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US5158644A Expired / Lapsed US ⏱️ 0.0 years remaining

Reactor chamber self-cleaning process

Assignee: Applied Materials Inc
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Filing: 1991-10-10
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Granted: 1992-10-27
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Expires: 2011-10-10
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Abstract

Abstract A reactor chamber self-cleaning process is disclosed which uses a fluorocarbon-containing gas and, preferably, C 2 F 6 in combination with oxygen. The two-step process involves, first, a chamber-wide etch at relatively low pressure and with relatively large separation between the gas inlet manifold and the wafer supports which are the RF electrodes and, second, a local etch step which uses a relatively high chamber pressure and smaller electrode spacing, to complete the cleaning of the RF electrodes.

Inventors

  • 👤 David Cheung
  • 👤 Peter Keswick
  • 👤 Jerry Wong

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-01 04:16
CPC Classifications
C; C23; C23C; C23C16/00; C23C16/44; C23C16/4401; C23C16/4405; C23C16/22; C23C16/30; C23C16/40; C23C16/401; C23C16/402; C23C16/455; C23C16/45519; C23C16/45521; C23C16/45563; C23C16/45565; C23C16/50; C23C16/505; C23C16/509; C23C16/5096; C23C16/54; H; H01; H01J; H01J37/00; H01J37/32; H01J37/32009; H01J37/32082; H01J37/32431; H01J37/3244; H01J37/32798; H01J37/32853; H01J37/32862; H10; H10P; H10P14/00; H10P14/60; H10P14/63; H10P14/6326; H10P14/6328; H10P72/00; H10P72/04; H10P72/0402; H10P72/0418; H10P72/0421; Y; Y02; Y02C; Y02C20/00; Y02C20/30; Y02P; Y02P70/00; Y02P70/50; Y10; Y10S; Y10S438/00; Y10S438/905

