Patent US5873992A successfully refreshed from Google Patents.
US5873992A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Method of electroplating a substrate, and products made thereby
Assignee: University of Arkansas at Little Rock
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Filing: 1997-03-24
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Granted: 1999-02-23
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Expires: 2017-03-24
Abstract
Abstract Disclosed is an electroplating method and products made therefrom, which in one embodiment includes using a current density JO, to form a conductive metal layer having a surface roughness no greater than the surface roughness of the underlying member. In another embodiment of electroplating a substrate surface having peaks and valleys, the method includes electroplating a conductive metal onto the peaks to cover the peaks with the conductive metal, and into the valleys to substantially fill the valleys with the conductive metal.
Inventors
- 👤 John H. Glezen
- 👤 Hameed A. Naseem
- 👤 William D. Brown
- 👤 Leonard W. Schaper
- 👤 Ajay P. Malshe
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-29 11:08
CPC Classifications
C; C25; C25D; C25D5/00; C25D5/10; C25D5/60; C25D5/605
Claims Analysis
Total Claims: 18
Claim 1
Independent Claim
152 words
A method of electroplating an article having a condutive surface with peaks and valleys of initial surface roughness R O , the method comprising: cleaning the conductive surface; and electroplating a conductive metal onto the peaks to cover the peaks with the conductive metal, and into the valleys to substantially fill the valleys with the conductive metal to form an electroplated article having a surface roughness R E , wherein the electroplating is carried out at a current density less than or equal to J O ; wherein J O is a current density which will result in the electroplated article having a surface roughness R E equal to R O ; wherein the article comprises a supporting member and a seed layer; wherein the supporting member comprises diamond, and the seed layer comprises chromium and gold, and the conducting metal comprises gold; and wherein the chromium is adhered to the diamond.
Claim 2
Independent Claim
152 words
A method of electroplating an article having a condutive surface with peaks and valleys of initial surface roughness R O , the method comprising: cleaning the conductive surface; and electroplating a conductive metal onto the peaks to cover the peaks with the conductive metal, and into the valleys to substantially fill the valleys with the conductive metal to form an electroplated article having a surface roughness R E , wherein the electroplating is carried out at a current density less than or equal to J O ; wherein J O is a current density which will result in the electroplated article having a surface roughness R E equal to R O ; wherein the article comprises a supporting member and a seed layer; wherein the supporting member comprises diamond, and the seed layer comprises chromium and gold, and the conducting metal comprises gold; and wherein the chromium is adhered to the diamond.
Claim 3
Independent Claim
132 words
A method of electroplating an article having a conductive surface with a surface roughness R O , the method comprising: cleaning the conductive surface; and electroplating a conductive metal onto the surface utilizing a current density less than or equal to J O , to form a conductive metal layer having a surface roughness R E no greater than the article surface roughness R O ; wherein J O is a current density which will result in the conductive metal layer having a surface roughness R E equal to R O . wherein the article comprises a supporting member and a seed layer: wherein the supporting member comprises diamond, and the seed layer comprises chromium and gold, and the conducting metal comprises gold; and wherein the chromium is adhered to the diamond.
Claim 4
Independent Claim
132 words
A method of electroplating an article having a conductive surface with a surface roughness R O , the method comprising: cleaning the conductive surface; and electroplating a conductive metal onto the surface utilizing a current density less than or equal to J O , to form a conductive metal layer having a surface roughness R E no greater than the article surface roughness R O ; wherein J O is a current density which will result in the conductive metal layer having a surface roughness R E equal to R O . wherein the article comprises a supporting member and a seed layer: wherein the supporting member comprises diamond, and the seed layer comprises chromium and gold, and the conducting metal comprises gold; and wherein the chromium is adhered to the diamond.
Claim 5
Independent Claim
169 words
A method of electroplating an article comprising a supporting member and a seed layer supported by the supporting member, with the seed layer having a conductive surface with peaks and valleys of initial surface roughness R O , the method comprising: cleaning the conductive surface; and electroplating a conductive metal onto the peaks to cover the peaks with the conductive metal and into the valleys to substantially fill the valleys with the conductive metal, to form an electroplated article having a surface roughness R E wherein the electroplating is carried out at a current density less than or equal to J O ; wherein J O is a current density which will result in the conductive metal layer having a surface roughness R E equal to R O , wherein the article comprises a supporting member and a seed layer; wherein the supporting member comprises diamond, and the seed layer comprises chromium and gold, and the conducting metal comprises gold; and wherein the chromium is adhered to the diamond.
Claim 6
Independent Claim
169 words
A method of electroplating an article comprising a supporting member and a seed layer supported by the supporting member, with the seed layer having a conductive surface with peaks and valleys of initial surface roughness R O , the method comprising: cleaning the conductive surface; and electroplating a conductive metal onto the peaks to cover the peaks with the conductive metal and into the valleys to substantially fill the valleys with the conductive metal, to form an electroplated article having a surface roughness R E wherein the electroplating is carried out at a current density less than or equal to J O ; wherein J O is a current density which will result in the conductive metal layer having a surface roughness R E equal to R O , wherein the article comprises a supporting member and a seed layer; wherein the supporting member comprises diamond, and the seed layer comprises chromium and gold, and the conducting metal comprises gold; and wherein the chromium is adhered to the diamond.
