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US5660880A Expired / Lapsed US ⏱️ 0.0 years remaining

Anti-oxidation protection of carbon-based materials

Assignee: Airbus Group SAS
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Filing: 1993-12-16
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Granted: 1997-08-26
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Expires: 2013-12-16
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Abstract

Abstract The invention relates to a process for obtaining refractory antioxidative coatings on carbon-based materials and articles operating in an oxidizing environment at temperatures of up to 2000° C. under thermal cycling and high-speed gas stream conditions. The process comprises the heat-treatment of the surface to be protected in silicon vapors and is characterized in that prior to said silicon vapor treatment, the surface to be protected is covered with a layer of the composition consisting of HfB 2 +C powdery filler and a carboxymethyl cellulose-based binder, followed by drying under normal conditions till it is completely dry. The process is intended for oxidation protection of structural elements and articles in metallurgy, aircraft, and other industries.

Inventors

  • 👤 Valeriya Veniaminovna Rodionova
  • 👤 Gennady Alexandrovich Kravetkii
  • 👤 Nadezhda Miklailovna Schestakova
  • 👤 Andrey Vasiljevich Kuznetzov
  • 👤 Valery Ivanovich Kostikov
  • 👤 Alexander Victorovich Demin

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-24 13:44
CPC Classifications
C; C04; C04B; C04B41/00; C04B41/009; C04B41/45; C04B41/50; C04B41/5053; C04B41/5057; C04B41/5059; C04B41/52; C04B41/80; C04B41/81; C04B41/85; C04B41/87; C04B41/89

Claims Analysis

Total Claims: 9
Claim 1
Independent Claim 69 words
A process for obtaining protective coatings on carbon-based materials and articles, which comprises heat treatment of the surface to be protected in silicon vapors, characterized in that prior to said silicon vapor treatment, the surface to be protected is covered with a layer of a composition consisting of HfB 2 +C powdery filler and a carboxymethyl cellulose-based binder, followed by drying under ambient conditions till it is completely dry.
Claim 2
Dependent Claim 69 words
A process for obtaining protective coatings on carbon-based materials and articles, which comprises heat treatment of the surface to be protected in silicon vapors, characterized in that prior to said silicon vapor treatment, the surface to be protected is covered with a layer of a composition consisting of HfB 2 +C powdery filler and a carboxymethyl cellulose-based binder, followed by drying under ambient conditions till it is completely dry.
Claim 3
Dependent Claim 26 words
A process according to claim 1, characterized in that said powdery components of said composition are taken in the HfB 2 : C ratio of 95:5.
Claim 4
Dependent Claim 15 words
A process according to claim 1, characterized in that C powdery filler is carbon black.
Claim 5
Dependent Claim 16 words
A process according to claim 1, characterized in that said C powdery filler is artificial graphite.
Claim 6
Dependent Claim 15 words
A process according to claim 1, characterized in that said C powdery filler is coke.
Claim 7
Dependent Claim 29 words
A process according to claim 1, characterized in that said carboxymethyl cellulose is used as a 5% aqueous solution in the volume ratio to said powdery components of 1:1.
Claim 8
Dependent Claim 42 words
A process according to claim 1, characterized in that said HfB 2 +C layer is treated in silicon vapors under a pressure of not over 10 Hg mm, at a temperature of about 1850° to 1900° C., for 1 to 3 h.
Claim 9
Dependent Claim 36 words
A process according to claim 1, characterized in that said layer of the composition consisting of the HfB 2 +C filler and the carboxymethyl cellulose-based binder is applied onto a non-siliconized carbon material or article substrate.

References Cited (Backward Citations)

DE1122465B Cited
US3770487A Cited
EP0428977A1 Cited
EP0435039A1 Cited
EP0448432A1 Cited
US5368940A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 2000-08-25 2001-02-24 2001-08-26 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 2004-08-25 2005-02-24 2005-08-26 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2008-08-25 2009-02-24 2009-08-26 $7700.00 Window Closed / Lapsed

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