal; and subjecting the coal to liquefaction.
Claim 21
Dependent Claim 71 words
A process for reducing oxidation of coal in order to enhance subsequent liquefaction of the coal, comprising, mixing a non-aqueous solvent of tetrahydrofuran with the coal, the solvent functioning to extract organics from the coal; applying heat to the coal sufficient to vaporize at least part of the solvent which is substantially free of the extracted organics which remain as a coating on the coal; and subjecting the coal to liquefaction.
Claim 22
Dependent Claim 113 words
A process for drying coal containing water and producing wax and resin from the coal, comprising mixing a nonaqueous solvent of tetrahydrofuran with the coal, the solvent having a lower heat of vaporization than the water and being miscible with the water and functioning to extract wax and resin from the coal; separating at least part of the solvent from the coal, the solvent containing wax and resin, and recovering the solvent from the wax and resin; applying heat to the coal to vaporize at least part of the solvent remaining with the coal and to vaporize at least part of the water; and recovering the solvent from the vaporized solvent and water.
Claim 23
Dependent Claim 113 words
A process for drying coal containing water and producing wax and resin from the coal, comprising mixing a nonaqueous solvent of tetrahydrofuran with the coal, the solvent having a lower heat of vaporization than the water and being miscible with the water and functioning to extract wax and resin from the coal; separating at least part of the solvent from the coal, the solvent containing wax and resin, and recovering the solvent from the wax and resin; applying heat to the coal to vaporize at least part of the solvent remaining with the coal and to vaporize at least part of the water; and recovering the solvent from the vaporized solvent and water.

References Cited (Backward Citations)

US3327402A Cited
US3953927A Cited
US4235603A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1987-07-17 1988-01-16 1988-07-17 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1991-07-17 1992-01-16 1992-07-17 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1995-07-17 1996-01-16 1996-07-17 $7700.00 Window Closed / Lapsed

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