Claim 7
Independent Claim
144 words
A method of electroplating an article comprising a diamond member and a seed layer supported by the diamond member, with the seed layer having a conducting surface with a surface roughness R O , the method comprising cleaning the conductive surface; and electroplating a conductive metal onto the seed layer surface utilizing a current density less than or equal to J O , to form a conductive metal layer having a surface roughness no greater than the seed layer surface roughness R O ; wherein J O is a current density which will result in the conductive metal layer having a surface roughness R E equal to R O . wherein the article comprises a supporting member and a seed layer; wherein the seed layer comprises chromium and gold, and the conducting metal comprises gold; and wherein the chromium is adhered to the diamond.
Claim 8
Independent Claim
144 words
A method of electroplating an article comprising a diamond member and a seed layer supported by the diamond member, with the seed layer having a conducting surface with a surface roughness R O , the method comprising cleaning the conductive surface; and electroplating a conductive metal onto the seed layer surface utilizing a current density less than or equal to J O , to form a conductive metal layer having a surface roughness no greater than the seed layer surface roughness R O ; wherein J O is a current density which will result in the conductive metal layer having a surface roughness R E equal to R O . wherein the article comprises a supporting member and a seed layer; wherein the seed layer comprises chromium and gold, and the conducting metal comprises gold; and wherein the chromium is adhered to the diamond.
Claim 9
Independent Claim
162 words
A method of metallizing a diamond film comprising: a applying a seed metal onto the diamond film to form a seed layer having a surface roughness R O , with the seed layer having a conductive surface with peaks and valleys; (b) cleaning the conductive surface; and (c) electroplating a conductive metal onto the peaks to cover the peaks with the conductive metal, and into the valleys to substantially fill the valleys with the conductive metal, to form an electroplated article having a surface roughness R E , wherein the electroplating is carried out at a current density less than or equal to J O ; wherein J O is a current density which will result in the electroplated article having a surface roughness R E equal to R O , wherein the seed metal comprises chromium, and the diamond film is heated to a temperature in the range of about 150° C. to about 400° C. prior to applying the chromium.
Claim 10
Independent Claim
162 words
A method of metallizing a diamond film comprising: a applying a seed metal onto the diamond film to form a seed layer having a surface roughness R O , with the seed layer having a conductive surface with peaks and valleys; (b) cleaning the conductive surface; and (c) electroplating a conductive metal onto the peaks to cover the peaks with the conductive metal, and into the valleys to substantially fill the valleys with the conductive metal, to form an electroplated article having a surface roughness R E , wherein the electroplating is carried out at a current density less than or equal to J O ; wherein J O is a current density which will result in the electroplated article having a surface roughness R E equal to R O , wherein the seed metal comprises chromium, and the diamond film is heated to a temperature in the range of about 150° C. to about 400° C. prior to applying the chromium.
Claim 11
Dependent Claim
12 words
The method of claim 5 wherein the seed metal further comprises gold.
Claim 12
Dependent Claim
11 words
The method of claim 6 wherein the conductive metal comprises gold.
Claim 13
Dependent Claim
26 words
The method of claim 7 wherein the electroplating is conducted at a current density in the range of about 0.001 to about 0.095 mA/cm 2 .
Claim 14
Independent Claim
139 words
A method of metallizing a diamond film comprising: (a) applying a seed metal onto the diamond film to form a seed layer, with the seed layer having a conductive surface with a surface roughness R O ; and (b) electroplating a conductive metal onto the seed layer surface utilizing a current density less than or equal to J O , to form a conductive metal layer having a surface roughness R E no greater than the seed layer surface roughness R O ; wherein J O is a current density which will result in the electroplated article having a surface roughness R E equal to R O ; wherein the seed metal comprises chromium, and the diamond film is heated to a temperature in the range of about 150° C. to about 400° C. prior to applying the chromium.
Claim 15
Independent Claim
139 words
A method of metallizing a diamond film comprising: (a) applying a seed metal onto the diamond film to form a seed layer, with the seed layer having a conductive surface with a surface roughness R O ; and (b) electroplating a conductive metal onto the seed layer surface utilizing a current density less than or equal to J O , to form a conductive metal layer having a surface roughness R E no greater than the seed layer surface roughness R O ; wherein J O is a current density which will result in the electroplated article having a surface roughness R E equal to R O ; wherein the seed metal comprises chromium, and the diamond film is heated to a temperature in the range of about 150° C. to about 400° C. prior to applying the chromium.
Claim 16
Dependent Claim
12 words
The method of claim 9 wherein the seed metal further comprises gold.
Claim 17
Dependent Claim
11 words
The method of claim 10 wherein the conductive metal comprises gold.
Claim 18
Dependent Claim
26 words
The method of claim 11 wherein the electroplating is conducted at a current density in the range of about 0.001 to about 0.095 mA/cm 2 .
References Cited (Backward Citations)
US3518168A
Cited
US3515649A
Cited
US3549507A
Cited
US3695854A
Cited
US3930963A
Cited
US3982235A
Cited
US5110422A
Cited
US5190796A
Cited
US5366814A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 2002-02-22 | 2002-08-24 | 2003-02-23 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 2006-02-22 | 2006-08-24 | 2007-02-23 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2010-02-22 | 2010-08-24 | 2011-02-23 | $7700.00 | Window Closed / Lapsed |