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US5158644A
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Reactor chamber self-cleaning process
Assignee: Applied Materials Inc
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Filing: 1991-10-10
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Granted: 1992-10-27
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Expires: 2011-10-10
Abstract
Abstract A reactor chamber self-cleaning process is disclosed which uses a fluorocarbon-containing gas and, preferably, C 2 F 6 in combination with oxygen. The two-step process involves, first, a chamber-wide etch at relatively low pressure and with relatively large separation between the gas inlet manifold and the wafer supports which are the RF electrodes and, second, a local etch step which uses a relatively high chamber pressure and smaller electrode spacing, to complete the cleaning of the RF electrodes.
Inventors
- 👤 David Cheung
- 👤 Peter Keswick
- 👤 Jerry Wong
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-01 04:16
CPC Classifications
C; C23; C23C; C23C16/00; C23C16/44; C23C16/4401; C23C16/4405; C23C16/22; C23C16/30; C23C16/40; C23C16/401; C23C16/402; C23C16/455; C23C16/45519; C23C16/45521; C23C16/45563; C23C16/45565; C23C16/50; C23C16/505; C23C16/509; C23C16/5096; C23C16/54; H; H01; H01J; H01J37/00; H01J37/32; H01J37/32009; H01J37/32082; H01J37/32431; H01J37/3244; H01J37/32798; H01J37/32853; H01J37/32862; H10; H10P; H10P14/00; H10P14/60; H10P14/63; H10P14/6326; H10P14/6328; H10P72/00; H10P72/04; H10P72/0402; H10P72/0418; H10P72/0421; Y; Y02; Y02C; Y02C20/00; Y02C20/30; Y02P; Y02P70/00; Y02P70/50; Y10; Y10S; Y10S438/00; Y10S438/905
Claims Analysis
Total Claims: 16
Claim 1
Independent Claim
119 words
A process for self-cleaning a vacuum processing reactor chamber having electrodes in the form of a gas inlet manifold and a wafer support electrode of variable spacing therebetween, comprising: in a first, extended etch step, supplying a fluorocarbon-containing gas into the chamber at a first pressure and a first electrode spacing, with selected power applied between the electrodes, for generating an etching plasma substantially throughout the chamber; and, in a second, local etch step, supplying the fluorocarbon-containing gas into the chamber at a second pressure greater than the first pressure, and a second electrode spacing which is less than the first electrode spacing, with selected power applied between the electrodes, for generating a local etching plasma between the electrodes.
Claim 2
Dependent Claim
119 words
A process for self-cleaning a vacuum processing reactor chamber having electrodes in the form of a gas inlet manifold and a wafer support electrode of variable spacing therebetween, comprising: in a first, extended etch step, supplying a fluorocarbon-containing gas into the chamber at a first pressure and a first electrode spacing, with selected power applied between the electrodes, for generating an etching plasma substantially throughout the chamber; and, in a second, local etch step, supplying the fluorocarbon-containing gas into the chamber at a second pressure greater than the first pressure, and a second electrode spacing which is less than the first electrode spacing, with selected power applied between the electrodes, for generating a local etching plasma between the electrodes.
Claim 3
Dependent Claim
48 words
The process of claim 1, wherein the first, extended etch step uses the gases C 2 F 6 and O 2 at a C 2 F 6 :O 2 flow rate ratio of (0.75-1.30):1, electrode spacing 750-1,000 mils, pressure 0.8-2 torr and power density 2.7-5.6 watts/cm 2 .
Claim 4
Dependent Claim
48 words
The process of claim 1, wherein the second, local etch step uses the gases C 2 F 6 and O 2 at a C 2 F 6 :O 2 flow rate ratio of (0.85-1):1, electrode spacing 180-350 mils, pressure 6-13 torr and power density 2.7-5.6 watts/cm 2 .
