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US4464940A Expired / Lapsed US ⏱️ 0.0 years remaining

Sampler for a gas chromatograph

Assignee: PE Manufacturing GmbH
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Filing: 1982-07-12
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Granted: 1984-08-14
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Expires: 2002-07-12
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Abstract

Abstract According to the head space method, samples are supplied from sealed sample vessels by means of a needle. A change-over valve, an optionally higher or reduced carrier gas pressure is applied to a carrier gas conduit comprising a shut-off valve and terminating between the needle and entrance of the separating column. This enables a defined sample feeding and analysis by an optimum carrier gas pressure even with volatile samples.

Inventors

  • 👤 Peter Pospisil

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-02 13:53
CPC Classifications
G; G01; G01N; G01N30/00; G01N30/02; G01N30/04; G01N30/24

Claims Analysis

Total Claims: 3
Claim 1
Independent Claim 152 words
A head space sampler for a gas chromatograph, said sampler comprising: a needle connected to the entrance of a gas chromatographic separating column by means of a connecting passage; a carrier gas conduit terminating at said connecting passage between said needle and said separating column; means for generating a first higher carrier gas pressure at a first carrier gas connection; means for generating a second carrier gas pressure, which pressure is comparatively lower that said said first pressure, at a second carrier gas connection; a change-over valve, said change-over valve having said first and second carrier gas connection as inputs and said carrier gas conduit as an output; a controllable shut-off valve disposed in said carrier gas conduit between said change-over valve and said termination of said carrier gas conduit at said connecting passage; and means for piercing said needle through a septum of a sample vessel into the head space thereof.
Claim 2
Dependent Claim 152 words
A head space sampler for a gas chromatograph, said sampler comprising: a needle connected to the entrance of a gas chromatographic separating column by means of a connecting passage; a carrier gas conduit terminating at said connecting passage between said needle and said separating column; means for generating a first higher carrier gas pressure at a first carrier gas connection; means for generating a second carrier gas pressure, which pressure is comparatively lower that said said first pressure, at a second carrier gas connection; a change-over valve, said change-over valve having said first and second carrier gas connection as inputs and said carrier gas conduit as an output; a controllable shut-off valve disposed in said carrier gas conduit between said change-over valve and said termination of said carrier gas conduit at said connecting passage; and means for piercing said needle through a septum of a sample vessel into the head space thereof.
Claim 3
Dependent Claim 18 words
Sampler as claimed in claim 1 wherein said change-over valve and said controllable shut-off valve are solenoid valves.

References Cited (Backward Citations)

US3668834A Cited
US4237733A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1987-08-14 1988-02-13 1988-08-14 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1991-08-14 1992-02-13 1992-08-14 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1995-08-14 1996-02-13 1996-08-14 $7700.00 Window Closed / Lapsed

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