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US5096533A Expired / Lapsed US ⏱️ 0.0 years remaining

Molecular beam epitaxial growth device and molecular beam control method therein for exactly controlling thickness and composition of epitaxial film

Assignee: Fujitsu Ltd
•
Filing: 1991-03-20
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Granted: 1992-03-17
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Expires: 2011-03-20
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Abstract

Abstract A measured molecular beam intensity V i is converted into a value V io at a reference temperature T O by calculating the following equation using the measured molecular beam intensity V i and a measured cell temperature T i : V io =V i ·exp(A(1/T O -1/T i )). Next, a molecular beam intensity V O (t) at a time (t) is estimated after the last conversion time based on the reference temperature T o in accordance with the converted molecular beam intensity V io and a corresponding time t i thereof. Further, the temperature of a molecular beam source cell is controlled in accordance with an estimated cell temperature T SP (V SP ), to realize a predetermined molecular beam intensity V SP , given by calculating the following equation using the estimated molecular beam intensity V O (t) and the predetermined molecular beam intensity V SP : T SP (V SP )=1/(1/T O +(log(V SP /V O (t)))/A).

Inventors

  • 👤 Takeshi Igarashi

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-29 22:35
CPC Classifications
C; C23; C23C; C23C14/00; C23C14/22; C23C14/54; C23C14/542; C23C14/543; C23C14/544; C23C14/548; C30; C30B; C30B23/00; C30B23/002