Claim 5
Dependent Claim
168 words
A process for self-cleaning a vacuum processing reactor chamber having RF electrodes in the form of a gas inlet manifold and a wafer support electrode of variable spacing therebetween, comprising: in a first, extended etch step supplying the gases C 2 F 6 and O 2 into the chamber at a C 2 F 6 :O 2 flow rate ratio of approximately (0.75-1.30):1, at a chamber pressure of approximately 0.8-2 torr and an electrode spacing of approximately 750-1,000 mils, with RF power density of approximately 2.7-5.6 watts/cm 2 applied between the electrodes for generating an etching plasma substantially throughout the chamber; and, in a second, local etch step, increasing the chamber pressure to a value of approximately 6-13 torr, decreasing the electrode spacing to a value of approximately 180-350 mils with selected RF power density of approximately 2.7-5.6 watts/cm 2 applied between the electrodes and wherein the C 2 F 6 :O 2 flow rate ratio is approximately (0.85-1):1, for generating a local etching plasma between the electrodes.
Claim 6
Dependent Claim
168 words
A process for self-cleaning a vacuum processing reactor chamber having RF electrodes in the form of a gas inlet manifold and a wafer support electrode of variable spacing therebetween, comprising: in a first, extended etch step supplying the gases C 2 F 6 and O 2 into the chamber at a C 2 F 6 :O 2 flow rate ratio of approximately (0.75-1.30):1, at a chamber pressure of approximately 0.8-2 torr and an electrode spacing of approximately 750-1,000 mils, with RF power density of approximately 2.7-5.6 watts/cm 2 applied between the electrodes for generating an etching plasma substantially throughout the chamber; and, in a second, local etch step, increasing the chamber pressure to a value of approximately 6-13 torr, decreasing the electrode spacing to a value of approximately 180-350 mils with selected RF power density of approximately 2.7-5.6 watts/cm 2 applied between the electrodes and wherein the C 2 F 6 :O 2 flow rate ratio is approximately (0.85-1):1, for generating a local etching plasma between the electrodes.
Claim 7
Dependent Claim
44 words
The process of claim 1, wherein the first, extended etch step uses C 2 F 6 flow rate of about 300-600 sccm, O 2 flow rate about 400-800 sccm, pressure about 0.8-2 torr, electrode spacing about 1,000 mils and RF power about 500-750 watts.
Claim 8
Dependent Claim
28 words
The process of claim 5, wherein the C 2 F 6 :O 2 flow rate ratio is 0.75:1 and the RF power density is 3.8-3.9 watts/cm 2 .
Claim 9
Dependent Claim
45 words
The process of claim 1, wherein the second, extended etch step uses a C 2 F 6 flow rate of about 600-800 sccm, O 2 flow rate about 700-900 sccm, pressure about 6-13 torr, electrode spacing about 180-300 mils and RF power about 500-750 watts.
Claim 10
Dependent Claim
29 words
The process of claim 7, wherein the C 2 F 6 :O 2 flow rate ratio is 0.85:1 and the RF power density is about 3.8-3.9 watts/cm 2 .
Claim 11
Dependent Claim
159 words
A process for self-cleaning a vacuum processing reactor chamber having RF electrodes in the form of a gas inlet manifold and a wafer support electrode of variable spacing therebetween, comprising: in a first, extended etch step supplying the gases C 2 F 6 and O 2 into the chamber at respective flow rates 300-600 sccm and 400-800 sccm, at a chamber pressure of approximately 0.8-2 torr, electrode spacing of approximately 1,000 mils, with RF power density of approximately 2.7-5.6 watts/cm 2 applied between the electrodes, for generating an etching plasma substantially throughout the chamber; and, in a second, local etch step, increasing the chamber pressure to approximately 6-13 torr, decreasing the electrode spacing to approximately 80-300 mils with selected RF power of approximately 2.7-5.6 watts/cm 2 applied between the electrodes and wherein the C 2 F 6 and O 2 flow rates are approximately 600-800 sccm and 700-900 sccm, respectively, for generating a local etching plasma between the electrodes.