Claims Analysis

Total Claims: 16
Claim 1
Independent Claim 119 words
A process for self-cleaning a vacuum processing reactor chamber having electrodes in the form of a gas inlet manifold and a wafer support electrode of variable spacing therebetween, comprising: in a first, extended etch step, supplying a fluorocarbon-containing gas into the chamber at a first pressure and a first electrode spacing, with selected power applied between the electrodes, for generating an etching plasma substantially throughout the chamber; and, in a second, local etch step, supplying the fluorocarbon-containing gas into the chamber at a second pressure greater than the first pressure, and a second electrode spacing which is less than the first electrode spacing, with selected power applied between the electrodes, for generating a local etching plasma between the electrodes.
Claim 2
Dependent Claim 119 words
A process for self-cleaning a vacuum processing reactor chamber having electrodes in the form of a gas inlet manifold and a wafer support electrode of variable spacing therebetween, comprising: in a first, extended etch step, supplying a fluorocarbon-containing gas into the chamber at a first pressure and a first electrode spacing, with selected power applied between the electrodes, for generating an etching plasma substantially throughout the chamber; and, in a second, local etch step, supplying the fluorocarbon-containing gas into the chamber at a second pressure greater than the first pressure, and a second electrode spacing which is less than the first electrode spacing, with selected power applied between the electrodes, for generating a local etching plasma between the electrodes.
Claim 3
Dependent Claim 48 words
The process of claim 1, wherein the first, extended etch step uses the gases C 2 F 6 and O 2 at a C 2 F 6 :O 2 flow rate ratio of (0.75-1.30):1, electrode spacing 750-1,000 mils, pressure 0.8-2 torr and power density 2.7-5.6 watts/cm 2 .
Claim 4
Dependent Claim 48 words
The process of claim 1, wherein the second, local etch step uses the gases C 2 F 6 and O 2 at a C 2 F 6 :O 2 flow rate ratio of (0.85-1):1, electrode spacing 180-350 mils, pressure 6-13 torr and power density 2.7-5.6 watts/cm 2 .
Claim 5
Dependent Claim 168 words
A process for self-cleaning a vacuum processing reactor chamber having RF electrodes in the form of a gas inlet manifold and a wafer support electrode of variable spacing therebetween, comprising: in a first, extended etch step supplying the gases C 2 F 6 and O 2 into the chamber at a C 2 F 6 :O 2 flow rate ratio of approximately (0.75-1.30):1, at a chamber pressure of approximately 0.8-2 torr and an electrode spacing of approximately 750-1,000 mils, with RF power density of approximately 2.7-5.6 watts/cm 2 applied between the electrodes for generating an etching plasma substantially throughout the chamber; and, in a second, local etch step, increasing the chamber pressure to a value of approximately 6-13 torr, decreasing the electrode spacing to a value of approximately 180-350 mils with selected RF power density of approximately 2.7-5.6 watts/cm 2 applied between the electrodes and wherein the C 2 F 6 :O 2 flow rate ratio is approximately (0.85-1):1, for generating a local etching plasma between the electrodes.
Claim 6
Dependent Claim 168 words
A process for self-cleaning a vacuum processing reactor chamber having RF electrodes in the form of a gas inlet manifold and a wafer support electrode of variable spacing therebetween, comprising: in a first, extended etch step supplying the gases C 2 F 6 and O 2 into the chamber at a C 2 F 6 :O 2 flow rate ratio of approximately (0.75-1.30):1, at a chamber pressure of approximately 0.8-2 torr and an electrode spacing of approximately 750-1,000 mils, with RF power density of approximately 2.7-5.6 watts/cm 2 applied between the electrodes for generating an etching plasma substantially throughout the chamber; and, in a second, local etch step, increasing the chamber pressure to a value of approximately 6-13 torr, decreasing the electrode spacing to a value of approximately 180-350 mils with selected RF power density of approximately 2.7-5.6 watts/cm 2 applied between the electrodes and wherein the C 2 F 6 :O 2 flow rate ratio is approximately (0.85-1):1, for generating a local etching plasma between the electrodes.
Claim 7
Dependent Claim 44 words
The process of claim 1, wherein the first, extended etch step uses C 2 F 6 flow rate of about 300-600 sccm, O 2 flow rate about 400-800 sccm, pressure about 0.8-2 torr, electrode spacing about 1,000 mils and RF power about 500-750 watts.
Claim 8
Dependent Claim 28 words
The process of claim 5, wherein the C 2 F 6 :O 2 flow rate ratio is 0.75:1 and the RF power density is 3.8-3.9 watts/cm 2 .
Claim 9
Dependent Claim 45 words
The process of claim 1, wherein the second, extended etch step uses a C 2 F 6 flow rate of about 600-800 sccm, O 2 flow rate about 700-900 sccm, pressure about 6-13 torr, electrode spacing about 180-300 mils and RF power about 500-750 watts.
Claim 10
Dependent Claim 29 words
The process of claim 7, wherein the C 2 F 6 :O 2 flow rate ratio is 0.85:1 and the RF power density is about 3.8-3.9 watts/cm 2 .
Claim 11
Dependent Claim 159 words