Claims Analysis

Total Claims: 14
Claim 1
Independent Claim 181 words
A molecular beam control method in a molecular beam epitaxial growth device comprising the steps of: measuring a temperature T i of a molecular beam source cell; measuring an intensity V i of a molecular beam from said molecular beam source cell; converting the measured molecular beam intensity V i into a value V iO at a reference temperature T O by calculating the following equation using the measured molecular beam intensity V i and the measured cell temperature T i , ##EQU20## estimating a molecular beam intensity V O (t) at a time (t) after the last conversion time based on the reference temperature T O in accordance with the converted molecular beam intensity V iO and a corresponding time t i thereof; and controlling a temperature of said molecular beam source cell in accordance with an estimated cell temperature T SP (V SP ), to realize a predetermined molecular beam intensity V SP , given by calculating the following equation using the estimated molecular beam intensity V O (t) and the predetermined molecular beam intensity V SP , ##EQU21##
Claim 2
Dependent Claim 181 words
A molecular beam control method in a molecular beam epitaxial growth device comprising the steps of: measuring a temperature T i of a molecular beam source cell; measuring an intensity V i of a molecular beam from said molecular beam source cell; converting the measured molecular beam intensity V i into a value V iO at a reference temperature T O by calculating the following equation using the measured molecular beam intensity V i and the measured cell temperature T i , ##EQU20## estimating a molecular beam intensity V O (t) at a time (t) after the last conversion time based on the reference temperature T O in accordance with the converted molecular beam intensity V iO and a corresponding time t i thereof; and controlling a temperature of said molecular beam source cell in accordance with an estimated cell temperature T SP (V SP ), to realize a predetermined molecular beam intensity V SP , given by calculating the following equation using the estimated molecular beam intensity V O (t) and the predetermined molecular beam intensity V SP , ##EQU21##
Claim 3
Dependent Claim 85 words
A molecular beam control method, as claimed in claim 1, wherein the step of measuring the temperature T i of said molecular beam source cell and the step of measuring the intensity V i of the molecular beam from said molecular beam source cell are carried out at the time of growing a buffer layer on a substrate, and the step of controlling the temperature of said molecular beam source cell is carried out at the time of growing a device layer on said substrate.
Claim 4
Dependent Claim 55 words
A molecular beam control method, as claimed in claim 1, wherein the step of measuring the temperature T i of said molecular beam source cell and the step of measuring the intensity V i of the molecular beam from said molecular beam source cell are carried out when stopping the growth of an epitaxial film.
Claim 5
Dependent Claim 28 words
A molecular beam control method, as claimed in claim 1, wherein said molecular beam control method is used for forming a compound semiconductor made of group III-V materials.
Claim 6
Dependent Claim 30 words
A molecular beam control method, as claimed in claim 4, wherein said group III materials include Aluminum, Gallium, or Indium, and said group V materials include Phosphorus, Antimony or Arsenic.
Claim 7
Dependent Claim 53 words
A molecular beam control method, as claimed in claim 4, wherein the step of measuring the temperature T i of said molecular beam source cell and the step of measuring the intensity V i of the molecular beam from said molecular beam source cell are carried out for only said group III materials.
Claim 8
Dependent Claim 204 words
A molecular beam control method in a molecular beam epitaxial growth device comprising the steps of: measuring a temperature T i of a molecular beam source cell; measuring an intensity V i of a molecular beam from said molecular beam source cell; converting the measured molecular beam intensity V i into a value V iO at a reference temperature T O by calculating the following equation using the measured molecular beam intensity V i and the measured cell temperature T i , ##EQU22## estimating a molecular beam intensity V O (t) at a time (t) after the last conversion time based on the reference temperature T O in accordance with the converted molecular beam intensity V iO and a corresponding time t i thereof; calculating a molecular beam intensity V SP (T SP ) at a cell temperature T SP by calculating the following equation using the estimated molecular beam intensity V O (t) and the cell temperature T SP at the time (t) of the estimated molecular beam intensity V O (t), ##EQU23## and controlling a shutter of said molecular beam source cell by using an integrated value relating to the time factor of the molecular beam intensity V SP (T SP ).
Claim 9
Dependent Claim 204 words
A molecular beam control method in a molecular beam epitaxial growth device comprising the steps of: measuring a temperature T i of a molecular beam source cell; measuring an intensity V i of a molecular beam from said molecular beam source cell; converting the measured molecular beam intensity V i into a value V iO at a reference temperature T O by calculating the following equation using the measured molecular beam intensity V i and the measured cell temperature T i , ##EQU22## estimating a molecular beam intensity V O (t) at a time (t) after the last conversion time based on the reference temperature T O in accordance with the converted molecular beam intensity V iO and a corresponding time t i thereof; calculating a molecular beam intensity V SP (T SP ) at a cell temperature T SP by calculating the following equation using the estimated molecular beam intensity V O (t) and the cell temperature T SP at the time (t) of the estimated molecular beam intensity V O (t), ##EQU23## and controlling a shutter of said molecular beam source cell by using an integrated value relating to the time factor of the molecular beam intensity V SP (T SP ).
Claim 10
Dependent Claim 58 words
A molecular beam control method, as claimed in claim 7, wherein the step of measuring the temperature T i of said molecular beam source cell and the step of measuring the intensity V i of the molecular beam from said molecular beam source cell are carried out at the time of growing a buffer layer of a substrate.
Claim 11
Dependent Claim 55 words
A molecular beam control method, as claimed in claim 7, wherein the step of measuring the temperature T i of said molecular beam source cell and the step of measuring the intensity V i of the molecular beam from said molecular beam source cell are carried out when stopping the growth of an epitaxial film.
Claim 12
Dependent Claim 28 words
A molecular beam control method, as claimed in claim 7, wherein said molecular beam control method is used for forming a compound semiconductor made of group III-V materials.
Claim 13
Dependent Claim 30 words
A molecular beam control method, as claimed in claim 10, wherein said group III materials include Aluminum, Gallium, or Indium, and said group V materials include Phosphorus, Antimony or Arsenic.
Claim 14
Dependent Claim 53 words
A molecular beam control method, as claimed in claim 10, wherein the step of measuring the temperature T i of said molecular beam source cell and the step of measuring the intensity V i of the molecular beam from said molecular beam source cell are carried out for only said group III materials.

References Cited (Backward Citations)

US3839084A Cited
US4119846A Cited
JPS53125761A Cited
JPS5552220A Cited
JPS5833824A Cited
JPS58119630A Cited
US4855013A Cited
US4636268A Cited
JPH0226888A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1995-03-17 1995-09-16 1996-03-17 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1999-03-17 1999-09-16 2000-03-17 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 2003-03-17 2003-09-16 2004-03-17 $7700.00 Window Closed / Lapsed

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