Claim 12
Dependent Claim
159 words
A process for self-cleaning a vacuum processing reactor chamber having RF electrodes in the form of a gas inlet manifold and a wafer support electrode of variable spacing therebetween, comprising: in a first, extended etch step supplying the gases C 2 F 6 and O 2 into the chamber at respective flow rates 300-600 sccm and 400-800 sccm, at a chamber pressure of approximately 0.8-2 torr, electrode spacing of approximately 1,000 mils, with RF power density of approximately 2.7-5.6 watts/cm 2 applied between the electrodes, for generating an etching plasma substantially throughout the chamber; and, in a second, local etch step, increasing the chamber pressure to approximately 6-13 torr, decreasing the electrode spacing to approximately 80-300 mils with selected RF power of approximately 2.7-5.6 watts/cm 2 applied between the electrodes and wherein the C 2 F 6 and O 2 flow rates are approximately 600-800 sccm and 700-900 sccm, respectively, for generating a local etching plasma between the electrodes.
Claim 13
Dependent Claim
56 words
The process of claim 9, wherein during the first, extended etch step, the C 2 F 6 :O 2 flow rate ratio is 0.75:1, during the second, local etch step, the C 2 F 6 :O 2 flow rate ratio is 0.85:1, and during both steps the RF power density is about 3.8-3.9 watts/cm 2 .
Claim 14
Dependent Claim
152 words
A process for depositing coatings on semiconductor wafers in a vacuum reactor chamber having a gas inlet manifold electrode and a wafer support electrode of variable spacing therebetween, and for self-cleaning the chamber, comprising: repetitively depositing coatings on one or more wafers in the chamber; and applying a process for self-cleaning the internal chamber surfaces, comprising: in a first, extended etch step, supplying a fluorocarbon-containing gas into the chamber at a first chamber pressure and a first electrode spacing with selected RF power applied between the electrodes, for generating an etching plasma substantially throughout the chamber; and, in a second, local etch step, increasing the chamber pressure to a second value which is greater than the first chamber pressure, and decreasing the electrode spacing to a second value which is less than the first electrode spacing with selected power applied between the electrodes, for generating a local etching plasma between the electrodes.
Claim 15
Dependent Claim
152 words
A process for depositing coatings on semiconductor wafers in a vacuum reactor chamber having a gas inlet manifold electrode and a wafer support electrode of variable spacing therebetween, and for self-cleaning the chamber, comprising: repetitively depositing coatings on one or more wafers in the chamber; and applying a process for self-cleaning the internal chamber surfaces, comprising: in a first, extended etch step, supplying a fluorocarbon-containing gas into the chamber at a first chamber pressure and a first electrode spacing with selected RF power applied between the electrodes, for generating an etching plasma substantially throughout the chamber; and, in a second, local etch step, increasing the chamber pressure to a second value which is greater than the first chamber pressure, and decreasing the electrode spacing to a second value which is less than the first electrode spacing with selected power applied between the electrodes, for generating a local etching plasma between the electrodes.
Claim 16
Dependent Claim
80 words
The process of claim 11, wherein the first, extended etch step uses C 2 F 6 and O 2 at a flow rate ratio of about (0.75-1.30):1, electrode spacing 750-1,000 mils, and pressure 0.8-2 torr; wherein the second, local etch step uses C 2 F 6 and O 2 at a flow rate ratio of about (0.85-1):1, electrode spacing 180-350 mils and pressure 6-13 torr; and wherein the power density during both etch steps is about 2.7-5.6 watts/cm 2 .
References Cited (Backward Citations)
US4138306A
Cited
FR2397067A1
Cited
US4529474A
Cited
US4576698A
Cited
WO1985002167A1
Cited
US4534816A
Cited
US4657616A
Cited
WO1987007309A1
Cited
EP0266288A2
Cited
EP0272140A2
Cited
EP0272142A2
Cited
US4960488A
Cited
EP0296891A2
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1995-10-27 | 1996-04-27 | 1996-10-27 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1999-10-27 | 2000-04-27 | 2000-10-27 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2003-10-27 | 2004-04-27 | 2004-10-27 | $7700.00 | Window Closed / Lapsed |