Patent US4832891A successfully refreshed from Google Patents.
US4832891A
Expired / Lapsed
US
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Method of making an epoxy bonded rare earth-iron magnet
Assignee: Eastman Kodak Co
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Filing: 1987-11-25
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Granted: 1989-05-23
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Expires: 2007-11-25
Abstract
Abstract A method of making a bonded permanent magnet including the steps of dissolving, in a solvent, an uncured epoxy resin having an incorporated catalyst which is inactive at a temperature of about 120° F. Particles of a rapidly quenched rare earth-iron-boron alloy are added to the epoxy resin solution. The solution with the particles are mixed at a temperature of about 120° F. until the solvent is removed and the magnetic particles are substantially uniformly coated with the resin. The epoxy coated particles are then cold-pressed into a compact to form a magnet and the epoxy compact is then cured by heating.
Inventors
- 👤 Allen Kass
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-30 16:20
CPC Classifications
H; H01; H01F; H01F1/00; H01F1/01; H01F1/03; H01F1/032; H01F1/04; H01F1/047; H01F1/053; H01F1/055; H01F1/057; H01F1/0571; H01F1/0575; H01F1/0578; C; C08; C08K; C08K3/00; C08K3/02; C08K3/08; Y; Y10; Y10S; Y10S264/00; Y10S264/58; Y10T; Y10T29/00; Y10T29/49; Y10T29/49002; Y10T29/4902; Y10T29/49075; Y10T29/49076
Claims Analysis
Total Claims: 10
Claim 1
Independent Claim
125 words
The method of making a bonded permanent magnet comprising the steps of: dissolving in a solvent an uncured epoxy resin having an incorporated catalyst which is inactive at a temperature of about 120° F.; adding particles of a rapidly quenched rare earth-iron-boron alloy to the epoxy resin solution; mixing said solution with said particles at a temperature of about 120° F. until said solvent is removed and said particles are substantially uniformly coated with said resin and are insubstantially free flowing powder form; cold pressing the epoxy resin coated particles into a compact to form a magnet; and curing said epoxy resin by heating said compact to a temperature of between about 250° F. and about 350° F. for a period of about 1-2 hours.
Claim 2
Independent Claim
125 words
The method of making a bonded permanent magnet comprising the steps of: dissolving in a solvent an uncured epoxy resin having an incorporated catalyst which is inactive at a temperature of about 120° F.; adding particles of a rapidly quenched rare earth-iron-boron alloy to the epoxy resin solution; mixing said solution with said particles at a temperature of about 120° F. until said solvent is removed and said particles are substantially uniformly coated with said resin and are insubstantially free flowing powder form; cold pressing the epoxy resin coated particles into a compact to form a magnet; and curing said epoxy resin by heating said compact to a temperature of between about 250° F. and about 350° F. for a period of about 1-2 hours.
Claim 3
Dependent Claim
22 words
The method according to claim 1 wherein said uncured epoxy resin equals about 1.3 to 3 weight percent of the final compact.
Claim 4
Dependent Claim
33 words
The method according to claim 1 wherein said epoxy resin is cured by heating to about 250° F. for about one hour and then heating at about 350° F. for about one hour.
Claim 5
Dependent Claim
20 words
The method according to claim 1 wherein said particles of rare earth-iron boron alloy have a size of about 30-550μ.
Claim 6
Dependent Claim
17 words
The method according to claim 1 wherein said cured compact has a density of about 5.0-6.0 gm/cc.
Claim 7
Dependent Claim
19 words
The method according to claim 1 wherein said mixing occurs under a vacuum of about 25-29 inches of Hg.
Claim 8
Dependent Claim
19 words
The method according to claim 1 wherein said coated particles are pressed at a pressure of about 100,000 psi.
Claim 9
Independent Claim
179 words
The method of making bonded permanent magnet comprising the steps of: dissolving in an acetone solvent an uncured thermally curable biphenol A epoxy resin having an incorporated catalyst which is inactive at a temperature of about 120° F.; adding magnetic particles of a rapidly quenched rare earth-iron-boron alloy having a size of from about 30μ to about 500μ to the epoxy resin solution whereby said resin equals about 1.3 to 3 weight percent of the final compact; mixing said solution with said magnetic particles at a temperature of about 120° F. and at a vacuum of about 25-29 inches of Hg until said solvent is removed and said magnetic particles are substantially uniformly coated with said resin and are in substantially free flowing powder from; cold pressing the epoxy resin coated particles at a pressure of about 100,000 psi into a compact having a density of about 5.0-6.0 gm/cc to form a magnet; and curing said epoxy resin by heating said compact to about 250° F. for one hour and then heating at 350° F. for an additional hour.
Claim 10
Independent Claim
179 words
The method of making bonded permanent magnet comprising the steps of: dissolving in an acetone solvent an uncured thermally curable biphenol A epoxy resin having an incorporated catalyst which is inactive at a temperature of about 120° F.; adding magnetic particles of a rapidly quenched rare earth-iron-boron alloy having a size of from about 30μ to about 500μ to the epoxy resin solution whereby said resin equals about 1.3 to 3 weight percent of the final compact; mixing said solution with said magnetic particles at a temperature of about 120° F. and at a vacuum of about 25-29 inches of Hg until said solvent is removed and said magnetic particles are substantially uniformly coated with said resin and are in substantially free flowing powder from; cold pressing the epoxy resin coated particles at a pressure of about 100,000 psi into a compact having a density of about 5.0-6.0 gm/cc to form a magnet; and curing said epoxy resin by heating said compact to about 250° F. for one hour and then heating at 350° F. for an additional hour.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1992-05-22 | 1992-11-21 | 1993-05-23 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1996-05-22 | 1996-11-21 | 1997-05-23 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 2000-05-22 | 2000-11-21 | 2001-05-23 | $7700.00 | Window Closed / Lapsed |