A process for self-cleaning a vacuum processing reactor chamber having RF electrodes in the form of a gas inlet manifold and a wafer support electrode of variable spacing therebetween, comprising: in a first, extended etch step supplying the gases C 2 F 6 and O 2 into the chamber at respective flow rates 300-600 sccm and 400-800 sccm, at a chamber pressure of approximately 0.8-2 torr, electrode spacing of approximately 1,000 mils, with RF power density of approximately 2.7-5.6 watts/cm 2 applied between the electrodes, for generating an etching plasma substantially throughout the chamber; and, in a second, local etch step, increasing the chamber pressure to approximately 6-13 torr, decreasing the electrode spacing to approximately 80-300 mils with selected RF power of approximately 2.7-5.6 watts/cm 2 applied between the electrodes and wherein the C 2 F 6 and O 2 flow rates are approximately 600-800 sccm and 700-900 sccm, respectively, for generating a local etching plasma between the electrodes.
Claim 12
Dependent Claim 159 words
A process for self-cleaning a vacuum processing reactor chamber having RF electrodes in the form of a gas inlet manifold and a wafer support electrode of variable spacing therebetween, comprising: in a first, extended etch step supplying the gases C 2 F 6 and O 2 into the chamber at respective flow rates 300-600 sccm and 400-800 sccm, at a chamber pressure of approximately 0.8-2 torr, electrode spacing of approximately 1,000 mils, with RF power density of approximately 2.7-5.6 watts/cm 2 applied between the electrodes, for generating an etching plasma substantially throughout the chamber; and, in a second, local etch step, increasing the chamber pressure to approximately 6-13 torr, decreasing the electrode spacing to approximately 80-300 mils with selected RF power of approximately 2.7-5.6 watts/cm 2 applied between the electrodes and wherein the C 2 F 6 and O 2 flow rates are approximately 600-800 sccm and 700-900 sccm, respectively, for generating a local etching plasma between the electrodes.
Claim 13
Dependent Claim 56 words
The process of claim 9, wherein during the first, extended etch step, the C 2 F 6 :O 2 flow rate ratio is 0.75:1, during the second, local etch step, the C 2 F 6 :O 2 flow rate ratio is 0.85:1, and during both steps the RF power density is about 3.8-3.9 watts/cm 2 .
Claim 14
Dependent Claim 152 words
A process for depositing coatings on semiconductor wafers in a vacuum reactor chamber having a gas inlet manifold electrode and a wafer support electrode of variable spacing therebetween, and for self-cleaning the chamber, comprising: repetitively depositing coatings on one or more wafers in the chamber; and applying a process for self-cleaning the internal chamber surfaces, comprising: in a first, extended etch step, supplying a fluorocarbon-containing gas into the chamber at a first chamber pressure and a first electrode spacing with selected RF power applied between the electrodes, for generating an etching plasma substantially throughout the chamber; and, in a second, local etch step, increasing the chamber pressure to a second value which is greater than the first chamber pressure, and decreasing the electrode spacing to a second value which is less than the first electrode spacing with selected power applied between the electrodes, for generating a local etching plasma between the electrodes.
Claim 15
Dependent Claim 152 words
A process for depositing coatings on semiconductor wafers in a vacuum reactor chamber having a gas inlet manifold electrode and a wafer support electrode of variable spacing therebetween, and for self-cleaning the chamber, comprising: repetitively depositing coatings on one or more wafers in the chamber; and applying a process for self-cleaning the internal chamber surfaces, comprising: in a first, extended etch step, supplying a fluorocarbon-containing gas into the chamber at a first chamber pressure and a first electrode spacing with selected RF power applied between the electrodes, for generating an etching plasma substantially throughout the chamber; and, in a second, local etch step, increasing the chamber pressure to a second value which is greater than the first chamber pressure, and decreasing the electrode spacing to a second value which is less than the first electrode spacing with selected power applied between the electrodes, for generating a local etching plasma between the electrodes.
Claim 16
Dependent Claim 80 words
The process of claim 11, wherein the first, extended etch step uses C 2 F 6 and O 2 at a flow rate ratio of about (0.75-1.30):1, electrode spacing 750-1,000 mils, and pressure 0.8-2 torr; wherein the second, local etch step uses C 2 F 6 and O 2 at a flow rate ratio of about (0.85-1):1, electrode spacing 180-350 mils and pressure 6-13 torr; and wherein the power density during both etch steps is about 2.7-5.6 watts/cm 2 .

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1995-10-27 1996-04-27 1996-10-27 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1999-10-27 2000-04-27 2000-10-27 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2003-10-27 2004-04-27 2004-10-27 $7700.00 Window Closed / Lapsed

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