Patent US4496697A successfully refreshed from Google Patents.
US4496697A
Expired / Lapsed
US
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Automatic process control system for curing polymeric material
Assignee: Lockheed Martin Corp
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Filing: 1982-08-24
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Granted: 1985-01-29
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Expires: 2002-08-24
Abstract
Abstract This invention is directed to a method of automatically controlling curing of a thermosetting polymeric material. The method comprises the steps of (a) applying heat to the polymeric material to initiate curing; (b) measuring a selected characteristic of the polymeric material at various times during the cure cycle thereof; (c) generating a set of signals corresponding to the measurements made; (d) determining from the signals the optimum time for applying pressure to the polymeric material; and (e) automatically applying pressure to the polymeric material at the optimum time, in a closed-loop system. The selected characteristic measured may be the capacitance or the dissipation of the polymeric material. In general, the pressure is automatically applied immediately after the minimum capacitance level is reached but before hardening of the polymeric material.
Inventors
- 👤 Andrew Zsolnay
- 👤 Kelly M. Perkins
- 👤 Leiv H. Blad
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-01 21:55
CPC Classifications
G; G01; G01N; G01N33/00; G01N33/44; G01N33/442; B; B29; B29C; B29C35/00; B29C35/02; B29C35/0288; G01N27/00; G01N27/02; G01N27/22; G01N27/221; G01N2203/00; G01N2203/0058; G01N2203/0092
Claims Analysis
Total Claims: 10
Claim 1
Independent Claim
94 words
An improved method of automatically controlling curing of a thermosetting polymeric material comprising: (a) applying heat to the polymeric material to initiate curing; (b) measuring a selected characteristic of the polymeric material at various times during the curing thereof; (c) generating a set of signals corresponding to the measurements made; (d) determining from said signals the optimum time after the initiation of curing but before the polymeric material has hardened for applying pressure to the polymeric material; and (e) automatically applying pressure to the polymeric material at said optimum time, in a closed-loop system.
Claim 2
Dependent Claim
94 words
An improved method of automatically controlling curing of a thermosetting polymeric material comprising: (a) applying heat to the polymeric material to initiate curing; (b) measuring a selected characteristic of the polymeric material at various times during the curing thereof; (c) generating a set of signals corresponding to the measurements made; (d) determining from said signals the optimum time after the initiation of curing but before the polymeric material has hardened for applying pressure to the polymeric material; and (e) automatically applying pressure to the polymeric material at said optimum time, in a closed-loop system.
Claim 3
Dependent Claim
18 words
The improved method of claim 1 wherein the selected characteristic measured is the capacitance of the polymeric material.
Claim 4
Dependent Claim
18 words
The improved method of claim 1 wherein the selected characteristic measured is the dissipation of the polymeric material.
Claim 5
Dependent Claim
20 words
The improved method of claim 2 wherein the pressure is automatically applied immediately after the minimum capacitance level is reached.
Claim 6
Dependent Claim
83 words
An improved method of curing a polymeric material, said method comprising: (a) initiating curing of a thermosetting polymeric material at a preselected temperature; (b) at least periodically during said curing, monitoring the cure state of said polymeric material by measuring a dielectric characteristic of said polymeric material which varies with the state of cure of said polymeric material; and (c) adjusting said temperature to control the rate of said curing of said polymeric material in response to the information provided by said measurement.
Claim 7
Dependent Claim
83 words
An improved method of curing a polymeric material, said method comprising: (a) initiating curing of a thermosetting polymeric material at a preselected temperature; (b) at least periodically during said curing, monitoring the cure state of said polymeric material by measuring a dielectric characteristic of said polymeric material which varies with the state of cure of said polymeric material; and (c) adjusting said temperature to control the rate of said curing of said polymeric material in response to the information provided by said measurement.
Claim 8
Dependent Claim
31 words
The improved method of claim 5 wherein said polymeric material undergoes a condensation-type reaction during said curing and wherein the capacitance of said polymeric material is measured to provide said information.
Claim 9
Dependent Claim
43 words
The improved method of claim 6 wherein said polymeric material is disposed in a laminate and wherein pressure is applied during said curing when the minimum level of said capacitance is reached in order to provide a void-free laminate having improved mechanical properties.
Claim 10
Dependent Claim
19 words
The improved method of claim 5 wherein said adjusting of said temperature in response to said information is automatic.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1988-01-29 | 1988-07-30 | 1989-01-29 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1992-01-29 | 1992-07-30 | 1993-01-29 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1996-01-29 | 1996-07-30 | 1997-01-29 | $7700.00 | Window Closed / Lapsed |